Rotating disk viscometer

Last updated

The Rotating disk viscometer, or "Mooney Machine" as it is sometimes referred to in the rubber industry, is the standard viscometer for measuring material viscosity and scorch time for rubber before vulcanization. It was developed in the 1930s by Melvin Mooney. [1] For a specific temperature, scorch time describes how long it will take the material to vulcanize. For example, a scorch time at ambient temperature indicates the rubber will be able to remain unvulcanized at room temperature for an extended period of time.

Overview

The Mooney machine itself consists of a cylindrical, serrated, metal disk designed to hold a material sample without slippage during rotation. This disk is surrounded by a die chamber where the rubber is pressed with 2500 pounds of force. The rubber is then warmed for two minutes. Next, the serrated disk is rotated, in one direction only, at a speed of 2 revolutions per minute, while the torque required to rotate the disk is recorded. The torque decrease per time can be directly related to viscosity.

As the material further warms during initial rotation of the serrated disk and the rubber begins to shear, the viscosity lowers and torque required decreases. Eventually, the torque will reach an inflection point, where the rubber begins to vulcanize and torque begins increasing. A shear pin on the machine prevents damage as the testing material stiffens. Comparing the torque versus time curves for different materials allows direct correlation of material viscosity and scorch time.

Related Research Articles

<span class="mw-page-title-main">Tesla turbine</span> Bladeless centripetal flow turbine

The Tesla turbine is a bladeless centripetal flow turbine invented by Nikola Tesla in 1913. It functions as nozzles apply a moving fluid to the edges of a set of discs. The engine uses smooth discs rotating in a chamber to generate rotational movement due to the momentum exchange between the fluid and the discs. The discs are arranged in an orientation similar to a stack of CDs on a pole.

A viscometer is an instrument used to measure the viscosity of a fluid. For liquids with viscosities which vary with flow conditions, an instrument called a rheometer is used. Thus, a rheometer can be considered as a special type of viscometer. Viscometers can measure only constant viscosity, that is, viscosity that does not change with flow conditions.

<span class="mw-page-title-main">Ball bearing</span> Type of rolling-element bearing

A ball bearing is a type of rolling-element bearing that uses balls to maintain the separation between the bearing races.

Fluid bearings are bearings in which the load is supported by a thin layer of rapidly moving pressurized liquid or gas between the bearing surfaces. Since there is no contact between the moving parts, there is no sliding friction, allowing fluid bearings to have lower friction, wear and vibration than many other types of bearings. Thus, it is possible for some fluid bearings to have near-zero wear if operated correctly.

Hemorheology, also spelled haemorheology, or blood rheology, is the study of flow properties of blood and its elements of plasma and cells. Proper tissue perfusion can occur only when blood's rheological properties are within certain levels. Alterations of these properties play significant roles in disease processes. Blood viscosity is determined by plasma viscosity, hematocrit and mechanical properties of red blood cells. Red blood cells have unique mechanical behavior, which can be discussed under the terms erythrocyte deformability and erythrocyte aggregation. Because of that, blood behaves as a non-Newtonian fluid. As such, the viscosity of blood varies with shear rate. Blood becomes less viscous at high shear rates like those experienced with increased flow such as during exercise or in peak-systole. Therefore, blood is a shear-thinning fluid. Contrarily, blood viscosity increases when shear rate goes down with increased vessel diameters or with low flow, such as downstream from an obstruction or in diastole. Blood viscosity also increases with increases in red cell aggregability.

<span class="mw-page-title-main">Mixing (process engineering)</span> Process of mechanically stirring a heterogeneous mixture to homogenize it

In industrial process engineering, mixing is a unit operation that involves manipulation of a heterogeneous physical system with the intent to make it more homogeneous. Familiar examples include pumping of the water in a swimming pool to homogenize the water temperature, and the stirring of pancake batter to eliminate lumps (deagglomeration).

In materials science and continuum mechanics, viscoelasticity is the property of materials that exhibit both viscous and elastic characteristics when undergoing deformation. Viscous materials, like water, resist shear flow and strain linearly with time when a stress is applied. Elastic materials strain when stretched and immediately return to their original state once the stress is removed.

<span class="mw-page-title-main">Elastomer</span> Polymer with rubber-like elastic properties

An elastomer is a polymer with viscoelasticity and with weak intermolecular forces, generally low Young's modulus (E) and high failure strain compared with other materials. The term, a portmanteau of elastic polymer, is often used interchangeably with rubber, although the latter is preferred when referring to vulcanisates. Each of the monomers which link to form the polymer is usually a compound of several elements among carbon, hydrogen, oxygen and silicon. Elastomers are amorphous polymers maintained above their glass transition temperature, so that considerable molecular reconformation is feasible without breaking of covalent bonds. At ambient temperatures, such rubbers are thus relatively compliant and deformable. Their primary uses are for seals, adhesives and molded flexible parts.

<span class="mw-page-title-main">Extrusion</span> Process of pushing material through a die to create long symmetrical-shaped objects

Extrusion is a process used to create objects of a fixed cross-sectional profile by pushing material through a die of the desired cross-section. Its two main advantages over other manufacturing processes are its ability to create very complex cross-sections; and to work materials that are brittle, because the material encounters only compressive and shear stresses. It also creates excellent surface finish and gives considerable freedom of form in the design process.

<span class="mw-page-title-main">Rheometer</span> Scientific instrument used to measure fluid flow (rheology)

A rheometer is a laboratory device used to measure the way in which a viscous fluid flows in response to applied forces. It is used for those fluids which cannot be defined by a single value of viscosity and therefore require more parameters to be set and measured than is the case for a viscometer. It measures the rheology of the fluid.

Spin casting, also known as centrifugal rubber mold casting (CRMC), is a method of utilizing inertia to produce castings from a rubber mold. Typically, a disc-shaped mold is spun along its central axis at a set speed. The casting material, usually molten metal or liquid thermoset plastic, is then poured in through an opening at the top-center of the mold. The filled mold then continues to spin as the metal solidifies.

<span class="mw-page-title-main">Tire manufacturing</span> Process of tire fabrication

Pneumatic tires are manufactured according to relatively standardized processes and machinery, in around 455 tire factories in the world. With over 1 billion tires manufactured worldwide annually, the tire industry is a major consumer of natural rubber. Tire factories start with bulk raw materials such as synthetic rubber, carbon black, and chemicals and produce numerous specialized components that are assembled and cured.

<span class="mw-page-title-main">Melvin Mooney</span>

Melvin Mooney (1893–1968) was an American physicist and rheologist.

Injection molding of liquid silicone rubber (LSR) is a process to produce pliable, durable parts in high volume.

Brookfield Engineering is an engineering and manufacturing company with headquarters in Middleboro, Massachusetts. It is a subsidiary of the conglomerate Ametek. Its product line includes laboratory viscometers, rheometers, texture analyzers, and powder flow testers as well as in-line process instrumentation. These instruments are used by research, design, and process control departments.

<span class="mw-page-title-main">Viscosity</span> Resistance of a fluid to shear deformation

The viscosity of a fluid is a measure of its resistance to deformation at a given rate. For liquids, it corresponds to the informal concept of "thickness": for example, syrup has a higher viscosity than water. Viscosity is defined scientifically as a force multiplied by a time divided by an area. Thus its SI units are newton-seconds per square meter, or pascal-seconds.

<span class="mw-page-title-main">Mooney viscometer</span>

A Mooney viscometer is an instrument used for measuring the Mooney viscosity of rubbers. Invented by Melvin Mooney, it contains a rotating spindle and heated dies, the substance encloses and overflows the spindle and the mooney viscosity is calculated from the torque on the spindle.

The viscous stress tensor is a tensor used in continuum mechanics to model the part of the stress at a point within some material that can be attributed to the strain rate, the rate at which it is deforming around that point.

Rheological weldability (RW) of thermoplastics considers the materials flow characteristics in determining the weldability of the given material. The process of welding thermal plastics requires three general steps, first is surface preparation. The second step is the application of heat and pressure to create intimate contact between the components being joined and initiate inter-molecular diffusion across the joint and the third step is cooling. RW can be used to determine the effectiveness of the second step of the process for given materials.

Squeeze flow is a type of flow in which a material is pressed out or deformed between two parallel plates or objects. First explored in 1874 by Josef Stefan, squeeze flow describes the outward movement of a droplet of material, its area of contact with the plate surfaces, and the effects of internal and external factors such as temperature, viscoelasticity, and heterogeneity of the material. Several squeeze flow models exist to describe Newtonian and non-Newtonian fluids undergoing squeeze flow under various geometries and conditions. Numerous applications across scientific and engineering disciplines including rheometry, welding engineering, and materials science provide examples of squeeze flow in practical use.

References

  1. Horve, Les (1996). Shaft Seals for Dynamic Applications. New York: Marcel Dekker, Inc. p. 17. ISBN   0-8247-9716-7.