Spinlock SRL

Last updated
Spinlock
Type Private corporation
Founded2003 in Argentina
FounderDr. Daniel J. Pusiol
Headquarters,
Key people
Dr. Daniel J. Pusiol, President; Eng. Gabriela Albert, CEO; Eng. Amadeo Sasia CTO; ID. Bernardo Ballesté, COO
ProductsSLK 200, SLK GOW, MFM III, MRI 1400, PM SERIES
Number of employees
25
Website http://spinlock.com.ar/

Spinlock is a technology based company specialized in the manufacture and development of nuclear magnetic resonance (NMR) and nuclear quadrupole resonance (NQR) equipment.

Contents

History

Spinlock was founded in 2003 by Dr. Daniel J. Pusiol, a renowned physicist specialized in NMR and NQR, professor at the National University of Córdoba and member of the National Scientific and Technical Research Council (CONICET) of Argentina.

Mr. Pusiol lead a team of young researchers to build Spinlock, manufacturing NMR spectrometers and providing Research and Development services for different industries, engaging on the discovery of new applications for the NMR technology.

Closely related to the National University of Córdoba, Spinlock contributes with the University on projects and receives continuous support in the form of education and consultation with leading scientists. [1]

The organization employs scientist and technical staff from diverse areas: engineering, physics, chemistry and computer sciences.

Spinlock has shared its knowledge in international publications and forums (see Determinación del contenido de ácido oleico en semillas de maní por medio de la resonancia magnética nuclear (RMN)).

Product lines

SLK - 100: (discontinued product) This Spectrometer use NMR spectroscopy to carry out a variety of analysis in food industry processes [2] (e.g. moisture and fat content in food; oil and fatty acids in oily seeds [3] and olives; solid and liquid fat ratio in cheese, chocolate and other dairy products).

SLK - 200: Desktop magnetic resonance equipment for measurement of oil or fat, moisture, fatty acid and protein content. Simultaneous, non-destructive and automated determination.

SLK-GOW Multiphase Water-Cut Meter: Resonance magnetic equipment for multiphase measurement Oil, water and gas. Deviates a multiphase sample to a secondary line (Bypass system). Water Cut Measurement (net oil and water), Gas Volume Fraction (GVF) and Oil Viscosity.

SLK-MFM-III Multiphase flow meter prototype equipment for magnetic resonance. Measures flow and cut of multiphase fluid, including water, gas and oil. Built for ø2´ lines with ø2´ Halbach magnet.

SLK-MRI-1400 Time domain magnetic resonance equipment (TD-NMR) suitable for imaging (MRI) with an ø 4´ circular Halbach magnet, with temperature control and compensation.

SLK-1000-PM Desktop magnetic resonance equipment for measurements of sidewall cores (core plugs) and other oil rock samples. Equipment for ambient pressure and temperature samples.

SLK-2000-PM Desktop magnetic resonance equipment for measurements of sidewall cores (core plugs) and other oil rock samples. Shale rock measurement capacity. It includes Z-gradient for diffusion experiments. Equipment suitable for high pressure and high temperature sample measurements

Related Research Articles

Magnetic resonance imaging Medical imaging technique

Magnetic resonance imaging (MRI) is a medical imaging technique used in radiology to form pictures of the anatomy and the physiological processes of the body. MRI scanners use strong magnetic fields, magnetic field gradients, and radio waves to generate images of the organs in the body. MRI does not involve X-rays or the use of ionizing radiation, which distinguishes it from CT and PET scans. MRI is a medical application of nuclear magnetic resonance (NMR) which can also be used for imaging in other NMR applications, such as NMR spectroscopy.

Fourier-transform spectroscopy is a measurement technique whereby spectra are collected based on measurements of the coherence of a radiative source, using time-domain or space-domain measurements of the radiation, electromagnetic or not. It can be applied to a variety of types of spectroscopy including optical spectroscopy, infrared spectroscopy, nuclear magnetic resonance (NMR) and magnetic resonance spectroscopic imaging (MRSI), mass spectrometry and electron spin resonance spectroscopy.

Nuclear quadrupole resonance spectroscopy or NQR is a chemical analysis technique related to nuclear magnetic resonance (NMR). Unlike NMR, NQR transitions of nuclei can be detected in the absence of a magnetic field, and for this reason NQR spectroscopy is referred to as "zero Field NMR". The NQR resonance is mediated by the interaction of the electric field gradient (EFG) with the quadrupole moment of the nuclear charge distribution. Unlike NMR, NQR is applicable only to solids and not liquids, because in liquids the quadrupole moment averages out. Because the EFG at the location of a nucleus in a given substance is determined primarily by the valence electrons involved in the particular bond with other nearby nuclei, the NQR frequency at which transitions occur is unique for a given substance. A particular NQR frequency in a compound or crystal is proportional to the product of the nuclear quadrupole moment, a property of the nucleus, and the EFG in the neighborhood of the nucleus. It is this product which is termed the nuclear quadrupole coupling constant for a given isotope in a material and can be found in tables of known NQR transitions. In NMR, an analogous but not identical phenomenon is the coupling constant, which is also the result of an internuclear interaction between nuclei in the analyte.

Well logging, also known as borehole logging is the practice of making a detailed record of the geologic formations penetrated by a borehole. The log may be based either on visual inspection of samples brought to the surface or on physical measurements made by instruments lowered into the hole. Some types of geophysical well logs can be done during any phase of a well's history: drilling, completing, producing, or abandoning. Well logging is performed in boreholes drilled for the oil and gas, groundwater, mineral and geothermal exploration, as well as part of environmental and geotechnical studies.

In nuclear magnetic resonance (NMR) spectroscopy, the chemical shift is the resonant frequency of a nucleus relative to a standard in a magnetic field. Often the position and number of chemical shifts are diagnostic of the structure of a molecule. Chemical shifts are also used to describe signals in other forms of spectroscopy such as photoemission spectroscopy.

Nuclear magnetic resonance spectroscopy Laboratory technique

Nuclear magnetic resonance spectroscopy, most commonly known as NMR spectroscopy or magnetic resonance spectroscopy (MRS), is a spectroscopic technique to observe local magnetic fields around atomic nuclei. The sample is placed in a magnetic field and the NMR signal is produced by excitation of the nuclei sample with radio waves into nuclear magnetic resonance, which is detected with sensitive radio receivers. The intramolecular magnetic field around an atom in a molecule changes the resonance frequency, thus giving access to details of the electronic structure of a molecule and its individual functional groups. As the fields are unique or highly characteristic to individual compounds, in modern organic chemistry practice, NMR spectroscopy is the definitive method to identify monomolecular organic compounds.

Electron paramagnetic resonance

Electron paramagnetic resonance (EPR) or electron spin resonance (ESR) spectroscopy is a method for studying materials with unpaired electrons. The basic concepts of EPR are analogous to those of nuclear magnetic resonance (NMR), but the spins excited are those of the electrons instead of the atomic nuclei. EPR spectroscopy is particularly useful for studying metal complexes and organic radicals. EPR was first observed in Kazan State University by Soviet physicist Yevgeny Zavoisky in 1944, and was developed independently at the same time by Brebis Bleaney at the University of Oxford.

National High Magnetic Field Laboratory Magnetism research institute in the United States

The National High Magnetic Field Laboratory (MagLab) is a facility at Florida State University, the University of Florida, and Los Alamos National Laboratory in New Mexico, that performs magnetic field research in physics, biology, bioengineering, chemistry, geochemistry, biochemistry. It is the only such facility in the US, and is among twelve high magnetic facilities worldwide. The lab is supported by the National Science Foundation and the state of Florida, and works in collaboration with private industry.

Free induction decay

In Fourier transform nuclear magnetic resonance spectroscopy, free induction decay (FID) is the observable NMR signal generated by non-equilibrium nuclear spin magnetization precessing about the magnetic field. This non-equilibrium magnetization can be created generally by applying a pulse of radio-frequency close to the Larmor frequency of the nuclear spins.

Nuclear magnetic resonance spectroscopy of proteins is a field of structural biology in which NMR spectroscopy is used to obtain information about the structure and dynamics of proteins, and also nucleic acids, and their complexes. The field was pioneered by Richard R. Ernst and Kurt Wüthrich at the ETH, and by Ad Bax, Marius Clore, Angela Gronenborn at the NIH, and Gerhard Wagner at Harvard University, among others. Structure determination by NMR spectroscopy usually consists of several phases, each using a separate set of highly specialized techniques. The sample is prepared, measurements are made, interpretive approaches are applied, and a structure is calculated and validated.

Spin–spin relaxation

In physics, the spin–spin relaxation is the mechanism by which Mxy, the transverse component of the magnetization vector, exponentially decays towards its equilibrium value in nuclear magnetic resonance (NMR) and magnetic resonance imaging (MRI). It is characterized by the spin–spin relaxation time, known as T2, a time constant characterizing the signal decay. It is named in contrast to T1, the spin–lattice relaxation time. It is the time it takes for the magnetic resonance signal to irreversibly decay to 37% (1/e) of its initial value after its generation by tipping the longitudinal magnetization towards the magnetic transverse plane. Hence the relation

Nuclear magnetic resonance (NMR) in the geomagnetic field is conventionally referred to as Earth's field NMR (EFNMR). EFNMR is a special case of low field NMR.

Magnetization transfer (MT), in NMR and MRI, refers to the transfer of nuclear spin polarization and/or spin coherence from one population of nuclei to another population of nuclei, and to techniques that make use of these phenomena. There is some ambiguity regarding the precise definition of magnetization transfer, however the general definition given above encompasses all more specific notions. NMR active nuclei, those with non-zero spin, can be energetically coupled to one another under certain conditions. The mechanisms of nuclear-spin energy-coupling have been extensively characterized and are described in the following articles: Angular momentum coupling, Magnetic dipole–dipole interaction, J-coupling, Residual dipolar coupling, Nuclear Overhauser effect, Spin–spin relaxation, and Spin saturation transfer. Alternatively, some nuclei in a chemical system are labile and exchange between non-equivalent environments. A more specific example of this case is presented in the section Chemical Exchange Magnetization transfer.

Nuclear magnetic resonance Spectroscopic technique relying on the energy of electrons

Nuclear magnetic resonance (NMR) is a physical phenomenon in which nuclei in a strong constant magnetic field are perturbed by a weak oscillating magnetic field and respond by producing an electromagnetic signal with a frequency characteristic of the magnetic field at the nucleus. This process occurs near resonance, when the oscillation frequency matches the intrinsic frequency of the nuclei, which depends on the strength of the static magnetic field, the chemical environment, and the magnetic properties of the isotope involved; in practical applications with static magnetic fields up to ca. 20 tesla, the frequency is similar to VHF and UHF television broadcasts (60–1000 MHz). NMR results from specific magnetic properties of certain atomic nuclei. Nuclear magnetic resonance spectroscopy is widely used to determine the structure of organic molecules in solution and study molecular physics and crystals as well as non-crystalline materials. NMR is also routinely used in advanced medical imaging techniques, such as in magnetic resonance imaging (MRI).

Measuring instrument Device for measuring a physical quantity

A measuring instrument is a device to measure a physical quantity. In the physical sciences, quality assurance, and engineering, measurement is the activity of obtaining and comparing physical quantities of real-world objects and events. Established standard objects and events are used as units, and the process of measurement gives a number relating the item under study and the referenced unit of measurement. Measuring instruments, and formal test methods which define the instrument's use, are the means by which these relations of numbers are obtained. All measuring instruments are subject to varying degrees of instrument error and measurement uncertainty. These instruments may range from simple objects such as rulers and stopwatches to electron microscopes and particle accelerators. Virtual instrumentation is widely used in the development of modern measuring instruments.

Thermoporometry and cryoporometry are methods for measuring porosity and pore-size distributions. A small region of solid melts at a lower temperature than the bulk solid, as given by the Gibbs–Thomson equation. Thus, if a liquid is imbibed into a porous material, and then frozen, the melting temperature will provide information on the pore-size distribution. The detection of the melting can be done by sensing the transient heat flows during phase transitions using differential scanning calorimetry – DSC thermoporometry, measuring the quantity of mobile liquid using nuclear magnetic resonance – NMR cryoporometry (NMRC) or measuring the amplitude of neutron scattering from the imbibed crystalline or liquid phases – ND cryoporometry (NDC).

A Benchtop nuclear magnetic resonance spectrometer refers to a Fourier transform nuclear magnetic resonance (FT-NMR) spectrometer that is significantly more compact and portable than the conventional equivalents, such that it is portable and can reside on a laboratory benchtop. This convenience comes from using permanent magnets, which have a lower magnetic field and decreased sensitivity compared to the much larger and more expensive cryogen cooled superconducting NMR magnets. Instead of requiring dedicated infrastructure, rooms and extensive installations these benchtop instruments can be placed directly on the bench in a lab and moved as necessary. These spectrometers offer improved workflow, even for novice users, as they are simpler and easy to use. They differ from relaxometers in that they can be used to measure high resolution NMR spectra and are not limited to the determination of relaxation or diffusion parameters.

Magritek is a scientific instrument company based in Wellington, New Zealand, and Aachen, Germany, that was established in 2004 and specialises in compact, portable and benchtop nuclear magnetic resonance (NMR) and magnetic resonance imaging (MRI) products. The technology was originally developed to enable NMR measurements in Antarctica by scientists at Massey and Victoria Universities in New Zealand, including Dr Robin Dykstra. This was combined with compact, handheld NMR magnet technology developed by researchers at RWTH University in Aachen.

The history of magnetic resonance imaging (MRI) includes the work of many researchers who contributed to the discovery of nuclear magnetic resonance (NMR) and described the underlying physics of magnetic resonance imaging, starting early in the twentieth century. MR imaging was invented by Paul C. Lauterbur who developed a mechanism to encode spatial information into an NMR signal using magnetic field gradients in September 1971; he published the theory behind it in March 1973. The factors leading to image contrast had been described nearly 20 years earlier by physician and scientist Erik Odeblad and Gunnar Lindström. Among many other researchers in the late 1970s and 1980s, Peter Mansfield further refined the techniques used in MR image acquisition and processing, and in 2003 he and Lauterbur were awarded the Nobel Prize in Physiology or Medicine for their contributions to the development of MRI. The first clinical MRI scanners were installed in the early 1980s and significant development of the technology followed in the decades since, leading to its widespread use in medicine today.

Surface nuclear magnetic resonance (SNMR), also known as magnetic resonance Sounding (MRS), is a geophysical technique specially designed for hydrogeology. It is based on the principle of nuclear magnetic resonance (NMR) and measurements can be used to indirectly estimate the water content of saturated and unsaturated zones in the earth's subsurface. SNMR is used to estimate aquifer properties, including the quantity of water contained in the aquifer, porosity, and hydraulic conductivity.

References

  1. Debaten sobre innovación tecnológica y propiedad intelectual en las universidades — Universidad Nacional de Córdoba
  2. Oil, Protein and Moisture Determination in Seeds Using NMR | Seed Laboratory | Oregon State University
  3. T. F. Conway and F. R. Earle, "Nuclear magnetic resonance for determining oil content of seeds", Journal of the American Oil Chemists' Society, Springer Berlin / Heidelberg, Volume 40, Number 7, July, 1963