Autoclave moulding

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Autoclave moulding is an advanced composite manufacturing process.

Procedure

It is a process that uses a two-sided mould set that forms both surfaces of the panel. On the upper side is a flexible membrane made from silicone or an extruded polymer film such as nylon and on the lower side is a rigid mould. Reinforcement materials can be placed manually or robotically. They involve continuous fibre forms fashioned into textile constructions. Usually, they are pre-impregnated with the resin in the form of prepreg fabrics or unidirectional tapes. In some situations, a film of resin is placed upon the lower mould, and dry reinforcement is placed above. The upper mould is installed, and the vacuum is applied to the mould cavity. The assembly is placed into an autoclave. This process is generally performed at both elevated pressure and elevated temperature. The use of elevated pressure facilitates a high fibre volume fraction and low void content for maximum structural efficiency. [1] [2]

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Composite material

A composite material is a material produced from two or more constituent materials with notably dissimilar chemical or physical properties that, when merged, create a material with properties, unlike the individual elements. The individual components remain separate and distinct within the finished structure, distinguishing composites from mixtures and solid solutions.

Injection moulding

Injection moulding is a manufacturing process for producing parts by injecting molten material into a mould, or mold. Injection moulding can be performed with a host of materials mainly including metals, glasses, elastomers, confections, and most commonly thermoplastic and thermosetting polymers. Material for the part is fed into a heated barrel, mixed, and injected into a mould cavity, where it cools and hardens to the configuration of the cavity. After a product is designed, usually by an industrial designer or an engineer, moulds are made by a mould-maker from metal, usually either steel or aluminium, and precision-machined to form the features of the desired part. Injection moulding is widely used for manufacturing a variety of parts, from the smallest components to entire body panels of cars. Advances in 3D printing technology, using photopolymers that do not melt during the injection moulding of some lower temperature thermoplastics, can be used for some simple injection moulds.

Fibre-reinforced plastic (FRP) is a composite material made of a polymer matrix reinforced with fibres. The fibres are usually glass, carbon, aramid, or basalt. Rarely, other fibres such as paper, wood, or asbestos have been used. The polymer is usually an epoxy, vinyl ester, or polyester thermosetting plastic, though phenol formaldehyde resins are still in use.

Pre-preg is "pre-impregnated" composite fibers where a polymer matrix material, such as epoxy or phenolic resin, or even thermoplastic materials. The fibers often take the form of a weave and the matrix is used to bond them together and to other components during manufacture. The thermoset matrix is only partially cured to allow easy handling; this B-Stage material requires cold storage to prevent complete curing. B-Stage pre-preg is always stored in cooled areas since heat accelerates complete polymerization. Hence, composite structures built of pre-pregs will mostly require an oven or autoclave to cure. The main idea behind a pre-preg material is the use of anisotropic mechanical properties along the fibers, while the polymer matrix provides filling properties, keeping the fibers in a single system.

Compression molding

Compression Moulding is a method of moulding in which the moulding material, generally preheated, is first placed in an open, heated mould cavity. The mould is closed with a top force or plug member, pressure is applied to force the material into contact with all mould areas, while heat and pressure are maintained until the moulding material has cured. The process employs thermosetting resins in a partially cured stage, either in the form of granules, putty-like masses, or preforms.

Filament winding is a fabrication technique mainly used for manufacturing open (cylinders) or closed end structures. This process involves winding filaments under tension over a rotating mandrel. The mandrel rotates around the spindle while a delivery eye on a carriage traverses horizontally in line with the axis of the rotating mandrel, laying down fibers in the desired pattern or angle. The most common filaments are glass or carbon and are impregnated in a bath with resin as they are wound onto the mandrel. Once the mandrel is completely covered to the desired thickness, the resin is cured. Depending on the resin system and its cure characteristics, often the rotating mandrel is placed in an oven or placed under radiant heaters until the part is cured. Once the resin has cured, the mandrel is removed or extracted, leaving the hollow final product. For some products such as gas bottles, the 'mandrel' is a permanent part of the finished product forming a liner to prevent gas leakage or as a barrier to protect the composite from the fluid to be stored.

Sheet moulding compound (SMC) or sheet moulding composite is a ready to mould glass-fibre reinforced polyester material primarily used in compression moulding. The sheet is provided in rolls weighing up to 1000 kg. Alternatively the resin and related materials may be mixed on site when a producer wants greater control over the chemistry and filler.

Spray-Up also known as chop method of creating fiberglass objects by spraying short strands of glass out of a pneumatic gun. This method is used often when one side of the finished product is not seen, or when large quantities of a product must be made cheaply and quickly without regards to strength. Corvette fenders and boat dinghies are commonly manufactured this way.

Precision glass moulding

Precision glass moulding is a replicative process that allows the production of high precision optical components from glass without grinding and polishing. The process is also known as ultra-precision glass pressing. It is used to manufacture precision glass lenses for consumer products such as digital cameras, and high-end products like medical systems. The main advantage over mechanical lens production is that complex lens geometries such as aspheres can be produced cost-efficiently.

A thermoset polymer matrix is a synthetic polymer reinforcement where polymers act as binder or matrix to secure in place incorporated particulates, fibres or other reinforcements. They were first developed for structural applications, such as glass-reinforced plastic radar domes on aircraft and graphite-epoxy payload bay doors on the space shuttle.

Carbon fiber reinforced polymer, Carbon fibre reinforced polymer, or carbon fiber reinforced plastic, or carbon fiber reinforced thermoplastic, is an extremely strong and light fiber-reinforced plastic which contains carbon fibers. The spelling 'fibre' is typically used outside the US. CFRPs can be expensive to produce, but are commonly used wherever high strength-to-weight ratio and stiffness (rigidity) are required, such as aerospace, superstructures of ships, automotive, civil engineering, sports equipment, and an increasing number of consumer and technical applications.

Vacuum bag moulding utilizes a flexible film to enclose the part and seal it from the outside air. The vacuum bag material is accessible in a tube shape or a sheet of material. Then, a vacuum is drawn on the vacuum bag, and atmospheric pressure compresses the part during the cure. When a tube-shaped bag is used, the entire part can be enclosed within the bag. When utilizing sheet bagging materials, the edges of the vacuum bag are sealed against the edges of the mould surface to enclose the part against an air-tight mould. When bagged in this way, the lower mould is a rigid structure and the upper surface of the part is formed by the flexible membrane vacuum bag. The flexible membrane can be a reusable silicone material or an extruded polymer film. A vacuum is drawn on the part during cure after sealing the part inside the vacuum bag. This process can be fulfiled at either ambient or elevated temperature with ambient atmospheric pressure acting upon the vacuum bag. A vacuum pump is used usually to draw a vacuum. A cost-effective method of drawing a vacuum is with a venturi vacuum and air compressor.


Out of autoclave composite manufacturing is an alternative to the traditional high pressure autoclave (industrial) curing process commonly used by the aerospace manufacturers for manufacturing composite material. Out of autoclave (OOA) is a process that achieves the same quality as an autoclave but through a different process. OOA curing achieves the desired fiber content and elimination of voids by placing the layup within a closed mold and applying vacuum, pressure, and heat by means other than an autoclave. An RTM press is the typical method of applying heat and pressure to the closed mold. There are several out of autoclave technologies in current use including resin transfer molding (RTM), Same Qualified Resin Transfer Molding (SQRTM), vacuum-assisted resin transfer molding (VARTM), and balanced pressure fluid molding. The most advanced of these processes can produce high-tech net shape aircraft components.

Tailored fiber placement

Tailored fiber placement (TFP) is a textile manufacturing technique based on the principle of sewing for a continuous placement of fibrous material for composite components. The fibrous material is fixed with an upper and lower stitching thread on a base material. Compared to other textile manufacturing processes fiber material can be placed near net-shape in curvilinear patterns upon a base material in order to create stress adapted composite parts.

Vacuum Assisted Resin Transfer Molding (VARTM) or Vacuum Injected Molding (VIM) is a closed mold, out of autoclave (OOA) composite manufacturing process. VARTM is a variation of Resin Transfer Molding (RTM) with its distinguishing characteristic being the replacement of the top portion of a mold tool with a vacuum bag and the use of a vacuum to assist in resin flow. The process involves the use of a vacuum to facilitate resin flow into a fiber layup contained within a mold tool covered by a vacuum bag. After the impregnation occurs the composite part is allowed to cure at room temperature with an optional post cure sometimes carried out.

CFSMC, or Carbon Fiber Sheet Molding Compound, is a ready to mold carbon fiber reinforced polymer composite material used in compression molding. While traditional SMC utilizes chopped glass fibers in a polymer resin, CFSMC utilizes chopped carbon fibers. The length and distribution of the carbon fibers is more regular, homogeneous, and constant than the standard glass SMC. CFSMC offers much higher stiffness and usually higher strength than standard SMC, but at a higher cost.

A Lay-Up process is a moulding process for composite materials, in which the final product is obtained by overlapping a specific number of different layers, usually made of continuous polymeric or ceramic fibres and a thermoset polymeric liquid matrix. It can be divided into Dry Lay-up and Wet Lay-Up, depending on whether the layers are pre-impregnated or not. Dry Lay-up is a common process in the aerospace industry, due to the possibility of obtaining complex shapes with good mechanical properties, characteristics required in this field. On the contrary, as Wet Lay-Up does not allow uni-directional fabrics, which have better mechanical properties, it is mainly adopted for all the other areas, which in general have lower requirements in terms of performances.

The main stages of the Lay-Up process are the cutting, the lamination and the polymerization. Even if some of the production steps can be automatised, this process is mainly manual, leading to laminates with high production costs and low production rates with respect to the other techniques. Hence, nowadays, it is mainly suitable for small series productions of 10 to 1000 parts.

Pressure bag moulding is a process for moulding reinforced plastics. This process is related to vacuum bag molding.

Resin transfer moulding is a process for producing high performance composite components.

Light resin transfer moulding is a process by which products of composite are manufactured using a closed mould system.

References

  1. "Autoclave Moulding (Pressure Vessel Moulding) – CSIR – NAL". www.nal.res.in. Retrieved 2020-11-10.
  2. "Autoclave molding – CSIR – NAL". www.nal.res.in. Retrieved 2020-11-10.