Complementary experiments

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In physics, two experimental techniques are often called complementary if they investigate the same subject in two different ways such that two different (ideally non-overlapping) properties or aspects can be investigated. [1] [2] For example, X-ray scattering and neutron scattering experiments are often said to be complementary because the former reveals information about the electron density of the atoms in the target but gives no information about the nuclei (because they are too small to affect the X-rays significantly), while the latter allows one to investigate the nuclei of the atoms but cannot tell one anything about their electron hulls (because the neutrons, being neutral, do not interact with the charged electrons).

Scattering experiments are sometimes also called complementary when they investigate the same physical property of a system from two complementary view points in the sense of Bohr. For example, time-resolved and energy-resolved experiments are said to be complementary. [3] The former uses a pulse which is well-defined in time. The latter uses a monochromatic pulse well defined in energy (its frequency is well known).

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<span class="mw-page-title-main">Muon</span> Subatomic particle

A muon is an elementary particle similar to the electron, with an electric charge of −1 e and a spin of 1/2, but with a much greater mass. It is classified as a lepton. As with other leptons, the muon is not thought to be composed of any simpler particles; that is, it is a fundamental particle.

<span class="mw-page-title-main">Neutron</span> Subatomic particle with no charge

The neutron is a subatomic particle, symbol
n
or
n0
, which has a neutral charge, and a mass slightly greater than that of a proton. Protons and neutrons constitute the nuclei of atoms. Since protons and neutrons behave similarly within the nucleus, and each has a mass of approximately one dalton, they are both referred to as nucleons. Their properties and interactions are described by nuclear physics. Protons and neutrons are not elementary particles; each is composed of three quarks.

<span class="mw-page-title-main">Nuclear physics</span> Field of physics that studies atomic nuclei

Nuclear physics is the field of physics that studies atomic nuclei and their constituents and interactions, in addition to the study of other forms of nuclear matter.

<span class="mw-page-title-main">Proton</span> Subatomic particle with positive charge

A proton is a stable subatomic particle, symbol
p
, H+, or 1H+ with a positive electric charge of +1 e (elementary charge). Its mass is slightly less than that of a neutron and 1,836 times the mass of an electron (the proton-to-electron mass ratio). Protons and neutrons, each with masses of approximately one atomic mass unit, are jointly referred to as "nucleons" (particles present in atomic nuclei).

<span class="mw-page-title-main">Spectroscopy</span> Study involving matter and electromagnetic radiation

Spectroscopy is the field of study that measures and interprets the electromagnetic spectra that result from the interaction between electromagnetic radiation and matter as a function of the wavelength or frequency of the radiation. In simpler terms, spectroscopy is the precise study of color as generalized from visible light to all bands of the electromagnetic spectrum.

<span class="mw-page-title-main">X-ray crystallography</span> Technique used for determining crystal structures and identifying mineral compounds

X-ray crystallography is the experimental science determining the atomic and molecular structure of a crystal, in which the crystalline structure causes a beam of incident X-rays to diffract into many specific directions. By measuring the angles and intensities of these diffracted beams, a crystallographer can produce a three-dimensional picture of the density of electrons within the crystal. From this electron density, the mean positions of the atoms in the crystal can be determined, as well as their chemical bonds, their crystallographic disorder, and various other information.

<span class="mw-page-title-main">Electron diffraction</span> Bending of electron beams due to electrostatic interactions with matter

Electron diffraction is a general term for phenomena associated with changes in the direction of electron beams due to elastic interactions with atoms. Close to the atoms the changes are described as Fresnel diffraction; far away they are called Fraunhofer diffraction. The resulting map of the directions of the electrons far from the sample is called a diffraction pattern, see for instance Figure 1. These patterns are similar to x-ray and neutron diffraction patterns, and are used to study the atomic structure of gases, liquids, surfaces and bulk solids. Electron diffraction also plays a major role in the contrast of images in electron microscopes.

<span class="mw-page-title-main">Neutron diffraction</span> Technique to investigate atomic structures using neutron scattering

Neutron diffraction or elastic neutron scattering is the application of neutron scattering to the determination of the atomic and/or magnetic structure of a material. A sample to be examined is placed in a beam of thermal or cold neutrons to obtain a diffraction pattern that provides information of the structure of the material. The technique is similar to X-ray diffraction but due to their different scattering properties, neutrons and X-rays provide complementary information: X-Rays are suited for superficial analysis, strong x-rays from synchrotron radiation are suited for shallow depths or thin specimens, while neutrons having high penetration depth are suited for bulk samples.

<span class="mw-page-title-main">Synchrotron light source</span> Particle accelerator designed to produce intense x-ray beams

A synchrotron light source is a source of electromagnetic radiation (EM) usually produced by a storage ring, for scientific and technical purposes. First observed in synchrotrons, synchrotron light is now produced by storage rings and other specialized particle accelerators, typically accelerating electrons. Once the high-energy electron beam has been generated, it is directed into auxiliary components such as bending magnets and insertion devices in storage rings and free electron lasers. These supply the strong magnetic fields perpendicular to the beam that are needed to stimulate the high energy electrons to emit photons.

<span class="mw-page-title-main">Nuclear reaction</span> Process in which two nuclei collide to produce one or more nuclides

In nuclear physics and nuclear chemistry, a nuclear reaction is a process in which two nuclei, or a nucleus and an external subatomic particle, collide to produce one or more new nuclides. Thus, a nuclear reaction must cause a transformation of at least one nuclide to another. If a nucleus interacts with another nucleus or particle and they then separate without changing the nature of any nuclide, the process is simply referred to as a type of nuclear scattering, rather than a nuclear reaction.

<span class="mw-page-title-main">Neutron scattering</span> Physical phenomenon

Neutron scattering, the irregular dispersal of free neutrons by matter, can refer to either the naturally occurring physical process itself or to the man-made experimental techniques that use the natural process for investigating materials. The natural/physical phenomenon is of elemental importance in nuclear engineering and the nuclear sciences. Regarding the experimental technique, understanding and manipulating neutron scattering is fundamental to the applications used in crystallography, physics, physical chemistry, biophysics, and materials research.

<span class="mw-page-title-main">Powder diffraction</span>

Powder diffraction is a scientific technique using X-ray, neutron, or electron diffraction on powder or microcrystalline samples for structural characterization of materials. An instrument dedicated to performing such powder measurements is called a powder diffractometer.

<span class="mw-page-title-main">Neutron detection</span>

Neutron detection is the effective detection of neutrons entering a well-positioned detector. There are two key aspects to effective neutron detection: hardware and software. Detection hardware refers to the kind of neutron detector used and to the electronics used in the detection setup. Further, the hardware setup also defines key experimental parameters, such as source-detector distance, solid angle and detector shielding. Detection software consists of analysis tools that perform tasks such as graphical analysis to measure the number and energies of neutrons striking the detector.

<span class="mw-page-title-main">Neutron reflectometry</span>

Neutron reflectometry is a neutron diffraction technique for measuring the structure of thin films, similar to the often complementary techniques of X-ray reflectivity and ellipsometry. The technique provides valuable information over a wide variety of scientific and technological applications including chemical aggregation, polymer and surfactant adsorption, structure of thin film magnetic systems, biological membranes, etc.

<span class="mw-page-title-main">Spin echo</span> Response of spin to electromagnetic radiation

In magnetic resonance, a spin echo or Hahn echo is the refocusing of spin magnetisation by a pulse of resonant electromagnetic radiation. Modern nuclear magnetic resonance (NMR) and magnetic resonance imaging (MRI) make use of this effect.

Delbrück scattering, the deflection of high-energy photons in the Coulomb field of nuclei as a consequence of vacuum polarization, was observed in 1975. The related process of the scattering of light by light, also a consequence of vacuum polarization, was not observed until 1998. In both cases, it is a process described by quantum electrodynamics.

<span class="mw-page-title-main">Atomic nucleus</span> Core of an atom; composed of nucleons (protons and neutrons)

The atomic nucleus is the small, dense region consisting of protons and neutrons at the center of an atom, discovered in 1911 by Ernest Rutherford based on the 1909 Geiger–Marsden gold foil experiment. After the discovery of the neutron in 1932, models for a nucleus composed of protons and neutrons were quickly developed by Dmitri Ivanenko and Werner Heisenberg. An atom is composed of a positively charged nucleus, with a cloud of negatively charged electrons surrounding it, bound together by electrostatic force. Almost all of the mass of an atom is located in the nucleus, with a very small contribution from the electron cloud. Protons and neutrons are bound together to form a nucleus by the nuclear force.

The EMC effect is the surprising observation that the cross section for deep inelastic scattering from an atomic nucleus is different from that of the same number of free protons and neutrons. From this observation, it can be inferred that the quark momentum distributions in nucleons bound inside nuclei are different from those of free nucleons. This effect was first observed in 1983 at CERN by the European Muon Collaboration, hence the name "EMC effect". It was unexpected, since the average binding energy of protons and neutrons inside nuclei is insignificant when compared to the energy transferred in deep inelastic scattering reactions that probe quark distributions. While over 1000 scientific papers have been written on the topic and numerous hypotheses have been proposed, no definitive explanation for the cause of the effect has been confirmed. Determining the origin of the EMC effect is one of the major unsolved problems in the field of nuclear physics.

The rms charge radius is a measure of the size of an atomic nucleus, particularly the proton distribution. The proton radius is approximately one femtometre = 10−15 metres. It can be measured by the scattering of electrons by the nucleus. Relative changes in the mean squared nuclear charge distribution can be precisely measured with atomic spectroscopy.

<span class="mw-page-title-main">Discovery of the neutron</span> Scientific background leading to the discovery of subatomic particles

The discovery of the neutron and its properties was central to the extraordinary developments in atomic physics in the first half of the 20th century. Early in the century, Ernest Rutherford developed a crude model of the atom, based on the gold foil experiment of Hans Geiger and Ernest Marsden. In this model, atoms had their mass and positive electric charge concentrated in a very small nucleus. By 1920, isotopes of chemical elements had been discovered, the atomic masses had been determined to be (approximately) integer multiples of the mass of the hydrogen atom, and the atomic number had been identified as the charge on the nucleus. Throughout the 1920s, the nucleus was viewed as composed of combinations of protons and electrons, the two elementary particles known at the time, but that model presented several experimental and theoretical contradictions.

References

  1. Led, Jens J; Gesmar, Henrik (1982-10-01). "The applicability of the magnetization-transfer NMR technique to determine chemical exchange rates in extreme cases. The importance of complementary experiments". Journal of Magnetic Resonance. 49 (3): 444–463. Bibcode:1982JMagR..49..444L. doi:10.1016/0022-2364(82)90257-8. ISSN   0022-2364.
  2. Fischer, R.; Dinklage, A.; Knuth, Kevin H.; Caticha, Ariel; Center, Julian L.; Giffin, Adom; Rodríguez, Carlos C. (2007). "The concept of Integrated Data Analysis of complementary experiments". AIP Conference Proceedings. AIP. 954: 195–202. Bibcode:2007AIPC..954..195F. doi:10.1063/1.2821262. hdl: 11858/00-001M-0000-0027-09CA-5 .
  3. Mehta, Halak N.; Benyathiar, Patnarin; Mishra, Dharmendra K.; Varney, Michael (2021-07-01). "Complementary experiments for parameter estimation in heat transfer model". Food and Bioproducts Processing. 128: 240–246. doi: 10.1016/j.fbp.2021.06.004 . ISSN   0960-3085. S2CID   237761703.