Cryogenic seal

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Cryogenic seals provide a mechanical containment mechanism for materials held at cryogenic temperatures, such as cryogenic fluids. Various techniques, including soldering and welding are available for creating seals; however, specialized materials and processes are necessary to hermetically entrap cryogenic constituents under vacuum-tight conditions. Most commonly used are liquid helium and liquid nitrogen, which boil at very low temperatures, below −153 °C (120 K), as well as hydrocarbons with low freezing points and refrigerating mixtures. [1] Pure indium wire or solder preform washers are accepted as the most reliable low temperature sealing materials. When correctly formed, indium will afford leak rates of less than 4.0x10 -9 mbar- liter/sec. [2] Alternative cryogenic seal materials include silicone grease conical seals, and Pb/Sn (lead-tin) wire seals. [3]

Contents

History

Fundamental cryogenic processing began in the 1940s, albeit primitive. Steel cutting tools were immersed in liquid nitrogen to enhance their service life.

Mechanical processes utilizing cryogenics were documented well in the 1950s and by the 1980s cryogenic fluids began to be considered for storage and use in modern devices.

Today, cryogenic seals are a necessity in high-tech commercial, medical, and military applications to encapsulate the cryogenic fluids critical for device resolution and function. [4]

Applications

Applications which utilize cryogenic seals include: [5]

Indium seals

Advantages

Advantages of indium cryogenic seals:

Disadvantages

Process information for indium seals

Reliability testing

Types

Manufacturers

Related Research Articles

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<span class="mw-page-title-main">Gasket</span> Type of mechanical seal

A gasket is a mechanical seal which fills the space between two or more mating surfaces, generally to prevent leakage from or into the joined objects while under compression. It is a deformable material that is used to create a static seal and maintain that seal under various operating conditions in a mechanical assembly.

<span class="mw-page-title-main">Flux (metallurgy)</span> Chemical used in metallurgy for cleaning or purifying molten metal

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<span class="mw-page-title-main">Ultrasonic welding</span> Welding process

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<span class="mw-page-title-main">O-ring</span> Mechanical, toroid gasket that seals an interface

An O-ring, also known as a packing or a toric joint, is a mechanical gasket in the shape of a torus; it is a loop of elastomer with a round cross-section, designed to be seated in a groove and compressed during assembly between two or more parts, forming a seal at the interface.

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<span class="mw-page-title-main">Heat sealer</span> Machine for joining thermoplastic materials using heat

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<span class="mw-page-title-main">Pipe (fluid conveyance)</span> Tubular section or hollow cylinder

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<span class="mw-page-title-main">Glass-to-metal seal</span> Airtight seal which joins glass and metal surfaces

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<span class="mw-page-title-main">Soldering</span> Process of joining metal pieces with heated filler metal

Soldering is a process of joining two metal surfaces together using a filler metal called solder. The soldering process involves heating the surfaces to be joined and melting the solder, which is then allowed to cool and solidify, creating a strong and durable joint.

Glass frit bonding, also referred to as glass soldering or seal glass bonding, describes a wafer bonding technique with an intermediate glass layer. It is a widely used encapsulation technology for surface micro-machined structures, e.g., accelerometers or gyroscopes. This technique utilizes low melting-point glass and therefore provides various advantages including that viscosity of glass decreases with an increase of temperature. The viscous flow of glass has effects to compensate and planarize surface irregularities, convenient for bonding wafers with a high roughness due to plasma etching or deposition. A low viscosity promotes hermetically sealed encapsulation of structures based on a better adaption of the structured shapes. Further, the coefficient of thermal expansion (CTE) of the glass material is adapted to silicon. This results in low stress in the bonded wafer pair. The glass has to flow and wet the soldered surfaces well below the temperature where deformation or degradation of either of the joined materials or nearby structures occurs. The usual temperature of achieving flowing and wetting is between 450 and 550 °C.

<span class="mw-page-title-main">Materials for use in vacuum</span>

Materials for use in vacuum are materials that show very low rates of outgassing in vacuum and, where applicable, are tolerant to bake-out temperatures. The requirements grow increasingly stringent with the desired degree of vacuum to be achieved in the vacuum chamber. The materials can produce gas by several mechanisms. Molecules of gases and water can be adsorbed on the material surface. Materials may sublimate in vacuum. Or the gases can be released from porous materials or from cracks and crevices. Traces of lubricants, residues from machining, can be present on the surfaces. A specific risk is outgassing of solvents absorbed in plastics after cleaning.

<span class="mw-page-title-main">Bismuth–indium</span>

The elements bismuth and indium have relatively low melting points when compared to other metals, and their alloy bismuth–indium (Bi–In) is classified as a fusible alloy. It has a melting point lower than the eutectic point of the tin–lead alloy. The most common application of the Bi-In alloy is as a low temperature solder, which can also contain, besides bismuth and indium, lead, cadmium, and tin.

References

  1. European Organization for Nuclear Research - An Introduction to Cryogenics
  2. 1 2 3 4 Design, Development and Testing of Vacuum Compatible Seals at Cryogenic Temperatures Archived 2011-09-27 at the Wayback Machine
  3. Stewart, MD; Koutroulakis, G; Kalechofsky, N; Mitrović, VF (2010). "A Reusable, Low-profile, Cryogenic Wire Seal". Cryogenics (Guildf). 50 (1): 50–51. doi:10.1016/j.cryogenics.2009.09.009. PMC   2805154 . PMID   20161550.
  4. Some Cryogenic History Archived 2011-11-25 at the Wayback Machine
  5. Applications for Stored Liquefied Cryogenic Gases Archived 2011-11-02 at the Wayback Machine
  6. Vacuum Service for a Gemini 200 NMR Archived 2011-09-28 at the Wayback Machine
  7. 1 2 Indium and Vacuum Seals
  8. Indium Wire and Cryogenic Sealing
  9. 1 2 3 4 5 6 Compact indium seal for cryogenic optical windows
  10. Demountable Cryogenic Seal Options
  11. "Indium for Sealing". Archived from the original on 2011-09-25. Retrieved 2011-08-29.
  12. "Indium Cold Welding". Archived from the original on 2011-09-29. Retrieved 2011-08-29.
  13. Neuhauser, Robert G (1979). "Pressure-made soft-metal vacuum seals for glass and ceramics". Vacuum. 29 (6–7): 231–235. Bibcode:1979Vacuu..29..231N. doi:10.1016/S0042-207X(79)80644-2.