A pole figure is a graphical representation of the orientation of objects in space. For example, pole figures in the form of stereographic projections are used to represent the orientation distribution of crystallographic lattice planes in crystallography and texture analysis in materials science.
Consider an object with a basis attached to it. The orientation of the object in space can be determined by three rotations to transform the reference basis of space to the basis attached to the object; these are the Euler angles.
If we consider a plane of the object, the orientation of the plane can be given by its normal line. If we draw a sphere with the center on the plane, then
A single pole is not enough to fully determine the orientation of an object: the pole stays the same if we apply a rotation around the normal line. The orientation of the object is fully determined by the use of poles of two planes that are not parallel.
The upper sphere is projected on a plane using the stereographic projection.
Consider the (x,y) plane of the reference basis; its trace on the sphere is the equator of the sphere. We draw a line joining the South pole with the pole of interest P.
It is possible to choose any projection plane parallel to the equator (except the South pole): the figures will be proportional (property of similar triangles). It is usual to place the projection plane at the North pole.
A Wulff net is used to read a pole figure.
The stereographic projection of a trace is an arc. The Wulff net is arcs corresponding to planes that share a common axis in the (x,y) plane.
If the pole and the trace of a plane are represented on the same diagram, then
Consider an axis Δ, and planes belonging to the zone of this axis, i.e. Δ is in all these planes, the intersection of all the planes is Δ. If we call P the plane that is perpendicular to Δ, then the normals to the planes all belong to P. Thus, the poles of the planes belonging to the same zone are on the trace of the plane P perpendicular to the axis.
The structure of a crystal is often represented by the pole figure of its crystallographic planes.
A plane is chosen as the equator, usually the (001) or (011) plane; its pole is the center of the figure. Then, the poles of the other planes are placed on the figure, with the Miller indices for each pole. The poles that belong to a zone are sometimes linked with the related trace.
"Texture" in the context of Materials Science means "crystallographic preferred orientation". If a polycrystalline material (i.e. a material composed of many different crystals or grains, like most metals, ceramics or minerals) has "texture" then that means that the crystal axes are not randomly (or, more correctly, uniformly) distributed.
To draw a pole figure, one chooses a particular crystal direction (e.g. the normal to the (100) plane) and then plots that direction, called a pole, for every crystal relative to a set of directions in the material. In a rolled metal, for example, the directions in the material are the rolling direction, transverse direction and rolling plane normal.
If a large number of crystals are involved, then it is typical to make a contour plot, rather than plotting individual poles.
The full determination of the texture requires the plot of two pole figures corresponding to planes that are not parallel and that do not have the same diffraction angle (thus different interplanar distances).
Consider the diffraction pattern obtained with a single crystal, on a plane that is perpendicular to the beam, e.g. X-ray diffraction with the Laue method, or electron diffraction in a transmission electron microscope. The diffraction figure shows spots.
The position of the spots is determined by the Bragg's law. It gives the orientation of the plane.
If the parameters of the optics are known (especially the distance between the crystal and the photographic film), it is possible to build the stereographic diagram from the diffraction diagram, i.e. to transform the diffraction pattern into a pole figure.[ citation needed ]
Crystallography is the experimental science of determining the arrangement of atoms in crystalline solids. Crystallography is a fundamental subject in the fields of materials science and solid-state physics. The word "crystallography" is derived from the Greek word κρύσταλλος (krystallos) "clear ice, rock-crystal", with its meaning extending to all solids with some degree of transparency, and γράφειν (graphein) "to write". In July 2012, the United Nations recognised the importance of the science of crystallography by proclaiming that 2014 would be the International Year of Crystallography.
In geography, latitude is a coordinate that specifies the north–south position of a point on the surface of the Earth or another celestial body. Latitude is given as an angle that ranges from –90° at the south pole to 90° at the north pole, with 0° at the Equator. Lines of constant latitude, or parallels, run east–west as circles parallel to the equator. Latitude and longitude are used together as a coordinate pair to specify a location on the surface of the Earth.
In group theory, the symmetry group of a geometric object is the group of all transformations under which the object is invariant, endowed with the group operation of composition. Such a transformation is an invertible mapping of the ambient space which takes the object to itself, and which preserves all the relevant structure of the object. A frequent notation for the symmetry group of an object X is G = Sym(X).
The equatorial coordinate system is a celestial coordinate system widely used to specify the positions of celestial objects. It may be implemented in spherical or rectangular coordinates, both defined by an origin at the centre of Earth, a fundamental plane consisting of the projection of Earth's equator onto the celestial sphere, a primary direction towards the vernal equinox, and a right-handed convention.
A circle of latitude or line of latitude on Earth is an abstract east–west small circle connecting all locations around Earth at a given latitude coordinate line.
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In mathematics, the complex plane is the plane formed by the complex numbers, with a Cartesian coordinate system such that the x-axis, called the real axis, is formed by the real numbers, and the y-axis, called the imaginary axis, is formed by the imaginary numbers.
Reflection high-energy electron diffraction (RHEED) is a technique used to characterize the surface of crystalline materials. RHEED systems gather information only from the surface layer of the sample, which distinguishes RHEED from other materials characterization methods that also rely on diffraction of high-energy electrons. Transmission electron microscopy, another common electron diffraction method samples mainly the bulk of the sample due to the geometry of the system, although in special cases it can provide surface information. Low-energy electron diffraction (LEED) is also surface sensitive, but LEED achieves surface sensitivity through the use of low energy electrons.
A gnomonic map projection is a map projection which displays all great circles as straight lines, resulting in any straight line segment on a gnomonic map showing a geodesic, the shortest route between the segment's two endpoints. This is achieved by casting surface points of the sphere onto a tangent plane, each landing where a ray from the center of the sphere passes through the point on the surface and then on to the plane. No distortion occurs at the tangent point, but distortion increases rapidly away from it. Less than half of the sphere can be projected onto a finite map. Consequently, a rectilinear photographic lens, which is based on the gnomonic principle, cannot image more than 180 degrees.
In geometry and science, a cross section is the non-empty intersection of a solid body in three-dimensional space with a plane, or the analog in higher-dimensional spaces. Cutting an object into slices creates many parallel cross-sections. The boundary of a cross-section in three-dimensional space that is parallel to two of the axes, that is, parallel to the plane determined by these axes, is sometimes referred to as a contour line; for example, if a plane cuts through mountains of a raised-relief map parallel to the ground, the result is a contour line in two-dimensional space showing points on the surface of the mountains of equal elevation.
In physical chemistry and materials science, texture is the distribution of crystallographic orientations of a polycrystalline sample. A sample in which these orientations are fully random is said to have no distinct texture. If the crystallographic orientations are not random, but have some preferred orientation, then the sample has a weak, moderate or strong texture. The degree is dependent on the percentage of crystals having the preferred orientation.
The scale of a map is the ratio of a distance on the map to the corresponding distance on the ground. This simple concept is complicated by the curvature of the Earth's surface, which forces scale to vary across a map. Because of this variation, the concept of scale becomes meaningful in two distinct ways.
In geometry, a point group in three dimensions is an isometry group in three dimensions that leaves the origin fixed, or correspondingly, an isometry group of a sphere. It is a subgroup of the orthogonal group O(3), the group of all isometries that leave the origin fixed, or correspondingly, the group of orthogonal matrices. O(3) itself is a subgroup of the Euclidean group E(3) of all isometries.
The Lambert azimuthal equal-area projection is a particular mapping from a sphere to a disk. It accurately represents area in all regions of the sphere, but it does not accurately represent angles. It is named for the Swiss mathematician Johann Heinrich Lambert, who announced it in 1772. "Zenithal" being synonymous with "azimuthal", the projection is also known as the Lambert zenithal equal-area projection.
Selected area (electron) diffraction, is a crystallographic experimental technique typically performed using a transmission electron microscope (TEM). It is a specific case of electron diffraction used primarily in material science and solid state physics as one of the most common experimental techniques. Especially with appropriate analytical software, SAD patterns (SADP) can be used to determine crystal orientation, measure lattice constants or examine its defects.
Fiber diffraction is a subarea of scattering, an area in which molecular structure is determined from scattering data. In fiber diffraction the scattering pattern does not change, as the sample is rotated about a unique axis. Such uniaxial symmetry is frequent with filaments or fibers consisting of biological or man-made macromolecules. In crystallography fiber symmetry is an aggravation regarding the determination of crystal structure, because reflexions are smeared and may overlap in the fiber diffraction pattern. Materials science considers fiber symmetry a simplification, because almost the complete obtainable structure information is in a single two-dimensional (2D) diffraction pattern exposed on photographic film or on a 2D detector. 2 instead of 3 co-ordinate directions suffice to describe fiber diffraction.
Kikuchi lines are patterns of electrons formed by scattering. They pair up to form bands in electron diffraction from single crystal specimens, there to serve as "roads in orientation-space" for microscopists uncertain of what they are looking at. In transmission electron microscopes, they are easily seen in diffraction from regions of the specimen thick enough for multiple scattering. Unlike diffraction spots, which blink on and off as one tilts the crystal, Kikuchi bands mark orientation space with well-defined intersections as well as paths connecting one intersection to the next.
In materials science, misorientation is the difference in crystallographic orientation between two crystallites in a polycrystalline material.
Zone axis, a term sometimes used to refer to "high-symmetry" orientations in a crystal, most generally refers to any direction referenced to the direct lattice of a crystal in three dimensions. It is therefore indexed with direct lattice indices, instead of with Miller indices.
CrysTBox is a suite of computer tools designed to accelerate material research based on transmission electron microscope images via highly accurate automated analysis and interactive visualization. Relying on artificial intelligence and computer vision, CrysTBox makes routine crystallographic analyses simpler, faster and more accurate compared to human evaluators. The high level of automation together with sub-pixel precision and interactive visualization makes the quantitative crystallographic analysis accessible even for non-crystallographers allowing for an interdisciplinary research. Simultaneously, experienced material scientists can take advantage of advanced functionalities for comprehensive analyses.