Petrographic microscope

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Plain light with the first filter (above), crossed-polarized light with both filters (below) in a volcanic lithic fragment (sand grain). Scale box in millimeters. LvMS-Lvm.jpg
Plain light with the first filter (above), crossed-polarized light with both filters (below) in a volcanic lithic fragment (sand grain). Scale box in millimeters.
Leica DMRX incident light microscope with mechanical stage and Swift F automated point counter for analysis of organic composition of coal and rock samples Leica DMRX.jpg
Leica DMRX incident light microscope with mechanical stage and Swift F automated point counter for analysis of organic composition of coal and rock samples
Thin sections under a microscope. Thin sections.JPG
Thin sections under a microscope.
Photomicrograph of a thin section of gabbro in cross-polarized light Gabbro pmg ss 2006.jpg
Photomicrograph of a thin section of gabbro in cross-polarized light

A petrographic microscope is a type of optical microscope used to identify rocks and minerals in thin sections. The microscope is used in optical mineralogy and petrography, a branch of petrology which focuses on detailed descriptions of rocks. The method includes aspects of polarized light microscopy (PLM).

Contents

Description

Depending on the grade of observation required, petrographic microscopes are derived from conventional brightfield microscopes of similar basic capabilities by:

Petrographic microscopes are constructed with optical parts that do not add unwanted polarizing effects due to strained glass, or polarization by reflection in prisms and mirrors. These special parts add to the cost and complexity of the microscope. However, a "simple polarizing" microscope is easily made by adding inexpensive polarizing filters to a standard biological microscope, often with one in a filter holder beneath the condenser, and a second inserted beneath the head or eyepiece. These can be sufficient for many non-quantitative purposes.

The two Nicol prisms (occasionally referred to as nicols) of the petrographic microscope have their polarizing planes oriented perpendicular to one another. When only an isotropic material such as air, water, or glass exists between the filters, all light is blocked, but most crystalline materials and minerals change the polarizing light directions, allowing some of the altered light to pass through the analyzer to the viewer. Using one polarizer makes it possible to view the slide in plane polarized light; using two allows for analysis under cross polarized light. A particular light pattern on the upper lens surface of the objectives is created as a conoscopic interference pattern (or interference figure) characteristic of uniaxial and biaxial minerals, and produced with convergent polarized light. To observe the interference figure, true petrographic microscopes usually include an accessory called a Bertrand lens, which focuses and enlarges the figure. It is also possible to remove an eyepiece lens to make a direct observation of the objective lens surface.

In addition to modifications of the microscope's optical system, petrographic microscopes allow for the insertion of specially-cut oriented filters of biaxial minerals (the quartz wedge, quarter-wave mica plate and half-wave mica plate), into the optical train between the polarizers to identify positive and negative birefringence, and in extreme cases, the mineral order when needed.

History

As early as 1808, the French physicist Étienne Louis Malus discovered the refraction and polarization of light.   William Nicol invented a prism for polarization in 1829, which was an indispensable part of the polarizing microscope for over 100 years. Later the Nicol prisms were replaced by cheaper polarizing filters.

The first complete polarizing microscope was built by Giovanni Battista Amici in 1830.

Rudolf Fuess built the first polarization microscope specifically for petrographic purposes in 1875. This was described by Harry Rosenbusch in the yearbook for mineralogy. [1]

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<span class="mw-page-title-main">Optics</span> Branch of physics that studies light

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<span class="mw-page-title-main">Optical microscope</span> Microscope that uses visible light

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In optical mineralogy and petrography, a thin section is a thin slice of a rock or mineral sample, prepared in a laboratory, for use with a polarizing petrographic microscope, electron microscope and electron microprobe. A thin sliver of rock is cut from the sample with a diamond saw and ground optically flat. It is then mounted on a glass slide and then ground smooth using progressively finer abrasive grit until the sample is only 30 μm thick. The method uses the Michel-Lévy interference colour chart to determine thickness, typically using quartz as the thickness gauge because it is one of the most abundant minerals.

<span class="mw-page-title-main">Optical mineralogy</span> Optical properties of rocks and minerals

Optical mineralogy is the study of minerals and rocks by measuring their optical properties. Most commonly, rock and mineral samples are prepared as thin sections or grain mounts for study in the laboratory with a petrographic microscope. Optical mineralogy is used to identify the mineralogical composition of geological materials in order to help reveal their origin and evolution.

<span class="mw-page-title-main">Extinction (optical mineralogy)</span>

Extinction is a term used in optical mineralogy and petrology, which describes when cross-polarized light dims, as viewed through a thin section of a mineral in a petrographic microscope. Isotropic minerals, opaque (metallic) minerals, and amorphous materials (glass) do not allow light transmission under cross-polarized light. Anisotropic minerals specifically will show one extinction for each 90 degrees of stage rotation.

Igneous petrology is the study of igneous rocks—those that are formed from magma. As a branch of geology, igneous petrology is closely related to volcanology, tectonophysics, and petrology in general. The modern study of igneous rocks utilizes a number of techniques, some of them developed in the fields of chemistry, physics, or other earth sciences. Petrography, crystallography, and isotopic studies are common methods used in igneous petrology.

<span class="mw-page-title-main">Interference colour chart</span>

In optical mineralogy, an interference colour chart, also known as the Michel-Levy chart, is a tool first developed by Auguste Michel-Lévy to identify minerals in thin section using a petrographic microscope. With a known thickness of the thin section, minerals have specific and predictable colours in cross-polarized light, and this chart can help identify minerals. The colours are produced by the difference in speed in the fast and slow rays, also known as birefringence.

A conoscopic interference pattern or interference figure is a pattern of birefringent colours crossed by dark bands, which can be produced using a geological petrographic microscope for the purposes of mineral identification and investigation of mineral optical and chemical properties. The figures are produced by optical interference when diverging light rays travel through an optically non-isotropic substance – that is, one in which the substance's refractive index varies in different directions within it. The figure can be thought of as a "map" of how the birefringence of a mineral would vary with viewing angle away from perpendicular to the slide, where the central colour is the birefringence seen looking straight down, and the colours further from the centre equivalent to viewing the mineral at ever increasing angles from perpendicular. The dark bands correspond to positions where optical extinction would be seen. In other words, the interference figure presents all possible birefringence colours for the mineral at once.

<span class="mw-page-title-main">Polarized light microscopy</span>

Polarized light microscopy can mean any of a number of optical microscopy techniques involving polarized light. Simple techniques include illumination of the sample with polarized light. Directly transmitted light can, optionally, be blocked with a polariser orientated at 90 degrees to the illumination. More complex microscopy techniques which take advantage of polarized light include differential interference contrast microscopy and interference reflection microscopy. Scientists will often use a device called a polarizing plate to convert natural light into polarized light.

References

  1. "R. Fuess Berlin #131. The Rosenbusch model c.1878". www.antique-microscopes.com. Retrieved 2020-10-13.