Vacuum ceramic filter

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A vacuum ceramic filter is designed to separate liquids from solids for dewatering of ore concentrates purposes. The device consists of a rotator, slurry tank, ceramic filter plate, distributor, discharge scraper, cleaning device, frame, agitating device, pipe system, vacuum system, automatic acid dosing system, automatic lubricating system, valve and discharge chute. The operation and construction principle of vacuum ceramic filter resemble those of a conventional disc filter, but the filter medium is replaced by a finely porous ceramic disc. The disc material is inert, has a long operational life and is resistant to almost all chemicals. Performance can be optimized by taking into account all those factors which affect the overall efficiency of the separation process. Some of the variables affecting the performance of a vacuum ceramic filter include the solid concentration, speed rotation of the disc, slurry level in the feed basin, temperature of the feed slurry, and the pressure during dewatering stages and filter cake formation. [1]

Contents

Range of applications

Vacuum ceramic filters are to be found in the following industries:

The process is used during a large continuous process of separating free filtering suspensions where washing is not required. [2] Basically the filter works to separates solid-liquid mixtures by removing the water from mineral concentrates and moulding the feed slurries into pellets. [3] This is accomplished by capillary action under low vacuum pressure. [2] The pelletizing of the slurries is done by adding some solid matter to the sewage sludge so that water can be easily removed from the mixture. Eventually, the final cake products contain very little moisture and can be deposited as sewage. This process is commonly followed by bleaching and heating the cake. The end product of this filtration is a dry cake and filtrate containing no solid product.

Advantages and limitations

The main advantage over other filtration systems is the reduction in energy consumption, up to 90% because no air flows through the discs [4] due to the use of capillary force acting on the pores. Air breakthrough is prevented by the fine pores of the filter, thus allowing retention of higher vacuum levels. [5] Therefore, the vacuum losses are less, which means the vacuum pump required is smaller than in conventional disc filters, thus minimizing operating costs. Power consumed by a vacuum ceramic filter with 45 m2 of filtration area is 15 kW while 170 kW is consumed by similar filters with cloth membranes. [6]

Generally, conventional disc filters are not suitable for cake washing because the water quickly runs off the surface of the cake. As the cake solids are sprayed with a wash liquid to remove impurities, they are not suitable for conventional filtration systems where channelling or uneven distribution occurs, leading to cake cracking. [4] However, cake washing has been proved to be more efficient with vacuum ceramic filters due to the steady flow profile and the even distribution of the cake. [7]

A further advantage of vacuum ceramic filter is the high output capacity with a very low water content and drier filter cake. [4] By comparison, the performance of a VDFK-3 ceramic filter was compared with the existing BOU-40 and BLN40-3 drum type vacuum filters to filter aluminium hydroxide. From the results, the average moisture content was 5% (abs? or rel?) lower when a vacuum ceramic filter was used. [6]

Vacuum ceramic filters also have a longer service life while cloth filters have to be replaced, which eventually increases the moisture content of the cake, lowers the productivity and disturbs the production operations. [6] In addition, the ceramic filter is both mechanically and chemically reliable enough to withstand regeneration. [8]

Whilst the vacuum ceramic filter has proved to be a great innovation, there are still some limitations involved when operating the equipment. Ceramic filters exhibit large fluctuations in the recoiling washing pressure (0.05~0.35  MPa). This raises the short-term negative pressure and induces dilute acid due to the falling suck phenomenon. Therefore, the cleaning effect of the ceramic plates and the efficiency of the filter will be negatively affected. [9]

Designs available

There are many design criteria which vary according to the type of disc and the required filtering capacity. [10] The typical filter for extracting iron contains 12 ceramic filtering plates of the filtering elements (discs), which have a diameter of about 2705 mm, making the total filter surface 120 m2. [11] This filter is most suited to filter feed slurries with high solid concentrations (5-20% w/w) [2] and particles ranging in size from 1–700  μm. [2] The area of the filters available in the ceramic filter is up to 45 m2, making them useful for metal and mineral concentrate processing. [2]

The ceramic discs are available in two types, cast plate and membrane plate. [10] The cast plate is a one piece ceramic plate with a homogeneous surface and a granulated core. The filter medium of the cast plate is the thick walls, separated by ceramic granules. These features form a rigid mechanical structure. The membrane plate type contains a thin membrane over a coarser core and a multi-layer porous structure made of aluminium oxide. The coarse part of the equipment provides mechanical strength to its structure while the intermediate layer acts as a membrane carrier. The outer layer membrane acts as a filtering layer. The filtration layer of the ceramic filter has uniform pores, which means that only a certain size of particles can be filtered by using vacuum ceramic filters.

Main process characteristics

There are at least three stages involve in the operation of a vacuum disc filter:

Stage 1: Cake formation

The discs rotate in a slurry trough, compartmentalized to reduce the volume held in it at any one time, and therefore to reduce the residence time of slurry in the trough. The time available for this stage depends on two factors, the rotation speed of the disc and the height of the slurry level in the basin. [7] A vacuum is applied inside the discs to promote cake filtration.

Stage 2: Cake dewatering

Washing is largely restricted to the upper portions where the cake surface is nearly horizontal in orientation, [2] which occurs at the temperature of the feed. The ceramic filter uses a sintered alumina disc to dewater slurry under low vacuum. The dewatering occurs by drawing water from the slurry by capillary action. This ensures that no air or particles are drawn into the filter medium to cause blockage. [3] However, if too much wash water is applied then it can cascade down the cake and into the feed trough, where it merely dilutes the slurry.

Stage 3: Cake drying

The final water (moisture) content in the cake is regulated by passing dry (cold or hot) air or gas through the cake. Drying time is dependent on the distribution valve timing, slurry level on the basin, rotation speed, and scraper position. [12]

Stage 4: Cake discharge

These are the typical conditions for the overall operation of the vacuum ceramic filter:

Assessment of main characteristics

The most important operating parameters of disc filters are the height of the slurry tank, agitation and the intensity and rotation speed of the disc as these will determine the cake formation and drying times. [7] It is important to continuously agitate the slurry in order to prevent sedimentation of the solids. Excessively high agitation intensity may affect cake formation or change the particle size distribution of the product. One of the most commonly used agitators for filtration using vacuum disc filters is an oscillating cradle-type agitator located in the bottom of the basin, which requires fairly high rotation speeds to form homogeneous slurry. For processing rapidly settling high concentration slurries, bottom-feed rotary disc filters are usually used.

Stage 1: Filtration

The filtrate from the internal passages of the discs is removed by the low vacuum used in the filter, while the small pressure differential across the disc causes cake formation. [3] With a thicker cake produced in this stage, more effective washing is achieved at higher wash liquor flows. However, this causes larger air volumes to be consumed at discharge due to reduced resistance and marginally lower cake moisture.

Stage 2: Dewatering

In rare cases, due to the even structure of the cakes formed, the steady flow profile of the ceramic filter media and the gas free filtrate flow cake, washing has proved to be efficient in ceramic disc filters. [7] The formation of thicker cakes during filtration and higher vacuum level leads to greater removal of solute. [2]

Stage 3: Discharge

The basic scraper works well when the cakes are relatively thick and non-sticky. The final cakes are discharged by blade or wire scrapers on either side of the discs However, other types of agitators should be considered and installed if the cake is sticky or thin. An air blow-back system is often employed to aid cake removal where wetter cakes are discharged from disc filter.

Design heuristics

Rate of cake buildupRateMedium used for filtration
Rapid0.1-10.0 cm/sBelts, top feed drums, pusher-type centrifuges
Medium0.1-10.0 cm/minVacuum drums, disks, peeler type centrifuges
Slow0.1- 10.0 cm/hPressure filters, sedimentation centrifuges

Waste stream production and post-treatment

Filtrate is the waste that has been discharge in vacuum ceramic filters through the waste stream. During cake washing, a wash liquid is sprayed on the cake solids to remove impurities or additional filtrate. The filtrate goes into filtrate tank and is drained through a discharge system. However, the filtrate is recyclable and has low suspended solid content. Thus, it can be recycled through the system without further treatment. Filtrate is used to flush the disc during back flow washing to clean the micro-porous structure and remove any residual cake.

New developments

One improvement over the standard design of ceramic vacuum filter is to use serialized pore size distributions of non-fibrous porous ceramic filters. [12] The porosity of this type of ceramic can be varied from 20% to 60% by volume, which allows a low-pressure drop of liquid and gas flow. [12] Custom sizes from 1 mm diameter/0.5 mm bore of porous ceramic filters are available for a range of designs. A non-fibrous porous ceramic filter is more resistant in alkaline and acidic conditions compared to fibrous ceramic filters. Thus, it has a longer service life as it has good wearing and erosion resistance as well as being able to withstand high temperatures. [12]

Another improvement is applied at the regeneration stage when the residual filter cake is removed by back-flushing the clean plant water to wash the internal ceramic filter. [15] Filter cake dewatering of ceramic filters produces low final cake moistures at minimum operation and maintenance costs. The residuals moisture are removed from the filter cake due to capillary action within the ceramic elements, which rotate above the slurry level. This process gives maximum filtration, and the final cake can be maintained at the lowest moisture content due to the effective cleaning of both ceramic sectors. In addition, performance can be optimized by using an ultrasonic cleaning system to achieve efficient operation conditions [15] for regeneration of plates. The use of filtrate in looped water cycle in the design operation can reduce the water consumption up to 30-50%. [15] High filtrate purity can be obtained, as there is only 0.001-0.005 g/L solids in the filtrate produced from this process. [12] This eventually results in the reduction of polymer flocculant consumption in thickeners. Ceramic scraper knives have been introduced to this design as they are able to shave through the mass formed in filter cake dewatering. [15] The remaining layer of solid residue on the filter provides protection from mechanical abrasion. Therefore, the maintenance costs can be reduced while the service life of the ceramic filter increases.

See also

Related Research Articles

<span class="mw-page-title-main">Filtration</span> Process that separates solids from fluids

Filtration is a physical separation process that separates solid matter and fluid from a mixture using a filter medium that has a complex structure through which only the fluid can pass. Solid particles that cannot pass through the filter medium are described as oversize and the fluid that passes through is called the filtrate. Oversize particles may form a filter cake on top of the filter and may also block the filter lattice, preventing the fluid phase from crossing the filter, known as blinding. The size of the largest particles that can successfully pass through a filter is called the effective pore size of that filter. The separation of solid and fluid is imperfect; solids will be contaminated with some fluid and filtrate will contain fine particles. Filtration occurs both in nature and in engineered systems; there are biological, geological, and industrial forms.

<span class="mw-page-title-main">Coal preparation plant</span> Coal processing stage

A coal preparation plant is a facility that washes coal of soil and rock, crushes it into graded sized chunks (sorting), stockpiles grades preparing it for transport to market, and more often than not, also loads coal into rail cars, barges, or ships.

<span class="mw-page-title-main">Sewage sludge treatment</span> Processes to manage and dispose of sludge during sewage treatment

Sewage sludge treatment describes the processes used to manage and dispose of sewage sludge produced during sewage treatment. Sludge treatment is focused on reducing sludge weight and volume to reduce transportation and disposal costs, and on reducing potential health risks of disposal options. Water removal is the primary means of weight and volume reduction, while pathogen destruction is frequently accomplished through heating during thermophilic digestion, composting, or incineration. The choice of a sludge treatment method depends on the volume of sludge generated, and comparison of treatment costs required for available disposal options. Air-drying and composting may be attractive to rural communities, while limited land availability may make aerobic digestion and mechanical dewatering preferable for cities, and economies of scale may encourage energy recovery alternatives in metropolitan areas.

<span class="mw-page-title-main">Rotary vacuum-drum filter</span> Drum used to filter a slurry

A Rotary Vacuum Filter Drum consists of a cylindrical filter membrane that is partly sub-merged in a slurry to be filtered. The inside of the drum is held lower than the ambient pressure. As the drum rotates through the slurry, the liquid is sucked through the membrane, leaving solids to cake on the membrane surface while the drum is submerged. A knife or blade is positioned to scrape the product from the surface.

<span class="mw-page-title-main">Agitated Nutsche Filter</span> Type of filter for liquid

Agitated Nutsche filter (ANF) is a filtration technique used in applications such as dye, paint, and pharmaceutical production and waste water treatment. Safety requirements and environmental concerns due to solvent evaporation led to the development of this type of filter wherein filtration under vacuum or pressure can be carried out in closed vessels and solids can be discharged straightaway into a dryer.

<span class="mw-page-title-main">Cross-flow filtration</span>

In chemical engineering, biochemical engineering and protein purification, crossflow filtration is a type of filtration. Crossflow filtration is different from dead-end filtration in which the feed is passed through a membrane or bed, the solids being trapped in the filter and the filtrate being released at the other end. Cross-flow filtration gets its name because the majority of the feed flow travels tangentially across the surface of the filter, rather than into the filter. The principal advantage of this is that the filter cake is substantially washed away during the filtration process, increasing the length of time that a filter unit can be operational. It can be a continuous process, unlike batch-wise dead-end filtration.

<span class="mw-page-title-main">Filter press</span>

An industrial filter press is a tool used in separation processes, specifically to separate solids and liquids. The machine stacks many filter elements and allows the filter to be easily opened to remove the filtered solids, and allows easy cleaning or replacement of the filter media.

Electrofiltration is a method that combines membrane filtration and electrophoresis in a dead-end process.

<span class="mw-page-title-main">Belt filter</span>

The belt filter is an industrial machine, used for solid/liquid separation processes, particularly the dewatering of sludges in the chemical industry, mining and water treatment. Belt filter presses are also used in the production of apple juice, cider and winemaking. The process of filtration is primarily obtained by passing a pair of filtering cloths and belts through a system of rollers. The system takes a sludge or slurry as a feed, and separates it into a filtrate and a solid cake.

Membrane technology encompasses the scientific processes used in the construction and application of membranes. Membranes are used to facilitate the transport or rejection of substances between mediums, and the mechanical separation of gas and liquid streams. In the simplest case, filtration is achieved when the pores of the membrane are smaller than the diameter of the undesired substance, such as a harmful microorganism. Membrane technology is commonly used in industries such as water treatment, chemical and metal processing, pharmaceuticals, biotechnology, the food industry, as well as the removal of environmental pollutants.

A filter drier is a piece of process equipment used during the filtration and drying phase of a pharmaceutical, bio pharmaceutical or chemical process for an active pharmaceutical ingredient (API) or other compounds production. Filter dryers are designed for washing and isolating solids with or without integrated containment systems.

A pusher centrifuge is a type of filtration technique that offers continuous operation to de-water and wash materials such as relatively in-compressible feed solids, free-draining crystalline, polymers and fibrous substances. It consists of a constant speed rotor and is fixed to one of several baskets. This assembly is applied with centrifugal force that is generated mechanically for smaller units and hydraulically for larger units to enable separation.

The peeler centrifuge is a device that performs by rotating filtration basket in an axis. A centrifuge follows on the principle of centrifugal force to separate solids from liquids by density difference. High rotation speed provides high centrifugal force that allows the suspended solid in feed to settle on the inner surface of basket. There are three kinds of centrifuge, horizontal, vertical peeler centrifuge and siphon peeler centrifuge. These classes of instrument apply to various areas such as fertilisers, pharmaceutical, plastics and food including artificial sweetener and modified starch.

A centrifuge is a device that employs a high rotational speed to separate components of different densities. This becomes relevant in the majority of industrial jobs where solids, liquids and gases are merged into a single mixture and the separation of these different phases is necessary. A decanter centrifuge separates continuously solid materials from liquids in the slurry, and therefore plays an important role in the wastewater treatment, chemical, oil, and food processing industries. There are several factors that affect the performance of a decanter centrifuge, and some design heuristics are to be followed which are dependent upon given applications.

A solid bowl centrifuge is a type of centrifuge that uses the principle of sedimentation. A centrifuge is used to separate a mixture that consists of two substances with different densities by using the centrifugal force resulting from continuous rotation. It is normally used to separate solid-liquid, liquid-liquid, and solid-solid mixtures. Solid bowl centrifuges are widely used in various industrial applications, such as wastewater treatment, coal manufacturing, and polymer manufacturing. One advantage of solid bowl centrifuges for industrial uses is the simplicity of installation compared to other types of centrifuge. There are three design types of solid bowl centrifuge, which are conical, cylindrical, and conical-cylindrical.

A conical plate centrifuge is a type of centrifuge that has a series of conical discs which provides a parallel configuration of centrifugation spaces.

Screen/Scroll centrifuge is a filtering or screen centrifuge which is also known as worm screen or conveyor discharge centrifuge. This centrifuge was first introduced in the midst of 19th century. After developing new technologies over the decades, it is now one of the widely used processes in many industries for the separation of crystalline, granular or fibrous materials from a solid-liquid mixture. Also, this process is considered to dry the solid material. This process has been some of the most frequently seen within, especially, coal preparation industry. Moreover, it can be found in other industries such as chemical, environmental, food and other mining fields.

<span class="mw-page-title-main">Tilting pan filter</span>

A tilting pan filter is a chemical equipment used in continuous solid-liquid filtration.

Pile Cloth Media Filtration is a mechanical process for the separation of organic and inorganic solids from liquids. It belongs to the processes of surface filtration and cake filtration where, in addition to the sieve effect, real filtration effects occur over the depth of the pile layer. Pile Cloth Media Filtration represents a branch of cloth filtration processes and is used for water and wastewater treatment in medium and large scale. In Pile Cloth Media Filtration, three-dimensional textile fabrics are used as filter media. During the filter cleaning of the pile layer the filtration process continues and is not interrupted.

Diatomaceous earth (DE) filtration is a special filtration process that removes particles from liquids as it passes through a layer of fossilized remains of microscopic water organism called diatoms. These diatoms are mined from diatomite deposits which are located along the Earth's surface as they have accumulated in sediment of open and moving bodies of water. Obtained diatomaceous earth is then purified using acid leaching or liquid-liquid extraction in order for it to be used in any form of application. The process of D.E. filtration is composed of three main stages: pre-coating, body feed, and cleaning.

References

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Further reading