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A particulate matter sampler is an instrument for measuring the properties (such as mass concentration or chemical composition) of particulates in the ambient air.
Two different types of particulate matter samplers exist that measure particulate mass concentration: manual samplers and automated samplers.
Manual samplers draw a known volume of air through a filter. The filter is weighed on an analytical balance before and after sampling, and the difference in weight divided by the volume of air pulled through the filter gives the mass concentration of the particulate. [1]
Automated samplers do the weighing in the field. There are two types of automated samplers in common usage: samplers that use a beta gauge for mass measurement and samplers that use a tapered element oscillating microbalance (TEOM) for mass measurement.
Beta gauge particulate samplers have an appearance that is similar to a reel to reel tape recorder. Air is pulled through a filter tape to accumulate a sample, the mass of the tape before and after sampling is determined by advancing the tape spot into the beta attenuation cell.
The tapered element oscillating microbalance (TEOM) particulate sampler operates by drawing air through a filter attached at the tip of a glass tube. An electrical circuit places the tube into oscillation, and the resonant frequency of the tube is proportional to the square root of the mass on the filter.
Recently, microphone based instruments have been devised that monitor noise levels in specific frequency bands to predict local PNC levels. Prototypes of such instruments have been tested in Europe and in Bangalore. [2]
Particles of different sizes have different health effects. Inertial separators are used to eliminate particles outside of the desired size range. If a gas stream containing particles of different sizes is forced to turn a sharp corner, the inertia of the large particles causes them to separate from the gas stream lines. The larger particles can be collected and removed from the gas stream after collisions with the walls of the vessel.
The two common types of inertial separators are cyclones, which spin the gas stream, causing collisions of the heavier particles with the outside of the cyclone wall, and impactors, where the gas particle stream is directed at a greased metal plate and turned at the last moment, causing the larger particles to stick to the greased plate.
Modern particulate samplers use a volumetric flow control system that pulls air through the particle separator at the velocity required to achieve the desired cutpoint.
For air pollution applications, the definition of "particulate" does not include uncombined water, and water from a particulate sample must be removed before it is weighed. This can be done either by heating the sample to evaporate the water or by placing the sample in a low humidity environment before weighing.
A nephelometer or aerosol photometer is an instrument for measuring the concentration of suspended particulates in a liquid or gas colloid. A nephelometer measures suspended particulates by employing a light beam and a light detector set to one side of the source beam. Particle density is then a function of the light reflected into the detector from the particles. To some extent, how much light reflects for a given density of particles is dependent upon properties of the particles such as their shape, color, and reflectivity. Nephelometers are calibrated to a known particulate, then use environmental factors (k-factors) to compensate lighter or darker colored dusts accordingly. K-factor is determined by the user by running the nephelometer next to an air sampling pump and comparing results. There are a wide variety of research-grade nephelometers on the market as well as open source varieties.
Cyclonic separation is a method of removing particulates from an air, gas or liquid stream, without the use of filters, through vortex separation. When removing particulate matter from liquid, a hydrocyclone is used; while from gas, a gas cyclone is used. Rotational effects and gravity are used to separate mixtures of solids and fluids. The method can also be used to separate fine droplets of liquid from a gaseous stream.
A particulate air filter is a device composed of fibrous, or porous materials which removes solid particulates such as dust, pollen, mold, and bacteria from the air. Filters containing an adsorbent or catalyst such as charcoal (carbon) may also remove odors and gaseous pollutants such as volatile organic compounds or ozone. Air filters are used in applications where air quality is important, notably in building ventilation systems and in engines.
An ampoule is a small sealed vial which is used to contain and preserve a sample, usually a solid or liquid. Ampoules are usually made of glass.
A microbalance is an instrument capable of making precise measurements of weight of objects of relatively small mass: of the order of a million parts of a gram. In comparison, a standard analytical balance is 100 times less sensitive; i.e. it is limited in precision to 0.1 milligrams. Microbalances are generally used in a laboratory as standalone instruments but are also incorporated into other instruments, such as thermogravimetry, sorption/desorption systems, and surface property instruments. It is the precision of the microbalance that distinguishes it from other weighing devices.
A Lucas cell is a type of scintillation counter. It is used to acquire a gas sample, filter out the radioactive particulates through a special filter and then count the radioactive decay. The inside of the gas chamber is coated with ZnS(Ag) - a chemical that emits light when struck by alpha particles. A photomultiplier tube at the top of the chamber counts the photons and sends the count to a data logger.
A dust collector is a system used to enhance the quality of air released from industrial and commercial processes by collecting dust and other impurities from air or gas. Designed to handle high-volume dust loads, a dust collector system consists of a blower, dust filter, a filter-cleaning system, and a dust receptacle or dust removal system. It is distinguished from air purifiers, which use disposable filters to remove dust.
A particle counter is used for monitoring and diagnosing particle contamination within specific clean media, including air, water and chemicals. Particle counters are used in a variety of applications in support of clean manufacturing practices, industries include: electronic components and assemblies, pharmaceutical drug products and medical devices, and industrial technologies such as oil and gas.
A coal preparation plant is a facility that washes coal of soil and rock, crushes it into graded sized chunks (sorting), stockpiles grades preparing it for transport to market, and more often than not, also loads coal into rail cars, barges, or ships.
A venturi scrubber is designed to effectively use the energy from a high-velocity inlet gas stream to atomize the liquid being used to scrub the gas stream. This type of technology is a part of the group of air pollution controls collectively referred to as wet scrubbers.
Bioaerosols are a subcategory of particles released from terrestrial and marine ecosystems into the atmosphere. They consist of both living and non-living components, such as fungi, pollen, bacteria and viruses. Common sources of bioaerosols include soil, water, and sewage.
The particle-size distribution (PSD) of a powder, or granular material, or particles dispersed in fluid, is a list of values or a mathematical function that defines the relative amount, typically by mass, of particles present according to size. Significant energy is usually required to disintegrate soil, etc. particles into the PSD that is then called a grain size distribution.
Aerosol Impaction is the process in which particles are removed from an air stream by forcing the gases to make a sharp bend. Particles above a certain size possess so much momentum that they can not follow the air stream and strike a collection surface which is available for later analysis of mass and composition. Removal of particles from an air-stream by impaction followed by mass and composition analysis has always been a different approach as to filter sampling, yet has been little utilized for routine analysis because of lack of suitable analytical methods.
An aethalometer is an instrument for measuring the concentration of optically absorbing (‘black’) suspended particulates in a gas colloid stream; commonly visualized as smoke or haze, often seen in ambient air under polluted conditions. The word aethalometer is derived from the Classical Greek verb ‘aethaloun’, meaning ‘to blacken with soot’.
Beta attenuation monitoring (BAM) is a widely used air monitoring technique employing the absorption of beta radiation by solid particles extracted from air flow. This technique allows for the detection of PM10 and PM2.5, which are monitored by most air pollution regulatory agencies. The main principle is based on a kind of Bouguer (Lambert–Beer) law: the amount by which the flow of beta radiation (electrons) is attenuated by a solid matter is exponentially dependent on its mass and not on any other feature (such as density, chemical composition or some optical or electrical properties) of this matter. So, the air is drawn from outside of the detector through an "infinite" (cycling) ribbon made from some filtering material so that the particles are collected on it. There are two sources of beta radiation placed one before and one after the region where air flow passes through the ribbon leaving particles on it; and there are also two detectors on the opposite side of the ribbon, facing the detectors. The sources' intensity and detectors' sensitivity being the same (or corrected with appropriate calibration lookup table), the intensity of beta rays detected by one of detectors is compared to that of the other. Thus one can deduce how much mass has the ribbon acquired upon being exposed to air flow; knowing the drain velocity, actual particle mass concentration in air could be assessed.
Aerosol mass spectrometry is the application of mass spectrometry to the analysis of the composition of aerosol particles. Aerosol particles are defined as solid and liquid particles suspended in a gas (air), with size range of 3 nm to 100 μm in diameter and are produced from natural and anthropogenic sources, through a variety of different processes that include wind-blown suspension and combustion of fossil fuels and biomass. Analysis of these particles is important owing to their major impacts on global climate change, visibility, regional air pollution and human health. Aerosols are very complex in structure, can contain thousands of different chemical compounds within a single particle, and need to be analysed for both size and chemical composition, in real-time or off-line applications.
Air pollution measurement is the process of collecting and measuring the components of air pollution, notably gases and particulates. The earliest devices used to measure pollution include rain gauges, Ringelmann charts for measuring smoke, and simple soot and dust collectors known as deposit gauges. Modern air pollution measurement is largely automated and carried out using many different devices and techniques. These range from simple absorbent test tubes known as diffusion tubes through to highly sophisticated chemical and physical sensors that give almost real-time pollution measurements, which are used to generate air quality indexes.
A tapered element oscillating microbalance (TEOM) is an instrument used for real-time detection of aerosol particles by measuring their mass concentration. It makes use of a small vibrating glass tube whose oscillation frequency changes when aerosol particles are deposited on it increasing its inertia. TEOM-based devices have been approved by the U.S. Environmental Protection Agency for environmental air quality monitoring, and by the U.S. Mine Safety and Health Administration for monitoring coal dust exposure for miners to prevent several respiratory diseases.
Workplace exposure monitoring is the monitoring of substances in a workplace that are chemical or biological hazards. It is performed in the context of workplace exposure assessment and risk assessment. Exposure monitoring analyzes hazardous substances in the air or on surfaces of a workplace, and is complementary to biomonitoring, which instead analyzes toxicants or their effects within workers.
NIOSH Manual of Analytical Methods (see chapters on aerosol sampling)
