Dye penetrant inspection (DP), also called liquid penetrate inspection (LPI) or penetrant testing (PT), is a widely applied and low-cost inspection method used to check surface-breaking defects in all non-porous materials (metals, plastics, or ceramics). The penetrant may be applied to all non-ferrous materials and ferrous materials, although for ferrous components magnetic-particle inspection is often used instead for its subsurface detection capability. LPI is used to detect casting, forging and welding surface defects such as hairline cracks, surface porosity, leaks in new products, and fatigue cracks on in-service components.
The oil and whiting method used in the railroad industry in the early 1900s was the first recognized use of the principles of penetrants to detect cracks. The oil and whiting method used an oil solvent for cleaning followed by the application of a whiting or chalk coating, which absorbed oil from the cracks revealing their locations. Soon a dye was added to the liquid. By the 1940s, the fluorescent or visible dye was added to the oil used to penetrate test objects.
Experience showed that temperature and soak time was important. This started the practice of written instructions to provide standard, uniform results. The use of written procedures has evolved, giving the ability for design engineers and manufacturers to get the high standard results from any properly trained and certified liquid penetrant testing technician.
DPI is based upon capillary action, where low surface tension fluid penetrates into clean and dry surface-breaking discontinuities. The penetrant may be applied to the test component by dipping, spraying, or brushing. After adequate penetration time has been allowed, the excess penetrant is removed and a developer is applied. The developer helps to draw penetrant out of the flaw so that an invisible indication becomes visible to the inspector. Inspection is performed under ultraviolet or white light, depending on the type of dye used - fluorescent or nonfluorescent (visible).
Below are the main steps of Liquid Penetrant Inspection:
1. Pre-cleaning:
The test surface is cleaned to remove any dirt, paint, oil, grease or any loose scale that could either keep penetrant out of a defect or cause irrelevant or false indications. Cleaning methods may include solvents, alkaline cleaning steps, vapour degreasing, or media blasting. The end goal of this step is a clean surface where any defects present are open to the surface, dry, and free of contamination. Note that if media blasting is used, it may "work over" small discontinuities in the part, and an etching bath is recommended as a post-blasting treatment.
2. Application of Penetrant:
The penetrant is then applied to the surface of the item being tested. The penetrant is usually a brilliant coloured mobile fluid with high wetting capability. [1] The penetrant is allowed "dwell time" to soak into any flaws (generally 5 to 30 minutes). The dwell time mainly depends upon the penetrant being used, the material being tested and the size of flaws sought. As expected, smaller flaws require a longer penetration time. Due to their incompatible nature, one must be careful not to apply solvent-based penetrant to a surface which is to be inspected with a water-washable developer.
3. Excess Penetrant Removal:
The excess penetrant is then removed from the surface. The removal method is controlled by the type of penetrant used. Water-washable, solvent-removable, lipophilic post-emulsifiable, or hydrophilic post-emulsifiable are the common choices. Emulsifiers represent the highest sensitivity level, and chemically interact with the oily penetrant to make it removable with a water spray. When using solvent remover and lint-free cloth it is important to not spray the solvent on the test surface directly, because this can remove the penetrant from the flaws. If excess penetrant is not properly removed, once the developer is applied, it may leave a background in the developed area that can mask indications or defects. In addition, this may also produce false indications severely hindering the ability to do a proper inspection. Also, the removal of excessive penetrant is done towards one direction either vertically or horizontally as the case may be.
4. Application of Developer:
After excess penetrant has been removed, a white developer is applied to the sample. Several developer types are available, including: non-aqueous wet developer, dry powder, water-suspendable, and water-soluble. Choice of developer is governed by penetrant compatibility (one can't use water-soluble or -suspendable developer with water-washable penetrant), and by inspection conditions. When using non-aqueous wet developer (NAWD) or dry powder, the sample must be dried prior to application, while soluble and suspendable developers are applied with the part still wet from the previous step. NAWD is commercially available in aerosol spray cans, and may employ acetone, isopropyl alcohol, or a propellant that is a combination of the two. Developer should form a semi-transparent, even coating on the surface.
The developer draws penetrant from defects out onto the surface to form a visible indication, commonly known as bleed-out. Any areas that bleed out can indicate the location, orientation and possible types of defects on the surface. Interpreting the results and characterizing defects from the indications found may require some training and/or experience [the indication size is not the actual size of the defect].
5. Inspection:
The inspector will use visible light with adequate intensity (100 foot-candles or 1100 lux is typical) for visible dye penetrant. Ultraviolet (UV-A) radiation of adequate intensity (1,000 micro-watts per centimetre squared is common), along with low ambient light levels (less than 2 foot-candles) for fluorescent penetrant examinations. Inspection of the test surface should take place after 10- to 30-minute development time, and is dependent on the penetrant and developer used. This time delay allows the blotting action to occur. The inspector may observe the sample for indication formation when using visible dye. It is also good practice to observe indications as they form because the characteristics of the bleed out are a significant part of interpretation characterization of flaws.
6. Post Cleaning:
The test surface is often cleaned after inspection and recording of defects, especially if post-inspection coating processes are scheduled.
The main advantages of DPI are the speed of the test and the low cost. Disadvantages include the detection of only surface flaws, skin irritation, and the inspection should be on a smooth clean surface where excessive penetrant can be removed prior to being developed. Conducting the test on rough surfaces, such as "as-welded" welds, will make it difficult to remove any excessive penetrant and could result in false indications. Water-washable penetrant should be considered here if no other option is available. Also, on certain surfaces, a great enough colour contrast cannot be achieved or the dye will stain the workpiece. [2]
Limited training is required for the operator — although experience is quite valuable. Proper cleaning is necessary to assure that surface contaminants have been removed and any defects present are clean and dry. Some cleaning methods have been shown to be detrimental to test sensitivity, so acid etching to remove metal smearing and re-open the defect may be necessary. [3]
Penetrant inspection can only be applied on non-porous materials
Paint is a material or mixture that, after applied to a solid material and allowed to dry, adds a film-like layer. As art, this is used to create an image, known as a painting. Paint can be made in many colors and types. Most paints are either oil-based or water-based, and each has distinct characteristics.
Nondestructive testing (NDT) is any of a wide group of analysis techniques used in science and technology industry to evaluate the properties of a material, component or system without causing damage. The terms nondestructive examination (NDE), nondestructive inspection (NDI), and nondestructive evaluation (NDE) are also commonly used to describe this technology. Because NDT does not permanently alter the article being inspected, it is a highly valuable technique that can save both money and time in product evaluation, troubleshooting, and research. The six most frequently used NDT methods are eddy-current, magnetic-particle, liquid penetrant, radiographic, ultrasonic, and visual testing. NDT is commonly used in forensic engineering, mechanical engineering, petroleum engineering, electrical engineering, civil engineering, systems engineering, aeronautical engineering, medicine, and art. Innovations in the field of nondestructive testing have had a profound impact on medical imaging, including on echocardiography, medical ultrasonography, and digital radiography.
Magnetic particle inspection (MPI) is a nondestructive testing process where a magnetic field is used for detecting surface, and shallow subsurface, discontinuities in ferromagnetic materials. Examples of ferromagnetic materials include iron, nickel, cobalt, and some of their alloys. The process puts a magnetic field into the part. The piece can be magnetized by direct or indirect magnetization. Direct magnetization occurs when the electric current is passed through the test object and a magnetic field is formed in the material. Indirect magnetization occurs when no electric current is passed through the test object, but a magnetic field is applied from an outside source. The magnetic lines of force are perpendicular to the direction of the electric current, which may be either alternating current (AC) or some form of direct current (DC).
Plastic welding is welding for semi-finished plastic materials, and is described in ISO 472 as a process of uniting softened surfaces of materials, generally with the aid of heat. Welding of thermoplastics is accomplished in three sequential stages, namely surface preparation, application of heat and pressure, and cooling. Numerous welding methods have been developed for the joining of semi-finished plastic materials. Based on the mechanism of heat generation at the welding interface, welding methods for thermoplastics can be classified as external and internal heating methods, as shown in Fig 1.
Eddy-current testing is one of many electromagnetic testing methods used in nondestructive testing (NDT) making use of electromagnetic induction to detect and characterize surface and sub-surface flaws in conductive materials.
Ultrasonic testing (UT) is a family of non-destructive testing techniques based on the propagation of ultrasonic waves in the object or material tested. In most common UT applications, very short ultrasonic pulse waves with centre frequencies ranging from 0.1-15 MHz and occasionally up to 50 MHz, are transmitted into materials to detect internal flaws or to characterize materials. A common example is ultrasonic thickness measurement, which tests the thickness of the test object, for example, to monitor pipework corrosion and erosion. Ultrasonic testing is extensively used to detect flaws in welds.
Phased array ultrasonics (PA) is an advanced method of ultrasonic testing that has applications in medical imaging and industrial nondestructive testing. Common applications are to noninvasively examine the heart or to find flaws in manufactured materials such as welds. Single-element probes, known technically as monolithic probes, emit a beam in a fixed direction. To test or interrogate a large volume of material, a conventional probe must be physically scanned to sweep the beam through the area of interest. In contrast, the beam from a phased array probe can be focused and swept electronically without moving the probe. The beam is controllable because a phased array probe is made up of multiple small elements, each of which can be pulsed individually at a computer-calculated timing. The term phased refers to the timing, and the term array refers to the multiple elements. Phased array ultrasonic testing is based on principles of wave physics, which also have applications in fields such as optics and electromagnetic antennae.
Time-of-flight diffraction (TOFD) method of ultrasonic testing is a sensitive and accurate method for the nondestructive testing of welds for defects. TOFD originated from tip diffraction techniques which were first published by Silk and Liddington in 1975 which paved the way for TOFD. Later works on this technique are given in a number of sources which include Harumi et al. (1989), Avioli et al. (1991), and Bray and Stanley (1997).
Industrial radiography is a modality of non-destructive testing that uses ionizing radiation to inspect materials and components with the objective of locating and quantifying defects and degradation in material properties that would lead to the failure of engineering structures. It plays an important role in the science and technology needed to ensure product quality and reliability. In Australia, industrial radiographic non-destructive testing is colloquially referred to as "bombing" a component with a "bomb".
Rail inspection is the practice of examining rail tracks for flaws that could lead to catastrophic failures. According to the United States Federal Railroad Administration Office of Safety Analysis, track defects are the second leading cause of accidents on railways in the United States. The leading cause of railway accidents is attributed to human error. The contribution of poor management decisions to rail accidents caused by infrequent or inadequate rail inspection is significant but not reported by the FRA, only the NTSB. Every year, North American railroads spend millions of dollars to inspect the rails for internal and external flaws. Nondestructive testing (NDT) methods are used as preventive measures against track failures and possible derailment.
Weld quality assurance is the use of technological methods and actions to test or assure the quality of welds, and secondarily to confirm the presence, location and coverage of welds. In manufacturing, welds are used to join two or more metal surfaces. Because these connections may encounter loads and fatigue during product lifetime, there is a chance they may fail if not created to proper specification.
Alternating current field measurement (ACFM) is an electromagnetic technique for non-destructive testing detection and sizing of surface breaking discontinuities. It was derived from the methods used in eddy-current testing and works on all metals, ferrous or non-ferrous. Since it doesn't require direct electrical contact with the surface it can work through thin coatings such as paint. This practice is intended for use on welds in any metallic material.
Fluorescent penetrant inspection (FPI) is a type of dye penetrant inspection in which a fluorescent dye is applied to the surface of a non-porous material in order to detect defects that may compromise the integrity or quality of the part in question. FPI is noted for its low cost and simple process, and is used widely in a variety of industries.
Hot plate welding, also called heated tool welding, is a thermal welding technique for joining thermoplastics. A heated tool is placed against or near the two surfaces to be joined in order to melt them. Then, the heat source is removed, and the surfaces are brought together under pressure. Hot plate welding has relatively long cycle times, ranging from 10 seconds to minutes, compared to vibration or ultrasonic welding. However, its simplicity and ability to produce strong joints in almost all thermoplastics make it widely used in mass production and for large structures, like large-diameter plastic pipes. Different inspection techniques are implemented in order to identify various discontinuities or cracks.
In metalworking, a welding defect is any flaw that compromises the usefulness of a weldment. There are many different types of welding defects, which are classified according to ISO 6520, while acceptable limits for welds are specified in ISO 5817 and ISO 10042.
Guided wave testing (GWT) is a non-destructive evaluation method. The method employs acoustic waves that propagate along an elongated structure while guided by its boundaries. This allows the waves to travel a long distance with little loss in energy. Nowadays, GWT is widely used to inspect and screen many engineering structures, particularly for the inspection of metallic pipelines around the world. In some cases, hundreds of meters can be inspected from a single location. There are also some applications for inspecting rail tracks, rods and metal plate structures.
Dye-n-Pry, also called Dye And Pry, Dye and Pull, Dye Staining, or Dye Penetrant, is a destructive analysis technique used on surface mount technology (SMT) components to either perform failure analysis or inspect for solder joint integrity. It is an application of dye penetrant inspection.
Welding of advanced thermoplastic composites is a beneficial method of joining these materials compared to mechanical fastening and adhesive bonding. Mechanical fastening requires intense labor, and creates stress concentrations, while adhesive bonding requires extensive surface preparation, and long curing cycles. Welding these materials is a cost-effective method of joining concerning preparation and execution, and these materials retain their properties upon cooling, so no post processing is necessary. These materials are widely used in the aerospace industry to reduce weight of a part while keeping strength.
A variety of non-destructive examination (NDE) techniques are available for inspecting plastic welds. Many of these techniques are similar to the ones used for inspecting metal welds. Traditional techniques include visual testing, radiography, and various ultrasonic techniques. Advanced ultrasonic techniques such as time of flight diffraction (TOFD) and phased-array ultrasonics (PAUT) are being increasingly studied and used for inspecting plastic pipeline welds. Research in the use of optical coherence tomography (OCT) and microwave reflectrometry has also been conducted.
Rebecca "Becky" Hall Sparling, P.E. was an American materials engineer and registered mechanical engineer in the manufacturing, automotive, and aerospace industries from the 1930s to the late 1960s, who had "established a nation-wide reputation as a metallurgist". Often working on classified projects, Sparling advanced the field of metallurgy in severe environments and developed non-destructive engineering test methods, especially in brittle, high-strength, or specialized materials.