Still

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Swan-necked copper pot stills in the Glenfiddich distillery Glenfiddich Distillery stills.jpg
Swan-necked copper pot stills in the Glenfiddich distillery
A still at Mackmyra Whisky Distillery A still at Mackmyra Whisky Distillery.jpg
A still at Mackmyra Whisky Distillery
Column still from Kilbeggan Distillery in County Westmeath in Ireland. Coffey Still.JPG
Column still from Kilbeggan Distillery in County Westmeath in Ireland.

A still is an apparatus used to distill liquid mixtures by heating to selectively boil and then cooling to condense the vapor. [1] A still uses the same concepts as a basic distillation apparatus, but on a much larger scale. Stills have been used to produce perfume and medicine, water for injection (WFI) for pharmaceutical use, generally to separate and purify different chemicals, and to produce distilled beverages containing ethanol.

Contents

Application

Since ethanol boils at a much lower temperature than water, simple distillation can separate ethanol from water by applying heat to the mixture. Historically, a copper vessel was used for this purpose, since copper removes undesirable sulfur-based compounds from the alcohol. However, many modern stills are made of stainless steel pipes with copper linings to prevent erosion of the entire vessel and lower copper levels in the waste product (which in large distilleries is processed to become animal feed). [2] Copper is the preferred material for stills because it yields an overall better-tasting spirit. The taste is improved by the chemical reaction between the copper in the still and the sulfur compounds created by the yeast during fermentation. These unwanted and flavor-changing sulfur compounds are chemically removed from the final product resulting in a smoother, better-tasting drink. All copper stills will require repairs about every eight years due to the precipitation of copper-sulfur compounds. The beverage industry was the first to implement a modern distillation apparatus and led the way in developing equipment standards which are now widely accepted in the chemical industry.

Old Ukrainian vodka still UkrainianVodkaStill.jpg
Old Ukrainian vodka still
Zambian artisanal Kachasu still and cooler Kachasu.jpg
Zambian artisanal Kachasu still and cooler

There is also an increasing usage of the distillation of gin under glass and PTFE, and even at reduced pressures, to facilitate a fresher product. This is irrelevant to alcohol quality because the process starts with triple distilled grain alcohol, and the distillation is used solely to harvest botanical flavors such as limonene and other terpene like compounds. The ethyl alcohol is relatively unchanged.

The simplest standard distillation apparatus is commonly known as a pot still, consisting of a single heated chamber and a vessel to collect purified alcohol. A pot still incorporates only one condensation, whereas other types of distillation equipment have multiple stages which result in higher purification of the more volatile component (alcohol). Pot still distillation gives an incomplete separation, but this can be desirable for the flavor of some distilled beverages.

If a purer distillate is desired, a reflux still is the most common solution. Reflux stills incorporate a fractionating column, commonly created by filling copper vessels with glass beads to maximize available surface area. [3] As alcohol boils, condenses, and reboils through the column, the effective number of distillations greatly increases. Vodka and gin and other neutral grain spirits are distilled by this method, then diluted to concentrations appropriate for human consumption.

Alcoholic products from home distilleries are common throughout the world but are sometimes in violation of local statutes. The product of illegal stills in the United States is commonly referred to as moonshine and in Ireland, poitín. However, poitín, although made illegal in 1661, has been legal for export in Ireland since 1997. Note that the term moonshine itself is often misused as many believe it to be a specific kind of high-proof alcohol that was distilled from corn, but the term can refer to any illicitly distilled alcohol. [4]

See also

Related Research Articles

<span class="mw-page-title-main">Distillation</span> Method of separating mixtures

Distillation, also classical distillation, is the process of separating the component substances of a liquid mixture of two or more chemically discrete substances; the separation process is realized by way of the selective boiling of the mixture and the condensation of the vapors in a still.

<span class="mw-page-title-main">Gin</span> Distilled alcoholic drink flavoured with juniper

Gin is a distilled alcoholic drink flavoured with juniper berries and other botanical ingredients.

<span class="mw-page-title-main">Whisky</span> Distilled alcoholic beverage

Whisky or whiskey is a type of liquor made from fermented grain mash. Various grains are used for different varieties, including barley, corn, rye, and wheat. Whisky is typically aged in wooden casks, which are typically made of charred white oak. Uncharred white oak casks previously used for the aging of port, rum or sherry are also sometimes used.

<span class="mw-page-title-main">Moonshine</span> High-proof distilled spirit, generally produced illicitly

Moonshine is high-proof liquor, traditionally made or distributed illegally. Its clandestine distribution is known as bootlegging. The name was derived from a tradition of distilling the alcohol at night to avoid detection. In the first decades of the 21st century, commercial distilleries have adopted the term for its outlaw cachet and begun producing their own legal "moonshine", including many novelty flavored varieties, that are said to continue the tradition by using a similar method and/or locale of production.

Fractional distillation is the separation of a mixture into its component parts, or fractions. Chemical compounds are separated by heating them to a temperature at which one or more fractions of the mixture will vaporize. It uses distillation to fractionate. Generally the component parts have boiling points that differ by less than 25 °C (45 °F) from each other under a pressure of one atmosphere. If the difference in boiling points is greater than 25 °C, a simple distillation is typically used.

<span class="mw-page-title-main">Pot still</span> Distillation apparatus for flavored liquors

A pot still is a type of distillation apparatus or still used to distill liquors such as whisky or brandy. In modern (post-1850s) practice, they are not used to produce rectified spirit, because they do not separate congeners from ethanol as effectively as other distillation methods. Pot stills operate on a batch distillation basis. Traditionally constructed from copper, pot stills are made in a range of shapes and sizes depending on the quantity and style of spirit desired.

<span class="mw-page-title-main">Column still</span> Apparatus used to distill liquid mixtures consisting of two columns

A column still, also called a continuous still, patent still or Coffey still, is a variety of still consisting of two columns. Column stills can produce rectified spirit.

<span class="mw-page-title-main">Arak (drink)</span> Middle Eastern distilled spirit

Arak or araq, is a distilled Levantine spirit of the anise drinks family. It is translucent and unsweetened.

Fusel alcohols or fuselol, also sometimes called fusel oils in Europe, are mixtures of several higher alcohols produced as a by-product of alcoholic fermentation. The word Fusel is German for "bad liquor".

<span class="mw-page-title-main">Liquor</span> Alcoholic drink produced by distillation

Liquor or distilled beverage is an alcoholic drink produced by the distillation of grains, fruits, vegetables, or sugar that have already gone through alcoholic fermentation. Other terms for liquor include spirit, spirituous liquor or hard liquor. The distillation process concentrates the liquid to increase its alcohol by volume. As liquors contain significantly more alcohol (ethanol) than other alcoholic drinks, they are considered "harder." In North America, the term hard liquor is sometimes used to distinguish distilled alcoholic drinks from non-distilled ones, whereas the term spirits is more commonly used in the UK. Some examples of liquors include vodka, rum, gin, and tequila. Liquors are often aged in barrels, such as for the production of brandy and whiskey, or are infused with flavorings to form flavored liquors, such as absinthe.

Rectified spirit, also known as neutral spirits, rectified alcohol or ethyl alcohol of agricultural origin, is highly concentrated ethanol that has been purified by means of repeated distillation in a process called rectification. In some countries, denatured alcohol or denatured rectified spirit may commonly be available as "rectified spirit", because in some countries the retail sale of rectified alcohol in its non-denatured form is prohibited.

<span class="mw-page-title-main">Continuous distillation</span> Form of distillation

Continuous distillation, a form of distillation, is an ongoing separation in which a mixture is continuously fed into the process and separated fractions are removed continuously as output streams. Distillation is the separation or partial separation of a liquid feed mixture into components or fractions by selective boiling and condensation. The process produces at least two output fractions. These fractions include at least one volatile distillate fraction, which has boiled and been separately captured as a vapor condensed to a liquid, and practically always a bottoms fraction, which is the least volatile residue that has not been separately captured as a condensed vapor.

<span class="mw-page-title-main">Fragrance extraction</span> Separation process of aromatic compounds from raw materials

Fragrance extraction refers to the separation process of aromatic compounds from raw materials, using methods such as distillation, solvent extraction, expression, sieving, or enfleurage. The results of the extracts are either essential oils, absolutes, concretes, or butters, depending on the amount of waxes in the extracted product.

Bathtub gin refers to any style of homemade spirit made in amateur conditions. The term first appeared in 1920, in the prohibition in the United States, in reference to the poor-quality alcohol that was being made.

This glossary of winemaking terms lists some of terms and definitions involved in making wine, fruit wine, and mead.

<span class="mw-page-title-main">Reflux</span> Condensation of vapors and their return to where they originated

Reflux is a technique involving the condensation of vapors and the return of this condensate to the system from which it originated. It is used in industrial and laboratory distillations. It is also used in chemistry to supply energy to reactions over a long period of time.

Brinjevec is a strong alcoholic drink, produced in the Karst and Brkini regions in Slovenia. It is re-distilled from ground and fermented juniper berries only and it differs from similar drinks that have different alcohol bases with added juniper flavor. It has a clear transparent color and it is meant for folk medicinal use and not for regular drinking. It contains between 40% and 50% alcohol and has a very distinctive tart taste

<span class="mw-page-title-main">Downslope Distilling</span>

Downslope Distilling is a craft beverage distillery in Centennial, Colorado, United States.

The Botanist is a dry gin made by the Bruichladdich Distillery in Islay, Scotland. It is one of two gins made on the island and is known for its hand-foraged botanicals. The name of the gin was inspired by two local botanists who helped develop the recipe for the gin alongside former Master Distiller, Jim McEwan. In 2024 it was ranked the seventh-bestselling brand of gin in the world by Drinks International.

References

  1. "DISTILLATION APPARATUS". Plymouth State University. Retrieved 22 March 2014.
  2. "Distillation by-Products as Animal Feeds". Oxford University Press. Retrieved 10 May 2021.
  3. Kister, Henry Z. (1992). Distillation Design (1st ed.). McGraw-Hill. ISBN   0-07-034909-6.
  4. "About Moonshine Stills and Alcohol Stills" . Retrieved 14 November 2014.

Wiktionary-logo-en-v2.svg The dictionary definition of still at Wiktionary