Spinning cone columns are used in a form of low temperature vacuum steam distillation to gently extract volatile chemicals from liquid foodstuffs while minimising the effect on the taste of the product. For instance, the columns can be used to remove some of the alcohol from wine, to remove "off" smells from cream, and to capture aroma compounds that would otherwise be lost in coffee processing.
The columns are made of stainless steel. Conical vanes are attached alternately to the wall of the column and to a central rotating shaft. The product is poured in at the top under vacuum, and steam is pumped into the column from below. [1] The vanes provide a large surface area over which volatile compounds can evaporate into the steam, and the rotation ensures a thin layer of the product is constantly moved over the moving cone. It typically takes 20 seconds for the liquid to move through the column, and industrial columns might process 16–160 litres per minute (960–9,600 L/h; 4.2–42.3 US gal/min; 250–2,540 US gal/h). The temperature and pressure can be adjusted depending on the compounds targeted.
Improvements in viticulture and warmer vintages have led to increasing levels of sugar in wine grapes, which have translated to higher levels of alcohol - which can reach over 15% ABV in Zinfandels from California. Some producers feel that this unbalances their wine, and use spinning cones to reduce the alcohol by 1-2 percentage points. In this case the wine is passed through the column once to distill out the most volatile aroma compounds which are then put to one side while the wine goes through the column a second time at higher temperature to extract alcohol. The aroma compounds are then mixed back into the wine. Some producers such as Joel Peterson of Ravenswood argue that technological "fixes" such as spinning cones remove a sense of terroir from the wine; if the wine has the tannins and other components to balance 15% alcohol, Peterson argues that it should be accepted on its own terms. [2]
The use of spinning cones, and other technologies such as reverse osmosis, was banned in the EU until recently, although for many years they could freely be used in wines imported into the EU from certain New World wine producing countries such as Australia and the USA. [3] In November 2007, the Wine Standards Branch (WSB) of the UK's Food Standards Agency banned the sale of a wine called Sovio, [3] made from Spanish grapes that would normally produce wines of 14% ABV. [4] Sovio runs 40-50% of the wine over spinning cones to reduce the alcohol content to 8%, which means that under EU law it could not be sold as wine as it was below 8.5%; above that, under the rules prevailing at the time, it would be banned because spinning cones could not be used in EU winemaking. [4]
Subsequently, the EU legalized dealcoholization with a 2% adjustment limit in its Code of Winemaking Practices, publishing that in its Commission Regulation (EC) No 606/2009 [5] and stipulating that the dealcoholization must be accomplished by physical separation techniques which would embrace the spinning cone method.
More recently, in International Organisation of Vine and Wine Resolutions OIV-OENO 394A-2012 [6] and OIV-OENO 394B-2012 [7] of June 22, 2012 EU recommended winemaking procedures were modified to permit use of the spinning cone column and membrane techniques such as reverse osmosis on wine, subject to a 20% limitation on the adjustment. That limitation is currently under review following the proposal by some EU members that it be eliminated altogether. The limitation is applicable only to products formally labeled as "wine".
Distillation, also classical distillation, is the process of separating the component substances of a liquid mixture of two or more chemically discrete substances; the separation process is realized by way of the selective boiling of the mixture and the condensation of the vapors in a still.
Gin is a distilled alcoholic drink flavoured with juniper berries and other botanical ingredients.
Low-alcohol beer is beer with little or no alcohol by volume that aims to reproduce the taste of beer while eliminating or reducing the inebriating effect, carbohydrates, and calories of regular alcoholic brews. Low-alcohol beers can come in different beer styles such as lagers, stouts, and ales. Low-alcohol beer is also known as light beer, non-alcoholic beer, small beer, small ale, or near-beer.
Whisky or whiskey is a type of liquor made from fermented grain mash. Various grains are used for different varieties, including barley, corn, rye, and wheat. Whisky is typically aged in wooden casks, which are typically made of charred white oak. Uncharred white oak casks previously used for the aging of port, rum or sherry are also sometimes used.
Brandy is a liquor produced by distilling wine. Brandy generally contains 35–60% alcohol by volume and is typically consumed as an after-dinner digestif. Some brandies are aged in wooden casks. Others are coloured with caramel colouring to imitate the effect of ageing, and some are produced using a combination of ageing and colouring. Varieties of wine brandy can be found across the winemaking world. Among the most renowned are Cognac and Armagnac from south-western France.
Fractional distillation is the separation of a mixture into its component parts, or fractions. Chemical compounds are separated by heating them to a temperature at which one or more fractions of the mixture will vaporize. It uses distillation to fractionate. Generally the component parts have boiling points that differ by less than 25 °C (45 °F) from each other under a pressure of one atmosphere. If the difference in boiling points is greater than 25 °C, a simple distillation is typically used.
A fractionating column or fractional column is equipment used in the distillation of liquid mixtures to separate the mixture into its component parts, or fractions, based on their differences in volatility. Fractionating columns are used in small-scale laboratory distillations as well as large-scale industrial distillations.
Winemaking, wine-making, or vinification is the production of wine, starting with the selection of the fruit, its fermentation into alcohol, and the bottling of the finished liquid. The history of wine-making stretches over millennia. There is evidence that suggests that the earliest wine production took place in Georgia and Iran around 6000 to 5000 B.C. The science of wine and winemaking is known as oenology. A winemaker may also be called a vintner. The growing of grapes is viticulture and there are many varieties of grapes.
Vacuum distillation or distillation under reduced pressure is a type of distillation performed under reduced pressure, which allows the purification of compounds not readily distilled at ambient pressures or simply to save time or energy. This technique separates compounds based on differences in their boiling points. This technique is used when the boiling point of the desired compound is difficult to achieve or will cause the compound to decompose. Reduced pressures decrease the boiling point of compounds. The reduction in boiling point can be calculated using a temperature-pressure nomograph using the Clausius–Clapeyron relation.
Aguardente (Portuguese) or aguardiente (Spanish) is a type of distilled alcoholic spirit that contains between 29% and 60% alcohol by volume (ABV). It is a somewhat generic term that can refer to liquors made from various foods. It originates from and is typically consumed on the Iberian Peninsula and in Iberian America.
Liquor or distilled beverages are alcoholic drinks produced by the distillation of grains, fruits, vegetables, or sugar that have already gone through alcoholic fermentation. Other terms for liquor include spirit, spirituous liquor or hard liquor. While the word liquor ordinarily refers to distilled alcoholic spirits rather than beverages produced by fermentation alone, it can sometimes be used more broadly to refer to any alcoholic beverage.
Rectified spirit, also known as neutral spirits, rectified alcohol or ethyl alcohol of agricultural origin, is highly concentrated ethanol that has been purified by means of repeated distillation in a process called rectification. In some countries, denatured alcohol or denatured rectified spirit may commonly be available as "rectified spirit", because in some countries the retail sale of rectified alcohol in its non-denatured form is prohibited.
Fragrance extraction refers to the separation process of aromatic compounds from raw materials, using methods such as distillation, solvent extraction, expression, sieving, or enfleurage. The results of the extracts are either essential oils, absolutes, concretes, or butters, depending on the amount of waxes in the extracted product.
An evaporator is a type of heat exchanger device that facilitates evaporation by utilizing conductive and convective heat transfer, which provides the necessary thermal energy for phase transition from liquid to vapour. Within evaporators, a circulating liquid is exposed to an atmospheric or reduced pressure environment causing it to boil at a lower temperature compared to normal atmospheric boiling.
European Union wine regulations are common legislation related to wine existing within the European Union (EU), the member states of which account for almost two-thirds of the world's wine production. These regulations form a part of the Common Agricultural Policy (CAP) of EU, and regulate such things as the maximum vineyard surface allowed to individual EU member states, allowed winemaking practices and principles for wine classification and labelling. The wine regulations exist to regulate total production in order to combat overproduction of wine and to provide an underpinning to Protected designations of origin (PDOs), among other things. In a sense, the wine regulations therefore try to protect both the producer and the consumer.
The aromas of wine are more diverse than its flavours. The human tongue is limited to the primary tastes perceived by taste receptors on the tongue – sourness, bitterness, saltiness, sweetness and savouriness. The wide array of fruit, earthy, leathery, floral, herbal, mineral, and woodsy flavour present in wine are derived from aroma notes sensed by the olfactory bulb. In wine tasting, wine is sometimes smelled before taking a sip in order to identify some components of the wine that may be present. Different terms are used to describe what is being smelled. The most basic term is aroma which generally refers to a "pleasant" smell as opposed to odour which refers to an unpleasant smell or possible wine fault. The term aroma may be further distinguished from bouquet which generally refers to the smells that arise from the chemical reactions of fermentation and aging of the wine.
This glossary of winemaking terms lists some of terms and definitions involved in making wine, fruit wine, and mead.
In viticulture, ripeness is the completion of the ripening process of wine grapes on the vine which signals the beginning of harvest. What exactly constitutes ripeness will vary depending on what style of wine is being produced and what the winemaker and viticulturist personally believe constitutes ripeness. Once the grapes are harvested, the physical and chemical components of the grape which will influence a wine's quality are essentially set so determining the optimal moment of ripeness for harvest may be considered the most crucial decision in winemaking.
Wine is a complex mixture of chemical compounds in a hydro-alcoholic solution with a pH around 4. The chemistry of wine and its resultant quality depend on achieving a balance between three aspects of the berries used to make the wine: their sugar content, acidity and the presence of secondary compounds. Vines store sugar in grapes through photosynthesis, and acids break down as grapes ripen. Secondary compounds are also stored in the course of the season. Anthocyanins give grapes a red color and protection against ultraviolet light. Tannins add bitterness and astringency which acts to defend vines against pests and grazing animals.
The role of yeast in winemaking is the most important element that distinguishes wine from fruit juice. In the absence of oxygen, yeast converts the sugars of the fruit into alcohol and carbon dioxide through the process of fermentation. The more sugars in the grapes, the higher the potential alcohol level of the wine if the yeast are allowed to carry out fermentation to dryness. Sometimes winemakers will stop fermentation early in order to leave some residual sugars and sweetness in the wine such as with dessert wines. This can be achieved by dropping fermentation temperatures to the point where the yeast are inactive, sterile filtering the wine to remove the yeast or fortification with brandy or neutral spirits to kill off the yeast cells. If fermentation is unintentionally stopped, such as when the yeasts become exhausted of available nutrients and the wine has not yet reached dryness, this is considered a stuck fermentation.
The Flavourtech Spinning Cone Column is a stripping column in which steam separates volatile compounds from liquids or slurries under vacuum.