Vacuum chamber

Last updated March 20, 2024

A vacuum chamber is a rigid enclosure from which air and other gases are removed by a vacuum pump. This results in a low-pressure environment within the chamber, commonly referred to as a vacuum. A vacuum environment allows researchers to conduct physical experiments or to test mechanical devices which must operate in outer space (for example) or for processes such as vacuum drying or vacuum coating. Chambers are typically made of metals which may or may not shield applied external magnetic fields depending on wall thickness, frequency, resistivity, and permeability of the material used. Only some materials are suitable for vacuum use.

Chambers often have multiple ports, covered with vacuum flanges, to allow instruments or windows to be installed in the walls of the chamber. In low to medium-vacuum applications, these are sealed with elastomer o-rings. In higher vacuum applications, the flanges have knife edges machined onto them, which cut into a copper gasket when the flange is bolted on.

A type of vacuum chamber frequently used in the field of spacecraft engineering is a thermal vacuum chamber, which provides a thermal environment representing what a spacecraft would experience in space.

Vacuum chamber materials

Vacuum chambers can be constructed of many materials. "Metals are arguably the most prevalent vacuum chamber materials."^[1] The strength, pressure, and permeability are considerations for selecting chamber material. Common materials are:

Stainless Steel
Aluminum
Mild Steel
Brass
High density ceramic
Glass
Acrylic
Hardened steel

Vacuum degassing

"Vacuum is the process of using vacuum to remove gases from compounds which become entrapped in the mixture when mixing the components."^[2] To assure a bubble-free mold when mixing resin and silicone rubbers and slower-setting harder resins, a vacuum chamber is required. A small vacuum chamber is needed for de-airing (eliminating air bubbles) for materials prior to their setting. The process is fairly straightforward. The casting or molding material is mixed according to the manufacturers directions.

Process

Since the material may expand 4–5 times under a vacuum, the mixing container must be large enough to hold a volume of four to five times the amount of the original material that is being vacuumed to allow for the expansion; if not, it will spill over the top of the container requiring clean-up that can be avoided. The material container is then placed into the vacuum chamber; a vacuum pump is connected and turned on. Once the vacuum reaches 29 inches (at sea level) of mercury, the material will begin to rise (resembling foam). When the material falls, it will plateau and stop rising. The vacuuming is continued for another 2 to 3 minutes to make certain all of the air has been removed from the material. Once this interval is reached, the vacuum pump is shut off and the vacuum chamber release valve is opened to equalize air pressure. The vacuum chamber is opened, the material is removed and is ready to pour into the mold.

Though a maximum vacuum one can theoretically achieve at sea level is 29.921 inches of mercury (Hg,) this will vary significantly as altitude increases. For example, in Denver, Colorado, at one mile (1.6 km) above sea level, it is only possible to achieve a vacuum on the mercury scale of 24.896 Hg.

To keep the material air-free, it must be slowly poured in a high and narrow stream starting from the corner of the mold box, or mold, letting the material flow freely into the box or mold cavity. Usually, this method will not introduce any new bubbles into the vacuumed material. To ensure that the material is totally devoid of air bubbles, the entire mold/mold box may be placed in the chamber for an additional few minutes; this will assist the material in flowing into difficult areas of the mold/mold box.

Vacuum drying

Water and other liquids may accumulate on a product during the production process. "Vacuum is often employed as a process for removing bulk and absorbed water (or other solvents) from a product. Combined with heat, vacuum can be an effective method for drying."^[3]^[4]

World's largest vacuum chamber

NASA's Space Power Facility houses the world's largest vacuum chamber. It was built in 1969 and stands 122 feet (37 m) high and 100 feet (30 m) in diameter, enclosing a bullet-shaped space. It was originally commissioned for nuclear-electric power studies under vacuum conditions, but was later decommissioned. Recently, it was recommissioned for use in testing spacecraft propulsion systems. Recent uses include testing the airbag landing systems for the Mars Pathfinder and the Mars Exploration Rovers, Spirit and Opportunity, under simulated Mars atmospheric conditions.

Each arm of the LIGO detectors in Livingston, Louisiana, and Hanford, Washington, is a vacuum chamber 4 kilometres (2.5 mi) long, making them the longest vacuum chambers in the world.

Related Research Articles

A vacuum pump is a type of pump device that draws gas particles from a sealed volume in order to leave behind a partial vacuum. The first vacuum pump was invented in 1650 by Otto von Guericke, and was preceded by the suction pump, which dates to antiquity.

A vacuum is space devoid of matter. The word is derived from the Latin adjective vacuus meaning "vacant" or "void". An approximation to such vacuum is a region with a gaseous pressure much less than atmospheric pressure. Physicists often discuss ideal test results that would occur in a perfect vacuum, which they sometimes simply call "vacuum" or free space, and use the term partial vacuum to refer to an actual imperfect vacuum as one might have in a laboratory or in space. In engineering and applied physics on the other hand, vacuum refers to any space in which the pressure is considerably lower than atmospheric pressure. The Latin term in vacuo is used to describe an object that is surrounded by a vacuum.

<span class="mw-page-title-main">Silicone</span> Family of polymers of the repeating form [R2Si–O–SiR2]

In organosilicon and polymer chemistry, a silicone or polysiloxane is a polymer composed of repeating units of siloxane. They are typically colorless oils or rubber-like substances. Silicones are used in sealants, adhesives, lubricants, medicine, cooking utensils, thermal insulation, and electrical insulation. Some common forms include silicone oil, grease, rubber, resin, and caulk.

Fiberglass or fibreglass is a common type of fiber-reinforced plastic using glass fiber. The fibers may be randomly arranged, flattened into a sheet called a chopped strand mat, or woven into glass cloth. The plastic matrix may be a thermoset polymer matrix—most often based on thermosetting polymers such as epoxy, polyester resin, or vinyl ester resin—or a thermoplastic.

<span class="mw-page-title-main">Liquid nitrogen</span> Liquid state of nitrogen

Liquid nitrogen—LN₂—is nitrogen in a liquid state at low temperature. Liquid nitrogen has a boiling point of about −196 °C (−321 °F; 77 K). It is produced industrially by fractional distillation of liquid air. It is a colorless, mobile liquid whose viscosity is about one tenth that of acetone (i.e. roughly one thirtieth that of room temperature water). Liquid nitrogen is widely used as a coolant.

A getter is a deposit of reactive material that is placed inside a vacuum system to complete and maintain the vacuum. When gas molecules strike the getter material, they combine with it chemically or by absorption. Thus the getter removes small amounts of gas from the evacuated space. The getter is usually a coating applied to a surface within the evacuated chamber.

<span class="mw-page-title-main">Sand casting</span> Metal casting process using sand as the mold material

Sand casting, also known as sand molded casting, is a metal casting process characterized by using sand — known as casting sand — as the mold material. The term "sand casting" can also refer to an object produced via the sand casting process. Sand castings are produced in specialized factories called foundries. In 2003, over 60% of all metal castings were produced via sand casting.

Ultra-high vacuum is the vacuum regime characterised by pressures lower than about 1×10⁻⁶ pascals. UHV conditions are created by pumping the gas out of a UHV chamber. At these low pressures the mean free path of a gas molecule is greater than approximately 40 km, so the gas is in free molecular flow, and gas molecules will collide with the chamber walls many times before colliding with each other. Almost all molecular interactions therefore take place on various surfaces in the chamber.

A hermetic seal is any type of sealing that makes a given object airtight. The term originally applied to airtight glass containers, but as technology advanced it applied to a larger category of materials, including rubber and plastics. Hermetic seals are essential to the correct and safe functionality of many electronic and healthcare products. Used technically, it is stated in conjunction with a specific test method and conditions of use. Colloquially, the exact requirements of such a seal varies with the application.

Vacuum casting is a casting process for elastomers using a vacuum to draw the liquid material into the mold. This process is used when air entrapment is a problem, there are intricate details or undercuts, or if the material is fiber or wire reinforced.

Rotational molding involves a heated mold which is filled with a charge or shot weight of the material. It is then slowly rotated, causing the softened material to disperse and stick to the walls of the mold forming a hollow part. In order to form an even thickness throughout the part, the mold rotates at all times during the heating phase, and then continues to rotate during the cooling phase to avoid sagging or deformation. The process was applied to plastics in the 1950s but in the early years was little used because it was a slow process restricted to a small number of plastics. Over time, improvements in process control and developments with plastic powders have resulted in increased use.

Vacuum engineering is the field of engineering that deals with the practical use of vacuum in industrial and scientific applications. Vacuum may improve the productivity and performance of processes otherwise carried out at normal air pressure, or may make possible processes that could not be done in the presence of air. Vacuum engineering techniques are widely applied in materials processing such as drying or filtering, chemical processing, application of metal coatings to objects, manufacture of electron devices and incandescent lamps, and in scientific research.

A vacuum flange is a flange at the end of a tube used to connect vacuum chambers, tubing and vacuum pumps to each other. Vacuum flanges are used for scientific and industrial applications to allow various pieces of equipment to interact via physical connections and for vacuum maintenance, monitoring, and manipulation from outside a vacuum's chamber. Several flange standards exist with differences in ultimate attainable pressure, size, and ease of attachment.

Vacuum packing is a method of packaging that removes air from the package prior to sealing. This method involves placing items in a plastic film package, removing air from inside and sealing the package. Shrink film is sometimes used to have a tight fit to the contents. The intent of vacuum packing is usually to remove oxygen from the container to extend the shelf life of foods and, with flexible package forms, to reduce the volume of the contents and package.

A resin dispensing system is a technical installation to process casting resin for the purpose of filling, sealing, covering or soaking technical parts, especially in the field of electricity and electronics like transformers, LCDs and other devices of various size.

Resin casting is a method of plastic casting where a mold is filled with a liquid synthetic resin, which then hardens. It is primarily used for small-scale production like industrial prototypes and dentistry. It can be done by amateur hobbyists with little initial investment, and is used in the production of collectible toys, models and figures, as well as small-scale jewellery production.

RTV silicone is a type of silicone rubber that cures at room temperature. It is available as a one-component product, or mixed from two components. Manufacturers provide it in a range of hardnesses from very soft to medium—usually from 15 to 40 Shore A. RTV silicones can be cured with a catalyst consisting of either platinum or a tin compound such as dibutyltin dilaurate. Applications include low-temperature over-molding, making molds for reproducing, and lens applications for some optically clear grades. It is also used widely in the automotive industry as an adhesive and sealant, for example to create gaskets in-place.

Out of autoclave composite manufacturing is an alternative to the traditional high pressure autoclave (industrial) curing process commonly used by the aerospace manufacturers for manufacturing composite material. Out of autoclave (OOA) is a process that achieves the same quality as an autoclave but through a different process. OOA curing achieves the desired fiber content and elimination of voids by placing the layup within a closed mold and applying vacuum, pressure, and heat by means other than an autoclave. An RTM press is the typical method of applying heat and pressure to the closed mold. There are several out of autoclave technologies in current use including resin transfer molding (RTM), Same Qualified Resin Transfer Molding (SQRTM), vacuum-assisted resin transfer molding (VARTM), and balanced pressure fluid molding. The most advanced of these processes can produce high-tech net shape aircraft components.

Flower preservation has existed since early history, although deliberate flower preservation is a more recent phenomenon. In the Middle East, the bones of pre-historic man were discovered with delicate wild flowers probably as a tribute to a passing loved one. Evidence of deliberate use of specific flowers is indicated by the pollen grains that were present. Brightly colored and vivid flowers were also found in Egyptian tombs. These flowers were approximated to be 4,000 years old. In the sixteenth century medicinal nosegays began to give way to ornamental ones. Flowers essentially started to be used for decorative purposes such as jewels, fans and gloves. During the Elizabethan Age the once familiar ruff was replaced by soft lacy collars, and bosom flowers also became popular.

Vacuum Assisted Resin Transfer Molding (VARTM) or Vacuum Injected Molding (VIM) is a closed mold, out of autoclave (OOA) composite manufacturing process. VARTM is a variation of Resin Transfer Molding (RTM) with its distinguishing characteristic being the replacement of the top portion of a mold tool with a vacuum bag and the use of a vacuum to assist in resin flow. The process involves the use of a vacuum to facilitate resin flow into a fiber layup contained within a mold tool covered by a vacuum bag. After the impregnation occurs the composite part is allowed to cure at room temperature with an optional post cure sometimes carried out.

References

↑ Danielson, PHil. "Choosing the Right Vacuum Materials" (PDF). The Vacuum Lab. Archived from the original (PDF) on July 24, 2012. Retrieved February 10, 2012.
↑ "Vacuum Degassing Epoxy & Silicone" (PDF). LACO Technologies, Inc. Retrieved February 10, 2012.
↑ "Vacuum Drying" (PDF). LACO Technologies, Inc. Retrieved February 10, 2012.
↑ Danielson, Phil. "Desorbing Water in Vacuum Systems: Bakeout or UV?" (PDF). The Vacuum Lab. Archived from the original (PDF) on May 16, 2011. Retrieved February 10, 2012.

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[1] Danielson, PHil. "Choosing the Right Vacuum Materials" (PDF). The Vacuum Lab. Archived from the original (PDF) on July 24, 2012. Retrieved February 10, 2012.

[2] "Vacuum Degassing Epoxy & Silicone" (PDF). LACO Technologies, Inc. Retrieved February 10, 2012.

[3] "Vacuum Drying" (PDF). LACO Technologies, Inc. Retrieved February 10, 2012.

[4] Danielson, Phil. "Desorbing Water in Vacuum Systems: Bakeout or UV?" (PDF). The Vacuum Lab. Archived from the original (PDF) on May 16, 2011. Retrieved February 10, 2012.

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