Terahertz nondestructive evaluation

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Terahertz nondestructive evaluation pertains to devices, and techniques of analysis occurring in the terahertz domain of electromagnetic radiation. These devices and techniques evaluate the properties of a material, component or system without causing damage. [1]

Contents

Terahertz imaging

XRay, Optical, and THz image of a packaged IC. XRay-Optical-THz-IC.gif
XRay, Optical, and THz image of a packaged IC.

Terahertz imaging is an emerging and significant nondestructive evaluation (NDE) technique used for dielectric (nonconducting, i.e., an insulator) materials analysis and quality control in the pharmaceutical, biomedical, security, materials characterization, and aerospace industries. [3] [4] It has proved to be effective in the inspection of layers in paints and coatings, [5] detecting structural defects in ceramic and composite materials [6] and imaging the physical structure of paintings [7] and manuscripts. [8] [9] The use of THz waves for non-destructive evaluation enables inspection of multi-layered structures and can identify abnormalities from foreign material inclusions, disbond and delamination, mechanical impact damage, heat damage, and water or hydraulic fluid ingression. [10] This new method can play a significant role in a number of industries for materials characterization applications where precision thickness mapping (to assure product dimensional tolerances within a product and from product-to-product) and density mapping (to assure product quality within a product and from product-to-product) are required. [11]

Nondestructive evaluation

Sensors and instruments are employed in the 0.1 to the 10 THz range for nondestructive evaluation, which includes detection. [11] [12]

Terahertz Density Thickness Imager

The Terahertz Density Thickness Imager is a nondestructive inspection method that employs terahertz energy for density and thickness mapping in dielectric, ceramic, and composite materials. This non-contact, single-sided terahertz electromagnetic measurement and imaging method characterizes micro-structure and thickness variation in dielectric (insulating) materials. This method was demonstrated for the Space Shuttle external tank sprayed-on foam insulation and has been designed for use as an inspection method for current and future NASA thermal protection systems and other dielectric material inspection applications where no contact can be made with the sample due to fragility and it is impractical to use ultrasonic methods. [11]

Rotational spectroscopy

Rotational spectroscopy uses electromagnetic radiation in the frequency range from 0.1 to 4 terahertz (THz). This range includes millimeter-range wavelengths and is particularly sensitive to chemical molecules. The resulting THz absorption produces a unique and reproducible spectral pattern that identifies the material. THz spectroscopy can detect trace amounts of explosives in less than one second. Because explosives continually emit trace amounts of vapor, it should be possible to use these methods to detect concealed explosives from a distance. [12]

THz-wave radar

THz-wave radar can sense gas leaks, chemicals and nuclear materials. In field tests, THz-wave radar detected chemicals at the 10-ppm level from 60 meters away. This method can be used in a fence line or aircraft mounted system that works day or night in any weather. It can locate and track chemical and radioactive plumes. THz-wave radar that can sense radioactive plumes from nuclear plants have detected plumes several kilometers away based on radiation-induced ionization effects in air. [12]

THz tomography

THz tomography techniques are nondestructive methods that can use THz pulsed beam or millimeter-range sources to locate objects in 3D. [13] These techniques include tomography, tomosynthesis, synthetic aperture radar and time of flight. Such techniques can resolve details on scales of less than one millimeter in objects that are several tens of centimeters in size.

Passive/active imaging techniques

Security imaging is currently being done by both active and passive methods. Active systems illuminate the subject with THz radiation whereas passive systems merely view the naturally occurring radiation from the subject.

Evidently passive systems are inherently safe, whereas an argument can be made that any form of "irradiation" of a person is undesirable. In technical and scientific terms, however, the active illumination schemes are safe according to all current legislation and standards.

The purpose of using active illumination sources is primarily to make the signal-to-noise ratio better. This is analogous to using a flash on a standard optical light camera when the ambient lighting level is too low.

For security imaging purposes the operating frequencies are typically in the range 0.1 THz to 0.8 THz (100 GHz to 800 GHz). In this range skin is not transparent so the imaging systems can look through clothing and hair, but not inside the body. There are privacy issues associated with such activities, especially surrounding the active systems since the active systems, with their higher quality images, can show very detailed anatomical features.

Active systems such as the L3 Provision and the Smiths eqo are actually mm-wave imaging systems rather than Terahertz imaging systems like Millitech systems. These widely deployed systems do not display images, avoiding any privacy issues. Instead they display generic "mannequin" outlines with any anomalous regions highlighted.

Since security screening is looking for anomalous images, items like false legs, false arms, colostomy bags, body-worn urinals, body-worn insulin pumps, and external breast augmentations will show up. Note that breast implants, being under the skin, will not be revealed.

Active imaging techniques can be used to perform medical imaging. Because THz radiation is biologically safe (non ionisant), it can be used in high resolution imaging to detect skin cancer. [12]

Space Shuttle inspections

NASA Space Shuttle inspections are an example of this technology's application.

After the Shuttle Columbia accident in 2003, Columbia Accident Investigation Board recommendation R3.2.1 stated “Initiate an aggressive program to eliminate all External Tank Thermal Protection System debris-shedding at the source….” To support this recommendation, inspection methods for flaws in foam are being evaluated, developed, and refined at NASA. [1] [11] [12]

STS-114 employed Space Shuttle Discovery, and was the first "Return to Flight" Space Shuttle mission following the Space Shuttle Columbia disaster. It launched at 10:39 EDT, 26 July 2005. During the STS-114 flight significant foam shedding was observed. Therefore, the ability to nondestructively detect and characterize crushed foam after that flight became a significant priority when it was believed that the staff processing the tank had crushed foam by walking on it or from hail damage when the shuttle was on the launch pad or during other preparations for launch.

Additionally, density variations in the foam were also potential points of flaw initiation causing foam shedding. The innovation described below answered the call to develop a nondestructive, totally non-contact, non-liquid-coupled method that could simultaneously and precisely characterize thickness variation (from crushed foam due to worker handling and hail damage) and density variation in foam materials. It was critical to have a method that did not require fluid (water) coupling; i.e.; ultrasonic testing methods require water coupling.

There are millions of dollars of ultrasonic equipment in the field and on the market that are used as thickness gauges and density meters. When terahertz nondestructive evaluation is fully commercialized into a more portable form, and becomes less expensive it will be able to replace the ultrasonic instruments for structural plastic, ceramic, and foam materials. The new instruments will not require liquid coupling thereby enhancing their usefulness in field applications and possibly for high-temperature in-situ applications where liquid coupling is not possible. A potential new market segment can be developed with this technology. [11] [12]

See also

Related Research Articles

<span class="mw-page-title-main">Ultrasound</span> Sound waves with frequencies above the human hearing range

Ultrasound is sound with frequencies greater than 20 kilohertz. This frequency is the approximate upper audible limit of human hearing in healthy young adults. The physical principles of acoustic waves apply to any frequency range, including ultrasound. Ultrasonic devices operate with frequencies from 20 kHz up to several gigahertz.

<span class="mw-page-title-main">Nondestructive testing</span> Evaluating the properties of a material, component, or system without causing damage

Nondestructive testing (NDT) is any of a wide group of analysis techniques used in science and technology industry to evaluate the properties of a material, component or system without causing damage. The terms nondestructive examination (NDE), nondestructive inspection (NDI), and nondestructive evaluation (NDE) are also commonly used to describe this technology. Because NDT does not permanently alter the article being inspected, it is a highly valuable technique that can save both money and time in product evaluation, troubleshooting, and research. The six most frequently used NDT methods are eddy-current, magnetic-particle, liquid penetrant, radiographic, ultrasonic, and visual testing. NDT is commonly used in forensic engineering, mechanical engineering, petroleum engineering, electrical engineering, civil engineering, systems engineering, aeronautical engineering, medicine, and art. Innovations in the field of nondestructive testing have had a profound impact on medical imaging, including on echocardiography, medical ultrasonography, and digital radiography.

<span class="mw-page-title-main">Terahertz radiation</span> Range 300-3000 GHz of the electromagnetic spectrum

Terahertz radiation – also known as submillimeter radiation, terahertz waves, tremendously high frequency (THF), T-rays, T-waves, T-light, T-lux or THz – consists of electromagnetic waves within the ITU-designated band of frequencies from 0.3 to 3 terahertz (THz), although the upper boundary is somewhat arbitrary and is considered by some sources as 30 THz. One terahertz is 1012 Hz or 1000 GHz. Wavelengths of radiation in the terahertz band correspondingly range from 1 mm to 0.1 mm = 100 µm. Because terahertz radiation begins at a wavelength of around 1 millimeter and proceeds into shorter wavelengths, it is sometimes known as the submillimeter band, and its radiation as submillimeter waves, especially in astronomy. This band of electromagnetic radiation lies within the transition region between microwave and far infrared, and can be regarded as either.

<span class="mw-page-title-main">Plastic welding</span> Welding of semi-finished plastic materials

Plastic welding is welding for semi-finished plastic materials, and is described in ISO 472 as a process of uniting softened surfaces of materials, generally with the aid of heat. Welding of thermoplastics is accomplished in three sequential stages, namely surface preparation, application of heat and pressure, and cooling. Numerous welding methods have been developed for the joining of semi-finished plastic materials. Based on the mechanism of heat generation at the welding interface, welding methods for thermoplastics can be classified as external and internal heating methods, as shown in Fig 1.

<span class="mw-page-title-main">Terahertz time-domain spectroscopy</span>

In physics, terahertz time-domain spectroscopy (THz-TDS) is a spectroscopic technique in which the properties of matter are probed with short pulses of terahertz radiation. The generation and detection scheme is sensitive to the sample's effect on both the amplitude and the phase of the terahertz radiation.

Laser-ultrasonics uses lasers to generate and detect ultrasonic waves. It is a non-contact technique used to measure materials thickness, detect flaws and carry out materials characterization. The basic components of a laser-ultrasonic system are a generation laser, a detection laser and a detector.

<span class="mw-page-title-main">Acoustic emission</span>

Acoustic emission (AE) is the phenomenon of radiation of acoustic (elastic) waves in solids that occurs when a material undergoes irreversible changes in its internal structure, for example as a result of crack formation or plastic deformation due to aging, temperature gradients, or external mechanical forces.

<span class="mw-page-title-main">Ultrasonic testing</span> Non-destructive material testing using ultrasonic waves

Ultrasonic testing (UT) is a family of non-destructive testing techniques based on the propagation of ultrasonic waves in the object or material tested. In most common UT applications, very short ultrasonic pulse waves with centre frequencies ranging from 0.1-15 MHz and occasionally up to 50 MHz, are transmitted into materials to detect internal flaws or to characterize materials. A common example is ultrasonic thickness measurement, which tests the thickness of the test object, for example, to monitor pipework corrosion and erosion. Ultrasonic testing is extensively used to detect flaws in welds.

<span class="mw-page-title-main">Characterization (materials science)</span> Study of material structure and properties

Characterization, when used in materials science, refers to the broad and general process by which a material's structure and properties are probed and measured. It is a fundamental process in the field of materials science, without which no scientific understanding of engineering materials could be ascertained. The scope of the term often differs; some definitions limit the term's use to techniques which study the microscopic structure and properties of materials, while others use the term to refer to any materials analysis process including macroscopic techniques such as mechanical testing, thermal analysis and density calculation. The scale of the structures observed in materials characterization ranges from angstroms, such as in the imaging of individual atoms and chemical bonds, up to centimeters, such as in the imaging of coarse grain structures in metals.

<span class="mw-page-title-main">Phased array ultrasonics</span> Testing method

Phased array ultrasonics (PA) is an advanced method of ultrasonic testing that has applications in medical imaging and industrial nondestructive testing. Common applications are to noninvasively examine the heart or to find flaws in manufactured materials such as welds. Single-element probes, known technically as monolithic probes, emit a beam in a fixed direction. To test or interrogate a large volume of material, a conventional probe must be physically scanned to sweep the beam through the area of interest. In contrast, the beam from a phased array probe can be focused and swept electronically without moving the probe. The beam is controllable because a phased array probe is made up of multiple small elements, each of which can be pulsed individually at a computer-calculated timing. The term phased refers to the timing, and the term array refers to the multiple elements. Phased array ultrasonic testing is based on principles of wave physics, which also have applications in fields such as optics and electromagnetic antennae.

Terahertz tomography is a class of tomography where sectional imaging is done by terahertz radiation. Terahertz radiation is electromagnetic radiation with a frequency between 0.1 and 10 THz; it falls between radio waves and light waves on the spectrum; it encompasses portions of the millimeter waves and infrared wavelengths. Because of its high frequency and short wavelength, terahertz wave has a high signal-to-noise ratio in the time domain spectrum. Tomography using terahertz radiation can image samples that are opaque in the visible and near-infrared regions of the spectrum. Terahertz wave three-dimensional (3D) imaging technology has developed rapidly since its first successful application in 1997, and a series of new 3D imaging technologies have been proposed successively.

<span class="mw-page-title-main">Electromagnetic acoustic transducer</span>

Electromagnetic acoustic transducer (EMAT) is a transducer for non-contact acoustic wave generation and reception in conducting materials. Its effect is based on electromagnetic mechanisms, which do not need direct coupling with the surface of the material. Due to this couplant-free feature, EMATs are particularly useful in harsh, i.e., hot, cold, clean, or dry environments. EMATs are suitable to generate all kinds of waves in metallic and/or magnetostrictive materials. Depending on the design and orientation of coils and magnets, shear horizontal (SH) bulk wave mode, surface wave, plate waves such as SH and Lamb waves, and all sorts of other bulk and guided-wave modes can be excited. After decades of research and development, EMAT has found its applications in many industries such as primary metal manufacturing and processing, automotive, railroad, pipeline, boiler and pressure vessel industries, in which they are typically used for nondestructive testing (NDT) of metallic structures.

Thermographic inspection refers to the nondestructive testing (NDT) of parts, materials or systems through the imaging of the temperature fields, gradients and/or patterns ("thermograms") at the object's surface. It is distinguished from medical thermography by the subjects being examined: thermographic inspection generally examines inanimate objects, while medical thermography generally examines living organisms. Generally, thermographic inspection is performed using an infrared sensor.

<span class="mw-page-title-main">Terahertz metamaterial</span>

A terahertz metamaterial is a class of composite metamaterials designed to interact at terahertz (THz) frequencies. The terahertz frequency range used in materials research is usually defined as 0.1 to 10 THz.

<span class="mw-page-title-main">TeraView</span>

TeraView Limited, or TeraView, is a company that designs terahertz imaging and spectroscopy instruments and equipment for measurement and evaluation of pharmaceutical tablets, nanomaterials, ceramics and composites, integrated circuit chips and more.

Terahertz spectroscopy detects and controls properties of matter with electromagnetic fields that are in the frequency range between a few hundred gigahertz and several terahertz. In many-body systems, several of the relevant states have an energy difference that matches with the energy of a THz photon. Therefore, THz spectroscopy provides a particularly powerful method in resolving and controlling individual transitions between different many-body states. By doing this, one gains new insights about many-body quantum kinetics and how that can be utilized in developing new technologies that are optimized up to the elementary quantum level.

Reflectometry is a general term for the use of the reflection of waves or pulses at surfaces and interfaces to detect or characterize objects, sometimes to detect anomalies as in fault detection and medical diagnosis.

Microwave imaging is a science which has been evolved from older detecting/locating techniques in order to evaluate hidden or embedded objects in a structure using electromagnetic (EM) waves in microwave regime. Engineering and application oriented microwave imaging for non-destructive testing is called microwave testing, see below.

Active thermography is an advanced nondestructive testing procedure, which uses a thermography measurement of a tested material thermal response after its external excitation. This principle can be used also for non-contact infrared non-destructive testing (IRNDT) of materials.

A variety of non-destructive examination (NDE) techniques are available for inspecting plastic welds. Many of these techniques are similar to the ones used for inspecting metal welds. Traditional techniques include visual testing, radiography, and various ultrasonic techniques. Advanced ultrasonic techniques such as time of flight diffraction (TOFD) and phased-array ultrasonics (PAUT) are being increasingly studied and used for inspecting plastic pipeline welds. Research in the use of optical coherence tomography (OCT) and microwave reflectrometry has also been conducted.

References

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Further reading