In optical mineralogy and petrography, a thin section (or petrographic thin section) is a thin slice of a rock or mineral sample, prepared in a laboratory, for use with a polarizing petrographic microscope, electron microscope and electron microprobe. A thin sliver of rock is cut from the sample with a diamond saw and ground optically flat. It is then mounted on a glass slide and then ground smooth using progressively finer abrasive grit until the sample is only 30 μm thick. The method uses the Michel-Lévy interference colour chart to determine thickness, typically using quartz as the thickness gauge because it is one of the most abundant minerals.
When placed between two polarizing filters set at right angles to each other, the optical properties of the minerals in the thin section alter the colour and intensity of the light as seen by the viewer. As different minerals have different optical properties, most rock forming minerals can be easily identified. Plagioclase for example can be seen in the photo on the right as a clear mineral with multiple parallel twinning planes. The large blue-green minerals are clinopyroxene with some exsolution of orthopyroxene.
Thin sections are prepared in order to investigate the optical properties of the minerals in the rock. This work is a part of petrology and helps to reveal the origin and evolution of the parent rock.
A photograph of a rock in thin section is often referred to as a photomicrograph.
Thin sections are also used in the microscopic study of bones, metals and ceramics.
In thin section, when viewed in plane polarized light (PPL), quartz is colorless with low relief and no cleavage. Its habit is either fairly equant or anhedral if it infills around other minerals as a cement. Under cross polarized light (XPL) quartz displays low interference colors and is usually the defining mineral used to determine if the thin section is at standardized thickness of 30 microns as quartz will only display up to a very pale yellow interference color and no further at that thickness, and it is very common in most rocks so it will likely be available to judge the thickness. [1]
In thin section, quartz grain provenance in a sedimentary rock can be estimated. In crossed polarized light, the quartz grain can go extinct all at once, called monocrystalline quartz, or in waves, called polycrystalline quartz. The extinction in waves is called undulose extinction and indicates dislocation walls in mineral grains. Dislocation walls are where dislocations, intracrystalline deformation via movement of a dislocation front within a plane, organize themselves into planes of sufficient quantity. They change the crystallographic orientation across the walls, so for example in quartz, the two sides of the wall will have slightly different extinction angles and thus result in undulose extinction. [2] Since undulose extinction requires dislocation walls to have developed, and these occur more easily at higher pressures and temperatures, quartz grains with undulose extinction indicate metamorphic rock provenance for that grain. Those grains that are monocrystalline quartz are more likely to have been formed by igneous processes. Differing sources suggest the extent to which this proxy for provenance can be used. Some note the trend for immature sandstones to have less polycrystalline quartz grains compared to mature sandstones, which have grains that have passed through many sedimentary cycles. [3] Quartz grains derived from previous sedimentary sources are determined by looking for authigenic, or grown in place, overgrowths of silica cement over the grain. [4]
The above descriptions of quartz in thin section are usually enough to identify it. Minerals with similar appearance may include plagioclase, although it can be distinguished by the distinctive twinning in crossed-polarized light and cleavage in plane-polarized light, and cordierite, although it can be distinguished by twinning or inclusions in the grain. However, for certainty, other distinguishing features of quartz include the fact that it is uniaxial, it has a positive optic sign, length-slow sign of elongation, and zero degree extinction angle. [5]
Fine-grained rocks, particularly those containing minerals of high birefringence, such as calcite, are sometimes prepared as ultra-thin sections. An ordinary 30 μm thin section is prepared as described above but the slice of rock is attached to the glass slide using a soluble cement such as Canada balsam (soluble in ethanol) to allow both sides to be worked on. The section is then polished on both sides using a fine diamond paste until it has a thickness in the range of 2–12 μm. This technique has been used to study the microstructure of fine-grained carbonates such as the Lochseitenkalk mylonite in which the matrix grains are less than 5 μm in size. [6] This method is also sometimes used in the preparation of mineral and rock specimens for transmission electron microscopy and allows greater accuracy in comparing features using both optical and electron imaging. [7]
Biotite is a common group of phyllosilicate minerals within the mica group, with the approximate chemical formula K(Mg,Fe)3AlSi3O10(F,OH)2. It is primarily a solid-solution series between the iron-endmember annite, and the magnesium-endmember phlogopite; more aluminous end-members include siderophyllite and eastonite. Biotite was regarded as a mineral species by the International Mineralogical Association until 1998, when its status was changed to a mineral group. The term biotite is still used to describe unanalysed dark micas in the field. Biotite was named by J.F.L. Hausmann in 1847 in honor of the French physicist Jean-Baptiste Biot, who performed early research into the many optical properties of mica.
Sandstone is a clastic sedimentary rock composed mainly of sand-sized silicate grains. Sandstones comprise about 20–25% of all sedimentary rocks.
Schist is a medium-grained metamorphic rock showing pronounced schistosity. This means that the rock is composed of mineral grains easily seen with a low-power hand lens, oriented in such a way that the rock is easily split into thin flakes or plates. This texture reflects a high content of platy minerals, such as mica, talc, chlorite, or graphite. These are often interleaved with more granular minerals, such as feldspar or quartz.
Sedimentary rocks are types of rock that are formed by the accumulation or deposition of mineral or organic particles at Earth's surface, followed by cementation. Sedimentation is the collective name for processes that cause these particles to settle in place. The particles that form a sedimentary rock are called sediment, and may be composed of geological detritus (minerals) or biological detritus. The geological detritus originated from weathering and erosion of existing rocks, or from the solidification of molten lava blobs erupted by volcanoes. The geological detritus is transported to the place of deposition by water, wind, ice or mass movement, which are called agents of denudation. Biological detritus was formed by bodies and parts of dead aquatic organisms, as well as their fecal mass, suspended in water and slowly piling up on the floor of water bodies. Sedimentation may also occur as dissolved minerals precipitate from water solution.
Metamorphic rocks arise from the transformation of existing rock to new types of rock in a process called metamorphism. The original rock (protolith) is subjected to temperatures greater than 150 to 200 °C and, often, elevated pressure of 100 megapascals (1,000 bar) or more, causing profound physical or chemical changes. During this process, the rock remains mostly in the solid state, but gradually recrystallizes to a new texture or mineral composition. The protolith may be an igneous, sedimentary, or existing metamorphic rock.
Amphibolite is a metamorphic rock that contains amphibole, especially hornblende and actinolite, as well as plagioclase feldspar, but with little or no quartz. It is typically dark-colored and dense, with a weakly foliated or schistose (flaky) structure. The small flakes of black and white in the rock often give it a salt-and-pepper appearance.
Petrology is the branch of geology that studies rocks and the conditions under which they form. Petrology has three subdivisions: igneous, metamorphic, and sedimentary petrology. Igneous and metamorphic petrology are commonly taught together because both make heavy use of chemistry, chemical methods, and phase diagrams. Sedimentary petrology is commonly taught together with stratigraphy because it deals with the processes that form sedimentary rock. Modern sedimentary petrology is making increasing use of chemistry.
The lithology of a rock unit is a description of its physical characteristics visible at outcrop, in hand or core samples, or with low magnification microscopy. Physical characteristics include colour, texture, grain size, and composition. Lithology may refer to either a detailed description of these characteristics, or a summary of the gross physical character of a rock. Examples of lithologies in the second sense include sandstone, slate, basalt, or limestone.
Petrography is a branch of petrology that focuses on detailed descriptions of rocks. Someone who studies petrography is called a petrographer. The mineral content and the textural relationships within the rock are described in detail. The classification of rocks is based on the information acquired during the petrographic analysis. Petrographic descriptions start with the field notes at the outcrop and include macroscopic description of hand-sized specimens. The most important petrographer's tool is the petrographic microscope. The detailed analysis of minerals by optical mineralogy in thin section and the micro-texture and structure are critical to understanding the origin of the rock.
Hornfels is the group name for a set of contact metamorphic rocks that have been baked and hardened by the heat of intrusive igneous masses and have been rendered massive, hard, splintery, and in some cases exceedingly tough and durable. These properties are caused by fine grained non-aligned crystals with platy or prismatic habits, characteristic of metamorphism at high temperature but without accompanying deformation. The term is derived from the German word Hornfels, meaning "hornstone", because of its exceptional toughness and texture both reminiscent of animal horns. These rocks were referred to by miners in northern England as whetstones.
Undulose extinction or undulatory extinction is a geological term referring to the type of extinction that occurs in certain minerals when examined in thin section under cross polarized light. As the microscope stage is rotated, individual mineral grains appear black when the polarization due to the mineral prevents any light from passing through. If a mineral is deformed plastically by dislocation processes without recovery, strain builds up within the crystal lattice causing it to warp. This means that different parts of a crystal reach extinction at slightly different angles, giving the crystal an irregular, mottled look.
Foliation in geology refers to repetitive layering in metamorphic rocks. Each layer can be as thin as a sheet of paper, or over a meter in thickness. The word comes from the Latin folium, meaning "leaf", and refers to the sheet-like planar structure. It is caused by shearing forces, or differential pressure. The layers form parallel to the direction of the shear, or perpendicular to the direction of higher pressure. Nonfoliated metamorphic rocks are typically formed in the absence of significant differential pressure or shear. Foliation is common in rocks affected by the regional metamorphic compression typical of areas of mountain belt formation.
Optical mineralogy is the study of minerals and rocks by measuring their optical properties. Most commonly, rock and mineral samples are prepared as thin sections or grain mounts for study in the laboratory with a petrographic microscope. Optical mineralogy is used to identify the mineralogical composition of geological materials in order to help reveal their origin and evolution.
In geology, texture or rock microstructure refers to the relationship between the materials of which a rock is composed. The broadest textural classes are crystalline, fragmental, aphanitic, and glassy. The geometric aspects and relations amongst the component particles or crystals are referred to as the crystallographic texture or preferred orientation. Textures can be quantified in many ways. The most common parameter is the crystal size distribution. This creates the physical appearance or character of a rock, such as grain size, shape, arrangement, and other properties, at both the visible and microscopic scale.
Stylolites are serrated surfaces within a rock mass at which mineral material has been removed by pressure dissolution, in a deformation process that decreases the total volume of rock. Minerals which are insoluble in water, such as clays, pyrite and oxides, as well as insoluble organic matter, remain within the stylolites and make them visible. Sometimes host rocks contain no insoluble minerals, in which case stylolites can be recognized by change in texture of the rock. They occur most commonly in homogeneous rocks, carbonates, cherts, sandstones, but they can be found in certain igneous rocks and ice. Their size vary from microscopic contacts between two grains (microstylolites) to large structures up to 20 m in length and up to 10 m in amplitude in ice. Stylolites usually form parallel to bedding, because of overburden pressure, but they can be oblique or even perpendicular to bedding, as a result of tectonic activity.
A petrographic microscope is a type of optical microscope used to identify rocks and minerals in thin sections. The microscope is used in optical mineralogy and petrography, a branch of petrology which focuses on detailed descriptions of rocks. The method includes aspects of polarized light microscopy (PLM).
A metamorphic facies is a set of mineral assemblages in metamorphic rocks formed under similar pressures and temperatures. The assemblage is typical of what is formed in conditions corresponding to an area on the two dimensional graph of temperature vs. pressure. Rocks which contain certain minerals can therefore be linked to certain tectonic settings, times and places in the geological history of the area. The boundaries between facies are wide because they are gradational and approximate. The area on the graph corresponding to rock formation at the lowest values of temperature and pressure is the range of formation of sedimentary rocks, as opposed to metamorphic rocks, in a process called diagenesis.
Quartz is the most abundant single mineral in the Earth's crust, and as such is present in a very large proportion of rocks both as primary crystals and as detrital grains in sedimentary and metamorphic rocks. Dynamic recrystallization is a process of crystal regrowth under conditions of stress and elevated temperature, commonly applied in the fields of metallurgy and materials science. Dynamic quartz recrystallization happens in a relatively predictable way with relation to temperature, and given its abundance quartz recrystallization can be used to easily determine relative temperature profiles, for example in orogenic belts or near intrusions.
S-type granites are a category of granites first proposed in 2001. They are recognized by a specific set of mineralogical, geochemical, textural, and isotopic characteristics. S-type granites are over-saturated in aluminium, with an ASI index greater than 1.1 where ASI = Al2O3 / (CaO + Na2O +K2O) in mol percent; petrographic features are representative of the chemical composition of the initial magma as originally put forth by Chappell and White are summarized in their table 1.
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