Olive oil regulation and adulteration

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International Olive Council building Consejo oleicola DSCF0508.JPG
International Olive Council building

Olive oil regulation and adulteration are complex issues overseen and studied by various governmental bodies, non-governmental organizations, and private researchers across the world. The most frequent type of adulteration is that oil of lower quality is mixed into olive oil.

Contents

Background of regulation

The EU regulates the use of different protected designation of origin labels for olive oils.[ citation needed ]

The International Olive Council (IOC) is an intergovernmental organization with 16 member states plus the European Union based in Madrid, Spain. It promotes olive oil around the world by tracking production, defining quality standards, and monitoring authenticity. More than 98 percent of the world's olives are grown in IOC member nations. [1]

The IOC officially governs 95 per cent of international production and holds great influence over the rest. IOC terminology is precise, but it can lead to confusion between the words that describe production and the words used on retail labels. Olive oil is classified by how it was produced, by its chemistry, and by its flavor. All production begins by transforming the olive fruit into olive paste. This paste is then malaxed to allow the microscopic oil droplets to concentrate. The oil is extracted by means of pressure (traditional method) or centrifugation (modern method). After extraction the remnant solid substance, called pomace, still contains a small quantity of oil.[ citation needed ]

United States

The United States is not a member of the IOC, and the US Department of Agriculture does not legally recognize its classifications, such as extra-virgin olive oil. In October 2011, the United States adopted new olive oil standards, revising those that had been in place since 1948, which affected importers and domestic growers and producers by ensuring conformity with the benchmarks commonly accepted in the U.S. and abroad. [2]

As of 1998, US Customs regulations on "country of origin" have stated that if a non-origin nation is shown on the label, then the real origin must be shown on the same side of the label and in comparable size letters so as not to mislead the consumer. [3] [4] Yet most major US brands continue to put "imported from Italy" on the front label in large letters and other origins on the back in very small print. These products are a mixture of olive oil from more than one nation and it is not clear what percentage of the olive oil is really of Italian origin. This practice makes it difficult for high quality, lower cost producers outside of Italy to enter the US market, and for genuine Italian producers to compete.[ citation needed ]

In the United States, the Food & Drug Administration (FDA) does not routinely test imported olive oil for adulteration.[ citation needed ]

Testing for purity

UV-Vis spectroscopy analysis of olive oil samples in an Italian laboratory Valentina Domenici 2015.jpg
UV-Vis spectroscopy analysis of olive oil samples in an Italian laboratory

The detection of olive oil adulteration is often complicated with no single test that can accomplish the task. A battery of tests is employed to determine olive oil authenticity and identity of the adulterant. Included in this testing regime is the determination of free acidity, peroxide value, Ultraviolet light extinction, fatty acid composition, sterol composition, triglyceride composition, wax content, steroidal hydrocarbons, and the Bellier test. [5] Methods employing chromatography/mass spectrometry and spectroscopy are also used to detect adulteration of olive oil [6] [7] [8]

Test results are measured against the International Olive Council trade standard to identify abnormalities. Each test provides key information which allows a decision to be made with respect to the grade of olive oil and the identity of any adulterants. However, the International Olive Council does not test for deodorisation which makes up the bulk of fake extra-virgin oils. Soft column deodorisation is the process where steam is forced through a tank of inferior oil which removes all taste, colour and nutrients, colouring is then added before the tank is topped up with real extra-virgin oil to add flavour. [9]

A test published in 1887 described the detection of olive oil adulterated with mineral oil by a simple titration of the carboxylic acid moieties present in natural vegetable oils. The procedure involved boiling 10 milliliters of olive oil with 40 milliliters of approximately 1 molar potassium hydroxide in 95% ethanol, adding water to 100 grams to dissolve the saponified lipids, and titrating against a normal sulfuric acid solution using phenolphthalein as a pH indicator dye. The base stock solution was titrated to neutralize an equal quantity of the acid, so without the presence of vegetable oil it would require 40 milliliters of acid to cause a color change, but in the pure oils tested (almond, benne, cottonseed, cod liver oil, linseed oil, and olive oil, only 6 milliliters were required. In accordance with this, olive oil adulterated with 10% mineral oil required 8 milliliters, and with 20% 11 milliliters. The adulterated oil tested in 1887 required 14 to 17 milliliters to neutralize, so it might have been 30–40% mineral oil. [10]

DNA analysis methods, based on the use of polymerase chain reaction (PCR) (e.g. DNA fingerprinting), have also been used. These techniques require extensive sample preparation, which needs specific optimization to ensure extraction of sufficient DNA, and that PCR inhibitors are not affecting the analysis. To date, there is no DNA extraction method applicable to any sample. [11]

In 2014, an “invisible oil tag” using artificial, sub-micrometer-sized DNA barcodes was suggested by researchers from ETH Zurich. The barcodes consist of magnetically recoverable silica particles containing synthetic DNA sequences, which are added to the oil in a very small amount (down to 1 ppb) and can be retrieved at any time for authenticity test by PCR/sequencing. The advantages of this method, compared to conventional techniques are its low-cost, minimal sample preparation and minute volumes, and its universalness, since it can be applied to any oil type/sample. [12] [13] [14]

Industry certifications of quality

As of 2015, the North American Olive Oil Association offered a Quality Seal Program to guarantee authenticity of olive oil. Members of the association agreed to have their oils tested twice a year to ensure the oil meets or exceeds the International Olive Council (IOC) standards. The testing includes both sensory (taste/smell) and chemical tests for purity. Samples are purchased from the retail marketplace to ensure that the products tested are the same as the ones purchased by consumers. The test samples are not selected and submitted by olive oil producers. Brands pay for the testing through a yearly licensing fee. [15]

The California Olive Oil Council tests samples of olive oil submitted by producers for extra virgin quality. The samples are provided by the producers. The testing is primarily sensory with some chemical tests. [16]

The Extra Virgin Alliance offers the EVA Mark of quality and authenticity. The EVA standard includes both sensory and chemical parameters for olive oils at their Best Before Date.[ citation needed ]

Simple home tests

Refrigeration

There is a persistent mistaken belief that when genuine olive oil (or, in some versions, extra virgin olive oil specifically) is refrigerated, it will solidify or become much more viscous. This mistaken belief is based on the fact that olive oil is composed mainly of the monounsaturated fat oleic acid, and pure oleic acid (triolein) has a melting point of 5 ˚C, which is slightly above the high end of proper refrigerator temperature. Thus, if olive oil were pure triolein, it would solidify in a properly set refrigerator. However, olive oil is a complex mixture with significant variability in its fatty acid structure, and can be anywhere from 55% to 83% oleic acid, [17] [18] with the remainder a mixture of polyunsaturated fat and saturated fat, as well as containing waxes, phytosterols, and other compounds that affect its melting temperature. Thus, in practice, many olive oils have significantly lower melting temperatures. [19] [20] [21] In fact, one might expect a refined seed oil with very high oleic acid content (such as high oleic sunflower oil) to be more likely to solidify in the refrigerator, based on their fatty acid composition and lack of minor compounds. [19]

The "fridge test" for adulteration was evaluated by scientists at the Olive Center at the University of California, Davis. Researchers put seven samples of different oils into a refrigerator at 4.7 ˚C, including a premium extra-virgin olive oil; low-quality extra-virgin olive oil; a blend of virgin and refined olive oil; refined canola oil; refined safflower oil; a 50:50 mixture of the premium extra virgin olive oil with the blended olive oil; and a 50:50 mixture of the premium extra virgin olive oil with the refined safflower oil. Several days of refrigeration was required before congealing of any of the samples became apparent. Although none of the samples solidified fully, the three which contained either 100% extra virgin olive oil or a 50:50 mix of extra virgin and blended olive oil had partially solidified after a week, whereas the other samples remained clear. The authors conclude that refrigeration is not reliable in detecting olive oil adulteration. However, based on these results, the absence or any visible congealing after a week of refrigeration would not be an encouraging sign if the olive oil had been sold as pure extra virgin. [22]

Ignition

Pure olive oil should burn in an oil lamp. The ignition test however, like the refrigerator test, is not conclusive. [23]

Investigations, incidents, and recalls

As of 2021, the most frequent type of adulteration of olive oil is that oil of lower quality is mixed into it. [24] Adulterated oil is usually no more serious than passing off inferior, but safe, products as superior olive oil, however in 1981 almost 700 people died, it is believed, as a consequence of consuming rapeseed (canola) oil adulterated with aniline intended for use as an industrial lubricant, but sold as olive oil in Spain (see toxic oil syndrome). [25]

In 1993, the FDA ordered a recall of Rubino U.S.A. Inc., (Cincinnati, Ohio) olive oils which were nothing more than canola oil. [26]

In 1997, the Canadian Food Inspection Agency began conducting tests on 100 oils claimed to be 100% olive oil and in 1999 the CFIA concluded that 20 per cent of the oils were fake. [27]

In 2007, NPR reported that with Italian extra-virgin olive oil in high demand with concomitant high prices, adulterated olive oil had become the biggest source of agricultural fraud problems in the European Union. [28] Some oil labeled "extra-virgin" is diluted with cheaper olive oils or other vegetable oils. In some cases, lampante, or "lamp oil," which is made from spoiled olives fallen from trees, is used, even though it can't legally be sold as food. One fraud ring was accused of coloring low-grade soy oil and canola oil with industrial chlorophyll, and flavoring it with beta-carotene. [28]

In August 2007, the The New Yorker stated that major Italian shippers routinely adulterate olive oil and that only about 40% of olive oil sold as "extra virgin" actually meets the specification. [29] In some cases, colza oil with added color and flavor has been labeled and sold as olive oil. [30] This extensive fraud prompted the Italian government to mandate a new labeling law in 2007 for companies selling olive oil, under which every bottle of Italian olive oil would have to declare the farm and press on which it was produced, as well as display a precise breakdown of the oils used, for blended oils. [31] In February 2008, however, EU officials took issue with the new law, stating that under EU rules such labeling should be voluntary rather than compulsory. [32] Under EU rules, olive oil may be sold as Italian even if it only contains a small amount of Italian oil. [31]

In March 2008, 400 Italian police officers conducted "Operation Golden Oil", arresting 23 people and confiscating 85 farms after an investigation revealed a large-scale scheme to relabel oils from other Mediterranean nations as Italian. [33] In April 2008, another operation impounded seven olive oil plants and arrested 40 people in nine provinces of northern and southern Italy for adding chlorophyll to sunflower and soybean oil and selling it as extra virgin olive oil, both in Italy and abroad. 25,000 liters of the fake oil were seized and prevented from being exported. [34]

In December 2008, the Guardia Civil in La Rioja (Spain) warned about the possible sale of adulterated olive oil in the area. This warning came after 550 litres of oil was found in a large container labelled "Astispumante 1510" in Rincón de Soto and after the theft of 1,750 litres of oil was reported in the area on December 18, 2008. [35]

In the first week of March 2010, researchers at the University of California at Davis' Olive Center purchased three bottles each of 14 imported olive oils and five California oils at retail stores in three different regions of California (Sacramento County, San Francisco Bay Area and Los Angeles County). All of the oils were labeled "extra-virgin olive oil." Samples were shipped to the Australian Oils Research Laboratory in Wagga Wagga, and were analyzed by their laboratory (which is recognized by the IOC to provide chemical analysis of olive oil) and tested by their sensory panel (which is recognized by the IOC as qualified to perform olive oil sensory analysis). Duplicate testing was performed at the UC Davis olive oil research project laboratories. Sixty-nine percent of the imported olive oils and 10% of the California oils failed to meet the IOC/USDA taste standards for extra-virgin olive oil. Samples that failed had a median of up to 3.5 IOC-standardized sensory defects (such as rancid, fusty, and musty). The standard IOC/USDA chemical tests only identified 31% of the failed oils as defective, primarily by exceeding the IOC/USDA limit for ultraviolet absorbance of late oxidation products (K232 and K268); two more recently introduced German chemical tests (now incorporated into the Australian extra-virgin standard) were each more than twice as effective at detection of defective oils. [36] A subsequent round of testing in 2011 found similar results. [37] The UC Davis report was contested by the North American Olive Oil Association on the grounds that UC Davis has a conflict of interest due to the fact that they market their own olive oil and have an interest in promoting olive oil from California. The IOC stated that the study contained "[an] evident undercurrent of aggressive, inexplicable criticism of imported olive oil quality". [38]

In March 2011, the Florence, Italy, prosecutor’s office, working in conjunction with the forestry department, indicted two managers and an officer of Carapelli, one of the brands of the Spanish company Grupo SOS (which recently changed its name to Deoleo) and Pietro Coricelli. The charges involved falsified documents and food fraud. Carapelli lawyer Neri Pinucci said the company was not worried about the charges and that "the case is based on an irregularity in the documents". [39] However, in June 2017 the Italian Antitrust Authority (Autorità Garante della Concorrenza e del Mercato), found them guilty of unfair business practices regarding their olive oil brands and imposed fines on them and the discount supermarket chain Lidl, amounting to nearly €1 million.

In 2012, The Advertiser wrote that while only less than 10% of world olive oil production met the criteria for labeling as extra-virgin, it had been estimated that up to 50% of retail oil is labeled "extra-virgin". [9] Tests by the Australian Olive Association (AOA) in 2012 showed that every imported brand of extra-virgin olive oil fell below the standard that would be required for AOA certification. The AOA has been campaigning to have the Australian Competition & Consumer Commission force supermarkets to adhere to the code. Standards Australia has adopted a code of practice for the testing of olive oils; however, while allowing oils to be certified as being genuine extra-virgin, the code regarding labeling is voluntary. [9]

In 2013, "Figures released at the [IOC's] Workshop on Olive Oil Authentication, held in Madrid June 10–11, showed that one in four olive oils sampled in Spain, and nearly one in three in Canada, failed recent official fraud tests." [40]

In June 2017, the Olive Oil Times published, that according to independent testing, oil from the brands Bertolli, Carapelli, Coricelli, Primadonna, and Sasso labelled as "extra virgin" was in fact only "virgin". [41]

In December 2023, it was reported that the Spanish Civil Guard and the Italian Carabinieri together with Europol had arrested 11 people, who adulterated more than 260,000 liters, or roughly 68,000 gallons, of olive oil with lampante oil in Tuscany, Sicily and Ciudad Real in November. [42] See Olive oil raids of 2023 in Europe for more.

See also

Related Research Articles

<span class="mw-page-title-main">Olive oil</span> Liquid fat made from olives

Olive oil is a liquid fat obtained by pressing whole olives, the fruit of Olea europaea, a traditional tree crop of the Mediterranean Basin, and extracting the oil.

<span class="mw-page-title-main">Oleic acid</span> Monounsaturated omega-9 fatty acid

Oleic acid is a fatty acid that occurs naturally in various animal and vegetable fats and oils. It is an odorless, colorless oil, although commercial samples may be yellowish. In chemical terms, oleic acid is classified as a monounsaturated omega-9 fatty acid, abbreviated with a lipid number of 18:1 cis-9, and a main product of Δ9-desaturase. It has the formula CH3−(CH2)7−CH=CH−(CH2)7−COOH. The name derives from the Latin word oleum, which means oil. It is the most common fatty acid in nature. The salts and esters of oleic acid are called oleates. It is a common component of oils, and thus occurs in many types of food, as well as in soap.

<span class="mw-page-title-main">Mustard oil</span> Oil derived from mustard plants

Mustard oil can mean either the pressed oil used for cooking, or a pungent essential oil also known as volatile oil of mustard. The essential oil results from grinding mustard seed, mixing the grounds with water, and isolating the resulting volatile oil by distillation. It can also be produced by dry distillation of the seed. Pressed mustard oil is used as cooking oil in some cultures, but sale is restricted in some countries due to high levels of erucic acid. Varieties of mustard seed also exist that are low in erucic acid.

<span class="mw-page-title-main">Saponification value</span> Milligrams of a base required to saponify 1g of fat

Saponification value or saponification number represents the number of milligrams of potassium hydroxide (KOH) or sodium hydroxide (NaOH) required to saponify one gram of fat under the conditions specified. It is a measure of the average molecular weight of all the fatty acids present in the sample in form of triglycerides. The higher the saponification value, the lower the fatty acids average length, the lighter the mean molecular weight of triglycerides and vice versa. Practically, fats or oils with high saponification value are more suitable for soap making.

The smoke point, also referred to as the burning point, is the temperature at which an oil or fat begins to produce a continuous bluish smoke that becomes clearly visible, dependent upon specific and defined conditions. Smoke point values can vary greatly, depending on factors such as the volume of oil utilized, the size of the container, the presence of air currents, the type and source of light as well as the quality of the oil and its acidity content, otherwise known as free fatty acid (FFA) content. The more FFA an oil contains, the quicker it will break down and start smoking. The lower the value of FFA, the higher the smoke point. However, the FFA content typically represents less than 1% of the total oil and consequently renders smoke point a poor indicator of the capacity of a fat or oil to withstand heat.

<span class="mw-page-title-main">Sunflower oil</span> Oil pressed from the seed of Helianthus annuus

Sunflower oil is the non-volatile oil pressed from the seeds of the sunflower. Sunflower oil is commonly used in food as a frying oil, and in cosmetic formulations as an emollient.

<span class="mw-page-title-main">Carapelli</span>

Carapelli is an Italian food company, currently owned by Deoleo, S.A, based in Tavarnelle Val di Pesa, which is a small town in the Metropolitan City of Florence, most famous for its extra virgin olive oil. The company was started as a home business in 1893 by Cesira and Costantino Carapelli. Other members of the Carapelli family joined the business and the company rapidly grew in size and popularity, to become the most modernised food company in Italy by the 1940s. Today, Carapelli Firenze SpA is the leading Italian extra virgin olive oil company where 30% of its production is exported to Europe and the Americas.

<span class="mw-page-title-main">Avocado oil</span> Edible oil pressed from the pulp of avocados

Avocado oil is an edible oil extracted from the pulp of avocados, the fruit of Persea americana. It is used as an edible oil both raw and for cooking, where it is noted for its high smoke point. It is also used for lubrication and in cosmetics.

<span class="mw-page-title-main">Bertolli</span> Brand of Italian food products

Bertolli is a brand of Italian food products produced by multiple companies around the world with the trademark owned by Mizkan Holdings. Originating as a brand of extra-virgin olive oil, in which it was the global market leader, pasta sauces and ready meals are now sold under the brand name as well.

Filippo Berio is a brand of olive oils exported from Italy and made of oil from Italy, Greece, Spain and Tunisia. The brand is used for virgin, extra-virgin and 'mild and light' oils, as well as wine vinegar, balsamic vinegar, pesto and olives.

Aprutino pescarese PDO is a Protected Designation of Origin (PDO) olive oil, produced in the province of Pescara, in the regions of Abruzzo. It is among the first group of Italian extra virgin olive oils to gain the PDO.

Sabina is a Protected Designation of Origin (PDO) that applies to the extra virgin olive oil produced in the Sabina region. This area approximately covers the territory originally occupied by the ancient Sabines tribe in the Province of Rome and the Province of Rieti. It is considered to be the first Italian PDO to gain the status, later being followed by Aprutino Pescarese, Brisighella, Collina di Brindisi and Canino.

<i>Extra Virginity</i> 2011 nonfiction book

Extra Virginity: The Sublime and Scandalous World of Olive Oil is a 2011 nonfiction book by American author Tom Mueller about olive oil. The book describes the history of olive oil, including its religious, economic, and culinary uses, as well as the current state of the olive oil industry. Extra Virginity asserts that the global olive oil industry is rife with corruption and fraud due to lax governmental regulations, but it also presents stories of individuals, including growers and government officials, who seek to curb such practices and promote genuine extra virgin olive oil. The book also includes an appendix with advice to consumers for choosing good oil. Extra Virginity expands upon "Slippery Business", an article Mueller wrote for The New Yorker in 2007 which described the state of the Italian olive oil industry.

<span class="mw-page-title-main">International Olive Council</span> Intergovernmental organization

The International Olive Council (IOC) is an intergovernmental organization of states that produce olives or products derived from olives, such as olive oil.

The Olive Oil Commission of California (OOCC) was founded in 2014 by California olive oil farmers. It is an entity of the State of California which was established as a result of a bill introduced by Lois Wolk. The primary goal is to improve the sales of olive oil grown in California.

<span class="mw-page-title-main">North American Olive Oil Association</span>

The North American Olive Oil Association (NAOOA) is a trade association of producers, packagers and importers of olive oil. The organization was established in 1989.

<span class="mw-page-title-main">Cooking oil</span> Oil consumed by humans, of vegetable or animal origin

Cooking oil is a plant or animal liquid fat used in frying, baking, and other types of cooking. Oil allows higher cooking temperatures than water, making cooking faster and more flavorful, while likewise distributing heat, reducing burning and uneven cooking. It sometimes imparts its own flavor. Cooking oil is also used in food preparation and flavoring not involving heat, such as salad dressings and bread dips.

<span class="mw-page-title-main">Olive oil acidity</span>

Olive oil contains small amounts of free fatty acids. Free acidity is an important parameter that defines the quality of olive oil. It is usually expressed as a percentage of oleic acid in the oil. As defined by the European Commission regulation No. 2568/91 and subsequent amendments, the highest quality olive oil must feature a free acidity lower than 0.8%. Virgin olive oil is characterized by acidity between 0.8% and 2%, while lampante olive oil features a free acidity higher than 2%. The increase of free acidity in olive oil is due to free fatty acids that are released from triglycerides.

Deoleo, S.A. is a Spanish multinational olive oil processing company. It is the world's largest bottler selling brands such as Bertolli, Carapelli, Carbonell, and Koipe. In India, it sells olive oil under brand name Figaro.

<span class="mw-page-title-main">Olive oil raids of 2023 in Europe</span>

The Olive oil raids of 2023 in Europe refers to a coordinated law enforcement effort named Operation OPSON by Spanish, Italian police and Europol to combat a significant food fraud operation involving the production and sale of counterfeit extra virgin olive oil. This operation, uncovered by officials, involved the production of over 260,000 liters of olive oil falsely labeled as high-quality and extra virgin but deemed "unfit for consumption" by the experts.

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