Oxalate phosphite

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The oxalate phosphites are chemical compounds containing oxalate and phosphite anions. They are also called oxalatophosphites or phosphite oxalates. Oxalate phosphates can form metal organic framework compounds.

Related compounds include the nitrite oxalates, arsenite oxalates, [1] [2] phosphate oxalates and oxalatophosphonates.

The oxalate ion is rectangular and planar. The phosphite ion is shaped as a triangular pyramid. Because of high charge and stiff shape they will bridge across more than one cation, in particular those hard cations with a higher charge such as +3. Hydrogen can convert some of the oxygen on the anions to OH and reduce the charge. Many oxalate phosphite compounds have microporous structures where amines direct the structure formation. [3]

List

namechemmwcrystal systemspace groupunit cell Åvolumedensitycommentreferences
peha = pentaethylenehexamine[(H6peha)0.17(H2O)1.5][Al2(HPO3)2(C2O4)(HCOO)]+formate [4]
(H13C5NOH)0.5(H2C13H14N2)0.25[Al2(HPO3)2(C2O4)(OH)(H2O)]0.5H2O [4]
Li2(VOHPO3)2C2O4•6H2OtriclinicP1a=6.3592, b=8.0789, c=9.1692, α=64.390°, β=87.277°, γ=67.624° [5]
Li2(VOHPO3)2C2O4•4H2OmonoclinicP21/aa=6.3555 b=12.6368 c=9.0242 β=105.167° [5]
Li2(VO)2(HPO3)2C2O4 [6]
diammonium (μ-oxalato)-bis(μ-phosphonato)-dioxo-di-vanadium hydrate(NH4)2(VOHPO3)2C2O4 2·9H2OtriclinicP1a = 6.3844, b = 7.2278, c = 9.2965, α = 67.260°, β = 72.927°, γ = 85.848° [7]
(μ6-Oxalato)-bis(μ4-hydrogen phosphonato)-bis(μ2-aqua)-bis(μ2-oxo)-di-sodium-di-vanadiumNa2(VO)2(HPO3)2C2O4463.87triclinicP1a 6.3255 b 6.7760 c 8.0759, α 104.992° β 101.679° γ 99.120° Z=1319.202.413blue [6]
K2(VO)2(HPO3)2C2O4514.10monoclinicC2/ca 17.75 b 6.370 c 13.977, β 115.42° Z=414272.393blue [6]
K2MnII2(H2O)2C2O4(HPO3)2472.09hexagonalP63/ma=9.7371 c=22.49241846.82.547pink [8]
(CN3H6)2·Mn2.5(HPO3)(C2O4)2.5(H2O)·H2O [9]
piperazine[C4N2H12][MnII2(HPO3)2(C2O4)]monoclinicP21/ca=6.0627 b=10.7122 c=10.387 β=97.956 Z=2668.12.217pale pink [10]
dab = 1,4-diaminobutaneH2dab·Mn2(HPO3)2(C2O4)(H2O)2monoclinicP21/na = 5.616, b = 15.431, c = 9.445, β = 91.72(2)°, Z = 2818.2 [11]
ethylenediammonium manganese phosphite-oxalate[C2N2H10][Mn2II(OH2)2(HPO3)2(C2O4)]monoclinicP21/ca 7.837 b 8.755 c 10.100, β 100.605° [12]
bis(1-(3-ammoniopropyl)imidazolium) tetrakis(μ-dihydrogen phosphato)-tetrakis(μ-oxalato)-tetra-manganesH2api·Mn2(H2PO4)2(C2O4)2triclinicP1a=7.6108 b=9.8476 c=15.2437, α=100.023° β=102.032° γ=110.612° [13]
(C6H14N2)0.5Mn(H2PO3)(C2O4) [14]
1,4-diazabicyclo[2.2.2]octane (DABCO)[C6N2H14]2[FeIII2F2(HPO3)2(C2O4)2]·2H2OmonoclinicP21/na=12.51 b=6.372 c=33.153 β=90.532 Z=42643.01.875colourless; chains [15]
TREN[C6N4H21]2[FeII4(HPO3)2(C2O4)5]·5H2OtriclinicP1a=8.719 b=8.827 c=15.908 α=78.617 β=84.047 γ=68.241 Z=21114.11.770brown; network [15]
[FeIII2(OH2)2(HPO3)2(C2O4)]·H2OmonoclinicP21/ca=4.875 b=17.707 c=6.984 β=106.728 Z=4577.462.368colourless [15]
ethylenediammonium[C2N2H10][FeII2(OH2)2(HPO3)2(C2O4)]monoclinicP21/ca=7.684 b=8.651 c=10.053 β=100.821 Z=4653.62.317brown [15]
BAPEN[C8N4H26][FeIII6(HPO3)8(C2O4)3]·4H2OmonoclinicP21/na=8.493 b=16.685 c=16.215 β=95.919 Z=42280.352.157colourless [15]
homopip[C5N2H14][FeII4(HPO3)2(C2O4)3]monoclinicP21/ca=7.682 b=7.726 c=18.092 β=94.443 Z=41070.82.004brown [15]
Piperazinediium bis(μ4-phosphito)-(μ4-oxalato)-bis(μ3-oxalato)-tetra-iron(ii)[C4N2H12][FeII4(HPO3)2(C2O4)3]monoclinicP21/ca 7.7286 b 7.587 c 17.9816 β 98.214° [16]
dab = 1,4-diaminobutane(H2dab)0.5·Co(H2PO3)(C2O4) [17]
[C4N2H12][Co4(HPO3)2(C2O4)3]monoclinicP21/ca=7.614 b=7.51 c=17.750 β=97.351 Z=21007.32.466 [18]
CN3H6·Co(H2PO3)(C2O4) [8]
Co(H2PO3)(C2O4)·(C2H8N)triclinicP1 [19]
Co(H2PO3)(C2O4)·(C2H8N)monoclinicP21/n [19]
Co2(H2PO3)2(C2O4)3(C6N2H16)2monoclinicP21/ca=5.8605 b=13.6144 c=19.361

β=105.582

1487.91.733pink [20]
Co2(H2PO3)2(C2O4)2(C6N2H16)monoclinicP21/ca=15.3007 b=8.2832 c=16.2601 β=113.487 Z=218902.010pink; proton conductor [20]
(C4H14N2)0.5Co(HPO3)(C2O4) [14]
bis(1,4-Diazoniabicyclo[2.2.2]octane) bis(μ3-hydrogen phosphito)-dihydroxy-bis(oxalato)-di-gallium(iii) dihydrate(C6N2H14)2[Ga2(OH)2(C2O4)2(HPO3)2]·2H2OmonoclinicP21/na 12.401 b 6.283 c 33.306 β 91.197° [21]
N,N,N',N'-Tetramethylethylenediammonium bis(μ3-hydrogen phosphito)-(μ2-oxalato)-dihydroxy-di-gallium(iii)(C6N2H18)0.5[Ga(OH)(C2O4)0.5(HPO3)]triclinicP1a 6.257 b 8.558 c 9.253, α 93.219° β 108.265° γ 106.956° [21]
bis(μ3-Hydrogen phosphito)-(μ2-oxalato)-bis(1H-imidazole)-di-gallium(iii)Ga(C2O4)0.5(C3N2H4)(HPO3)monoclinicP21/ca 8.038 b 8.709 c 11.487, β 91.85° [21]
Ga(HPO3)(C2O4)(C3N2H4)·(C3N2H5)orthorhombicPnmaa=13.288, b=6.361, c=1.5364, Z=4 [22]
[bis(1,4-dimethylpiperazinediium) tetrakis(μ2-phosphito)-tetrakis(μ2-hydrogen phosphito)-bis(μ2-oxalato)-tetra-gallium][Ga2(HPO3)2(H2PO3)2(C2O4)](C6N2H16)monoclinicP21/ca =10.183 b=12.525 c=16.295 β=98.218° [23]
[hemikis(1,4-dimethylpiperazinediium) bis(μ3-phosphito)-(μ2-hydrogen phosphito)-(μ2-oxalato)-di-gallium][Ga2(HPO3)2(H2PO3)(C2O4)](C6N2H16)0.5monoclinicC 2/ca =23.462 b= 8.1170 c =16.898, β 112.873° [23]
phen = 1,10-phenanthrolineCd2(phen)2(H2PO4)(H2PO3)(C2O4)chains [17]
Cd(C10H8N2)(HPO3)(C2O4)0.5 [14]
catena-(Piperazinedi-ium bis(μ3-hydrogen phosphito)-(μ2-oxalato)-(μ2-hydrogen phosphito)-di-indium)[C4H12N2][In2(HPO3)3(C2O4)]orthorhombicCmcma=6.555 b=15.384 c=18.135 [24]
[C4N2H12]3[In2(HPO3)2(C2O4)4].4H2O [25]
1,4-diazabicyclo[2.2.2]octane (dabco)C6H14N2[In2(HPO3)3(C2O4)]671.79orthorhombicPna21a = 12.414, b = 7.7166, c = 18.327, Z = 41755.62.542 [26]
[C4N2H12]2[In2(HPO3)3(C2O4)2].3H2O [25]
[C4N2H12]3[In4(HPO3)6(C2O4)3] [25]
[C4N2H14][In4(H2O)(HPO3)5(C2O4)2].2H2O [25]
H[In5(HPO3)6(H2PO3)2(C2O4)2]·(C4N2H11)2·H2OtriclinicP1a =7.822 b =10.626 c =13.156, α =94.720° β =92.336° γ =110.181° [27]
1-methylpiperazineIn5(HPO3)6(H1.5PO3)2(C2O4)2·(H2C5N2H12)2triclinicP1a 10.1574 b 10.4440 c 10.6857, α 70.006° β 76.100° γ 79.337° [28]
1-ethylpiperazineIn5(HPO3)6(H1.5PO3)2(C2O4)2·(H2C6N2H14)2triclinicP1a 10.1904 b 10.4327 c 10.7158, α 69.373° β 77.185° γ 79.268° [28]
dbu = 1,8-diazabicyclo[5.4.0]undec-7-eneHdbu·In2(HPO3)2(C2O4)1.5 [17]
Ba2(C2O4)(H2PO3)2531.38monoclinicC2/ca = 12.3829, b = 7.9124, c = 11.0858, β=114.788 (2)°, Z = 4986.103.534colourless [29]
[Pr(H2O)(C2O4)0.5(HPO3)]·H2O300.93triclinicP1a=6.6764 b=7.0684 c=7.8103 α=111.141° β=95.415° γ=90.457° Z=22.923 [30]
[Nd(H2O)(C2O4)0.5(HPO3)]·H2O304.26triclinicP1a=6.6544 b=7.0684 c=7.8103 α=111.160° β=95.307° γ=90.590° Z=22.985 [30]
[Sm(H2O)(C2O4)0.5(HPO3)]·H2O [30]
[Eu(H2O)(C2O4)0.5(HPO3)]·H2O311.98triclinicP1a=6.5619 b=6.9442 c=7.7412 α=111.369° β=95.495° γ=90.824° Z=23.173 [30]
[Gd(H2O)(C2O4)0.5(HPO3)]·H2O317.27triclinicP1a=6.5434 b=6.9311 c=7.7465 α=111.487° β=95.645° γ=90.833° Z=23.244 [30]
[Ho(H2O)(C2O4)0.5(HPO3)]·H2O324.95triclinicP1a=6.4628 b=6.8519 c=7.6936 α=111.646° β=95.779° γ=91.028° Z=23.421 [30]
[Er(H2O)(C2O4)0.5(HPO3)]·H2O327.28triclinicP1a=6.4400 b=6.8326 c=7.6747 α=111.654° β=95.757° γ=91.096° Z=23.487 [30]
[Tm(H2O)(C2O4)0.5(HPO3)]·H2OtriclinicP1 [30]
[Yb(H2O)(C2O4)0.5(HPO3)]·H2O333.06triclinicP1a=6.4075 b=6.8050 c=7.6647 α=111.753° β=95.858° γ=91.204° Z=23.589 [30]
[Lu(H2O)(C2O4)0.5(HPO3)]·H2OtriclinicP1 [30]

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References

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  22. ↑ "具有三维超分子结构的亚磷酸-草酸镓的溶剂热合成及结构表征（英文）--《人工晶体学报》2014年09期". www.cnki.com.cn. Retrieved 2021-09-04.
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  24. ↑ Li, Huiduan; Zhang, Lirong; Huo, Qisheng; Liu, Yunling (January 2013). "Construction of two novel indium phosphites with (3,6)- and (3,5)-connected frameworks: Synthesis, structure and characterization". Journal of Solid State Chemistry. 197: 75–80. Bibcode:2013JSSCh.197...75L. doi:10.1016/j.jssc.2012.09.017.
  25. 1 2 3 4 Ramaswamy, Padmini; Hegde, Nayana N.; Prabhu, Ramanath; Vidya, V. M.; Datta, Ayan; Natarajan, Srinivasan (2009-12-21). "Synthesis, Structure, and Transformation Studies in a Family of Inorganic−Organic Hybrid Framework Structures Based on Indium". Inorganic Chemistry. 48 (24): 11697–11711. doi:10.1021/ic901744m. ISSN   0020-1669. PMID   19911816.
  26. ↑ Li, Huiduan; Zhang, Lirong; Liu, Li; Jiang, Tianchan; Yu, Yang; Li, Guanghua; Huo, Qisheng; Liu, Yunling (October 2009). "Organic template-directed indium phosphite-oxalate hybrid material: Synthesis and characterization of a novel 3D |C6H14N2|[In2(HPO3)3(C2O4)] compound with intersecting channels". Inorganic Chemistry Communications. 12 (10): 1020–1023. doi:10.1016/j.inoche.2009.08.011.
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  29. ↑ Iveson, Samuel J.; Johnston, Chloe B.; Harrison, William T.A. (2011-06-08). "Barium Oxalates Combined with Oxo-Anions and Organic Cations: Syntheses and Structures of Ba2(C2O4)(H2PO3)2 and C2H10N2·Ba(H2O)2(HC2O4)4". Crystals. 1 (2): 59–68. doi: 10.3390/cryst1020059 . ISSN   2073-4352.
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