Fractography

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Broken crankshaft failed from a surface defect at lower centre. The semi-elliptical beachmarks near the origin, indicate crack growth from fatigue. Hachures are the lines on fracture surface that can be traced back to the origin of the fracture. Crankshaft fatigue.jpg
Broken crankshaft failed from a surface defect at lower centre. The semi-elliptical beachmarks near the origin, indicate crack growth from fatigue. Hachures are the lines on fracture surface that can be traced back to the origin of the fracture.

Fractography is the study of the fracture surfaces of materials. Fractographic methods are routinely used to determine the cause of failure in engineering structures, especially in product failure and the practice of forensic engineering or failure analysis. In material science research, fractography is used to develop and evaluate theoretical models of crack growth behavior.

Contents

One of the aims of fractographic examination is to determine the cause of failure by studying the characteristics of a fractured surface. Different types of crack growth (e.g. fatigue, stress corrosion cracking, hydrogen embrittlement) produce characteristic features on the surface, which can be used to help identify the failure mode. The overall pattern of cracking can be more important than a single crack, however, especially in the case of brittle materials like ceramics and glasses.

Usage

A broken window Day 195 - Shut the burglar out (9293361460).jpg
A broken window

Fractography is a widely used technique in forensic engineering, forensic materials engineering and fracture mechanics to understand the causes of failures and also to verify theoretical failure predictions with real life failures. It is of use in forensic science for analysing broken products which have been used as weapons, such as broken bottles for example. Thus a defendant might claim that a bottle was faulty and broke accidentally when it impacted a victim of an assault. Fractography could show the allegation to be false, and that considerable force was needed to smash the bottle before using the broken end as a weapon to deliberately attack the victim. Bullet holes in glass windscreens or windows can also indicate the direction of impact and the energy of the projectile. In these cases, the overall pattern of cracking is vital to reconstructing the sequence of events, rather than the specific characteristics of a single crack. Fractography can determine whether a cause of train derailment was a faulty rail, or if a wing of a plane had fatigue cracks before a crash.

Fractography is used also in materials research, since fracture properties can correlate with other properties and with structure of materials.

Feature identification

Origin

An important aim of fractography is to establish and examine the origin of cracking, as examination at the origin may reveal the cause of crack initiation. Initial fractographic examination is commonly carried out on a macro scale utilising low power optical microscopy and oblique lighting techniques to identify the extent of cracking, possible modes and likely origins. Optical microscopy or macrophotography are often enough to pinpoint the nature of the failure and the causes of crack initiation and growth if the loading pattern is known.

Common features that may cause crack initiation are inclusions, voids or empty holes in the material, contamination, and stress concentrations.

Fatigue crack growth

The image of a broken crankshaft shows the component failed from a surface defect near the bulb at lower centre. The semi-circular marks near the origin indicate a crack growing up into the bulk material by process known as fatigue. The crankshaft also shows hachures, which are the lines on fracture surfaces that can be traced back to the origin of the fracture. Some modes of crack growth can leave characteristic marks on the surface that identify the mode of crack growth and origin on a macro scale e.g. beachmarks or striations on fatigue cracks.

SEM image of microvoid coalescence seen on a ductile fracture surface of 6061-T6 Al Ductile Fracture Surface 6061-T6 Al SEM.png
SEM image of microvoid coalescence seen on a ductile fracture surface of 6061-T6 Al

Microscopy

Microscopes can be used to determine the initiation point and the mechanism that caused crack growth. The information can be obtained from images of the fracture surface known as fractographs and used in constructing diagrams. A schematic fracture surface map can be used to isolate and identify the features on the surface which show how the product failed. Such a map can be a valuable way of presenting information which shows clearly how a crack was initiated which grew with time.

USB Microscopy

USB microscopes are especially useful for examining fracture surface features since they are small enough to be hand-held. A variety of camera sizes and resolution are available commercially at low cost. The camera cable plugs into the computer via a USB plug and most such devices come with illumination at the camera supplied by LED lights.

Scanning electron microscopy

Fatigue fracture in rubber brake seal showing striations at left (SEM) Brake seal fatigue.jpg
Fatigue fracture in rubber brake seal showing striations at left (SEM)

In many cases, fractography requires examination at a finer scale, which is usually carried out in a scanning electron microscope or SEM. The resolution is much higher than the optical microscope, although samples are examined in a partial vacuum and colour is absent. Improved SEM's now allow examination at near atmospheric pressures, so allowing examination of sensitive materials such as those of biological origin. The SEM is especially useful when combined with Energy dispersive X-ray spectroscopy or EDX, which can be performed in the microscope, so very small areas of the sample can be analysed for their elemental composition.

Example

Fractured breast implant catheter in SEM Fractured breast implant.jpg
Fractured breast implant catheter in SEM
Fracture map of failed breast implant Fract map1.jpg
Fracture map of failed breast implant

Breast implant

A cusp is formed where brittle cracks meet, as shown on the picture of a failed catheter (Cp). The cusp was formed by brittle failure of the catheter on a breast implant in silicone rubber. The origin of the cracks is at the shoulder at the left-hand side. Identifying such features will allow a fracture surface map to be made of the surface being studied. The implant failed because of overload, all the imposed loads being concentrated at the connection between the catheter and the bag holding salt solution. As a result, the patient reported loss of fluid from the implant, and it was extracted surgically and replaced.

In the case of the failed breast implant catheter, the crack path was very simple, but the cause more subtle. Further scanning electron microscopy showed numerous microcracks between the bag and the catheter, indicating that the adhesive bond between the two components had failed prematurely, perhaps through faulty manufacture. The material of construction of both bag and catheter, silicone rubber is a physically weak elastomer, and product design must allow for the low tear or shear strength of the material.

Maritime Patrol Aircraft

A non-critical crack occurred in the fastener hole of a lower wing plank. The plank was made from a 3.2 mm thick AA7075-T6 aluminium alloy. The time of the detection of the crack and the aircraft's counting g-meter allowed investigators to find out the load on the aircraft from use. The cracks on an SEM showed evidence and patterns of fatigue. The cyclic load and fatigue appeared to have progressively gone worse with some cracks being large and others being small in length and width indicating occasional force stronger than 2> g's. The g-meter showed that the aircraft had flown 2,500 flights, with the g force and acceleration occasionally exceeding more than 2 G's. This was more than the maximum advertised for the manufacturer. [1] The conclusion was that fatigue and cracks should be inspected regularly on old or commonly used aircraft. [1] The study also found novel ways for Quantitative fractography to be used on aircraft, which compares load history (in this case the g-meter) and records of the alloy experiencing fatigue in a lab setting with different pressure, cycles, and temperatures. The study used the database of cracks to create a model that predicts forces and crack progression.

See also

Related Research Articles

<span class="mw-page-title-main">Forensic engineering</span> Investigation of failures associated with legal intervention

Forensic engineering has been defined as "the investigation of failures—ranging from serviceability to catastrophic—which may lead to legal activity, including both civil and criminal". It includes the investigation of materials, products, structures or components that fail or do not operate or function as intended, causing personal injury, damage to property or economic loss. The consequences of failure may give rise to action under either criminal or civil law including but not limited to health and safety legislation, the laws of contract and/or product liability and the laws of tort. The field also deals with retracing processes and procedures leading to accidents in operation of vehicles or machinery. Generally, the purpose of a forensic engineering investigation is to locate cause or causes of failure with a view to improve performance or life of a component, or to assist a court in determining the facts of an accident. It can also involve investigation of intellectual property claims, especially patents. In the US, forensic engineers require a professional engineering license from each state.

<span class="mw-page-title-main">Fracture</span> Split of materials or structures under stress

Fracture is the appearance of a crack or complete separation of an object or material into two or more pieces under the action of stress. The fracture of a solid usually occurs due to the development of certain displacement discontinuity surfaces within the solid. If a displacement develops perpendicular to the surface, it is called a normal tensile crack or simply a crack; if a displacement develops tangentially, it is called a shear crack, slip band or dislocation.

<span class="mw-page-title-main">Fatigue (material)</span> Initiation and propagation of cracks in a material due to cyclic loading

In materials science, fatigue is the initiation and propagation of cracks in a material due to cyclic loading. Once a fatigue crack has initiated, it grows a small amount with each loading cycle, typically producing striations on some parts of the fracture surface. The crack will continue to grow until it reaches a critical size, which occurs when the stress intensity factor of the crack exceeds the fracture toughness of the material, producing rapid propagation and typically complete fracture of the structure.

<span class="mw-page-title-main">Stress concentration</span> Location in an object where stress is far greater than the surrounding region

In solid mechanics, a stress concentration is a location in an object where the stress is significantly greater than the surrounding region. Stress concentrations occur when there are irregularities in the geometry or material of a structural component that cause an interruption to the flow of stress. This arises from such details as holes, grooves, notches and fillets. Stress concentrations may also occur from accidental damage such as nicks and scratches.

<span class="mw-page-title-main">Fracture mechanics</span> Study of propagation of cracks in materials

Fracture mechanics is the field of mechanics concerned with the study of the propagation of cracks in materials. It uses methods of analytical solid mechanics to calculate the driving force on a crack and those of experimental solid mechanics to characterize the material's resistance to fracture.

Failure causes are defects in design, process, quality, or part application, which are the underlying cause of a failure or which initiate a process which leads to failure. Where failure depends on the user of the product or process, then human error must be considered.

Failure analysis is the process of collecting and analyzing data to determine the cause of a failure, often with the goal of determining corrective actions or liability. According to Bloch and Geitner, ”machinery failures reveal a reaction chain of cause and effect… usually a deficiency commonly referred to as the symptom…”. Failure analysis can save money, lives, and resources if done correctly and acted upon. It is an important discipline in many branches of manufacturing industry, such as the electronics industry, where it is a vital tool used in the development of new products and for the improvement of existing products. The failure analysis process relies on collecting failed components for subsequent examination of the cause or causes of failure using a wide array of methods, especially microscopy and spectroscopy. Nondestructive testing (NDT) methods are valuable because the failed products are unaffected by analysis, so inspection sometimes starts using these methods.

<span class="mw-page-title-main">Stress corrosion cracking</span> Growth of cracks in a corrosive environment

Stress corrosion cracking (SCC) is the growth of crack formation in a corrosive environment. It can lead to unexpected and sudden failure of normally ductile metal alloys subjected to a tensile stress, especially at elevated temperature. SCC is highly chemically specific in that certain alloys are likely to undergo SCC only when exposed to a small number of chemical environments. The chemical environment that causes SCC for a given alloy is often one which is only mildly corrosive to the metal. Hence, metal parts with severe SCC can appear bright and shiny, while being filled with microscopic cracks. This factor makes it common for SCC to go undetected prior to failure. SCC often progresses rapidly, and is more common among alloys than pure metals. The specific environment is of crucial importance, and only very small concentrations of certain highly active chemicals are needed to produce catastrophic cracking, often leading to devastating and unexpected failure.

In materials science, environmental stress fracture or environment assisted fracture is the generic name given to premature failure under the influence of tensile stresses and harmful environments of materials such as metals and alloys, composites, plastics and ceramics.

Corrosion fatigue is fatigue in a corrosive environment. It is the mechanical degradation of a material under the joint action of corrosion and cyclic loading. Nearly all engineering structures experience some form of alternating stress, and are exposed to harmful environments during their service life. The environment plays a significant role in the fatigue of high-strength structural materials like steel, aluminum alloys and titanium alloys. Materials with high specific strength are being developed to meet the requirements of advancing technology. However, their usefulness depends to a large extent on the degree to which they resist corrosion fatigue.

Applied spectroscopy is the application of various spectroscopic methods for the detection and identification of different elements or compounds to solve problems in fields like forensics, medicine, the oil industry, atmospheric chemistry, and pharmacology.

<span class="mw-page-title-main">Forensic materials engineering</span>

Forensic materials engineering, a branch of forensic engineering, focuses on the material evidence from crime or accident scenes, seeking defects in those materials which might explain why an accident occurred, or the source of a specific material to identify a criminal. Many analytical methods used for material identification may be used in investigations, the exact set being determined by the nature of the material in question, be it metal, glass, ceramic, polymer or composite. An important aspect is the analysis of trace evidence such as skid marks on exposed surfaces, where contact between dissimilar materials leaves material traces of one left on the other. Provided the traces can be analysed successfully, then an accident or crime can often be reconstructed. Another aim will be to determine the cause of a broken component using the technique of fractography.

<span class="mw-page-title-main">Forensic polymer engineering</span> Study of failure in polymeric products

Forensic polymer engineering is the study of failure in polymeric products. The topic includes the fracture of plastic products, or any other reason why such a product fails in service, or fails to meet its specification. The subject focuses on the material evidence from crime or accident scenes, seeking defects in those materials that might explain why an accident occurred, or the source of a specific material to identify a criminal. Many analytical methods used for polymer identification may be used in investigations, the exact set being determined by the nature of the polymer in question, be it thermoset, thermoplastic, elastomeric or composite in nature.

<span class="mw-page-title-main">Environmental stress cracking</span> Brittle failure of thermoplastic polymers

Environmental Stress Cracking (ESC) is one of the most common causes of unexpected brittle failure of thermoplastic polymers known at present. According to ASTM D883, stress cracking is defined as "an external or internal crack in a plastic caused by tensile stresses less than its short-term mechanical strength". This type of cracking typically involves brittle cracking, with little or no ductile drawing of the material from its adjacent failure surfaces. Environmental stress cracking may account for around 15-30% of all plastic component failures in service. This behavior is especially prevalent in glassy, amorphous thermoplastics. Amorphous polymers exhibit ESC because of their loose structure which makes it easier for the fluid to permeate into the polymer. Amorphous polymers are more prone to ESC at temperature higher than their glass transition temperature (Tg) due to the increased free volume. When Tg is approached, more fluid can permeate into the polymer chains.

Material failure theory is an interdisciplinary field of materials science and solid mechanics which attempts to predict the conditions under which solid materials fail under the action of external loads. The failure of a material is usually classified into brittle failure (fracture) or ductile failure (yield). Depending on the conditions most materials can fail in a brittle or ductile manner or both. However, for most practical situations, a material may be classified as either brittle or ductile.

Metallurgical failure analysis is the process to determine the mechanism that has caused a metal component to fail. It can identify the cause of failure, providing insight into the root cause and potential solutions to prevent similar failures in the future, as well as culpability, which is important in legal cases. Resolving the source of metallurgical failures can be of financial interest to companies. The annual cost of corrosion in the United States was estimated by NACE International in 2012 to be $450 billion a year, a 67% increase compared to estimates for 2001. These failures can be analyzed to determine their root cause, which if corrected, would save reduce the cost of failures to companies.

Polymer fracture is the study of the fracture surface of an already failed material to determine the method of crack formation and extension in polymers both fiber reinforced and otherwise. Failure in polymer components can occur at relatively low stress levels, far below the tensile strength because of four major reasons: long term stress or creep rupture, cyclic stresses or fatigue, the presence of structural flaws and stress-cracking agents. Formations of submicroscopic cracks in polymers under load have been studied by x ray scattering techniques and the main regularities of crack formation under different loading conditions have been analyzed. The low strength of polymers compared to theoretically predicted values are mainly due to the many microscopic imperfections found in the material. These defects namely dislocations, crystalline boundaries, amorphous interlayers and block structure can all lead to the non-uniform distribution of mechanical stress.

<span class="mw-page-title-main">Southwest Airlines Flight 3472</span> 2016 aviation accident

Southwest Airlines Flight 3472 was a regularly scheduled passenger flight operating from New Orleans International Airport in New Orleans, Louisiana to Orlando International Airport in Orlando, Florida. On August 27, 2016, the Boeing 737-7H4, with 99 passengers and five crew, 12 minutes after departure from New Orleans, was climbing through 31,000 feet and heading east over the Gulf of Mexico when the aircraft's number one CFM International CFM56-7 engine suffered an engine failure. A fan blade in the engine broke due to a fatigue crack. The separated portion of the blade rotated within the engine, moving forward, striking the engine inlet. Debris from the damaged engine inlet punctured the left side of the fuselage causing a loss of cabin pressure and damaged the wing and empennage. Oxygen masks were deployed to passengers while the crew initiated an emergency descent to 10,000 feet. The aircraft then diverted to Pensacola International Airport for a safe landing about 20 minutes later without further incident. While the aircraft sustained substantial damage, there were no injuries.

<span class="mw-page-title-main">Striation (fatigue)</span>

Striations are marks produced on the fracture surface that show the incremental growth of a fatigue crack. A striation marks the position of the crack tip at the time it was made. The term striation generally refers to ductile striations which are rounded bands on the fracture surface separated by depressions or fissures and can have the same appearance on both sides of the mating surfaces of the fatigue crack. Although some research has suggested that many loading cycles are required to form a single striation, it is now generally thought that each striation is the result of a single loading cycle.

<span class="mw-page-title-main">Fatigue testing</span> Determination of a material or structures resiliency against cyclic loading

Fatigue testing is a specialised form of mechanical testing that is performed by applying cyclic loading to a coupon or structure. These tests are used either to generate fatigue life and crack growth data, identify critical locations or demonstrate the safety of a structure that may be susceptible to fatigue. Fatigue tests are used on a range of components from coupons through to full size test articles such as automobiles and aircraft.

References

  1. 1 2 Goldsmith, N. T.; Wanhill, R. J. H.; Molent, L. (2019-02-01). "Quantitative fractography of fatigue and an illustrative case study". Engineering Failure Analysis. 96: 426–435. doi:10.1016/j.engfailanal.2018.10.013. ISSN   1350-6307. S2CID   139907051.