Glass rod

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Example of a stirring rod Stirring rod.jpg
Example of a stirring rod

A glass stirring rod, glass rod, stirring rod or stir rod is a piece of laboratory equipment used to mix chemicals. They are usually made of solid glass, about the thickness and slightly longer than a drinking straw,[ clarification needed ] with rounded ends.

Contents

Structure

Stir rods are generally made of borosilicate (commonly known as Pyrex) glass or polypropylene plastic. They are usually between 10 and 40 centimeters in length and about half a centimeter in diameter. Glass rods are created from a single length of thin glass that is then cut into smaller segments. The ends are generally rounded (for example, by flame polishing) to prevent scratching the surface of glassware during use, which may lead to cracks if the glassware is later heated. [1] Other shapes are possible, such as a flat paddle which can be used to circulate sediment, a triangular paddle to imitate a rubber policeman or a round button used to crush solids. [2] [3]

Uses

A stirring rod is used for mixing liquids, or solids and liquids.

Stir rods are used as part of proper laboratory technique when decanting supernatants because the contact helps to negate the adhesion between the side of the glassware and the supernatant that is responsible for the liquid running down the side. Using a stir rod also grants more control over the rate of flow, which is important in cases where chemicals may react violently. This process is also used to pour a large-mouthed flask or beaker into a test tube. [4]

Glass rods can also be used to induce crystallization in a recrystallization procedure, when they are used to scratch the inside surface of a test tube or beaker.

They can also break up an emulsion during an extraction. [5]

Stir rod in beaker Glass rod.jpg
Stir rod in beaker

Teaching

These are two classic physics experiments performed using glass rods.

Vanishing rods experiment

This experiment introduces students to the concept of an index of refraction in a liquid. Glass rods are placed in beakers of liquid, in this case oil and water. In water, the glass rods are visible because the refractive index of water is different for water and glass. In the oil, however, the glass rods seem to disappear because they have a refractive index very similar to that of glass, so the light does not bend as it crosses the glass/oil interface. [6]

Electrification

Glass rods can also be used to demonstrate electrification by friction. This occurs when there are two surfaces rubbing together. In this instance, rubbing a glass rod with silk transfers negative charge from it. This effect is known as the triboelectric effect and can be performed with a variety of materials. [7] Because glass rods and silk are relatively common, they are often chosen to demonstrate this effect.

See also

Related Research Articles

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<span class="mw-page-title-main">Test tube</span> Glass or plastic laboratory glassware

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<span class="mw-page-title-main">Watch glass</span> Piece of laboratory glassware

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Laboratory flasks are vessels or containers that fall into the category of laboratory equipment known as glassware. In laboratory and other scientific settings, they are usually referred to simply as flasks. Flasks come in a number of shapes and a wide range of sizes, but a common distinguishing aspect in their shapes is a wider vessel "body" and one narrower tubular sections at the top called necks which have an opening at the top. Laboratory flask sizes are specified by the volume they can hold, typically in metric units such as milliliters or liters. Laboratory flasks have traditionally been made of glass, but can also be made of plastic.

<span class="mw-page-title-main">Beaker (laboratory equipment)</span> Glass container used in laboratories

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<span class="mw-page-title-main">Fleaker</span>

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<span class="mw-page-title-main">Round-bottom flask</span> Laboratory equipment

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<span class="mw-page-title-main">Agitated Nutsche Filter</span> Type of filter for liquid

Agitated Nutsche filter (ANF) is a filtration technique used in applications such as dye, paint, and pharmaceutical production and waste water treatment. Safety requirements and environmental concerns due to solvent evaporation led to the development of this type of filter wherein filtration under vacuum or pressure can be carried out in closed vessels and solids can be discharged straightaway into a dryer.

<span class="mw-page-title-main">Eye dropper</span> Device used to transfer small quantities of liquids

An eye dropper, also called Pasteur pipette or simply dropper, is a device used to transfer small quantities of liquids. They are used in the laboratory and also to dispense small amounts of liquid medicines. A very common use was to dispense eye drops into the eye. The commonly recognized form is a glass tube tapered to a narrow point and fitted with a rubber bulb at the top, although many styles of both plastic and glass droppers exist. The combination of the pipette and rubber bulb has also been referred to as a teat pipette. The Pasteur pipette name is from the French scientist Louis Pasteur, who used a variant of them extensively during his research. In the past, there was no equipment to transfer a chemical solution without exposing it to the external environment. The hygiene and purity of chemical compounds is necessary for the expected result of each experiment. The eye dropper, both glass and plastic types, can be sterilized and plugged with a rubber bulb at the open end of the pipette preventing any contamination from the atmosphere. Generally, they are considered cheap enough to be disposable, however, so long as the glass point is not chipped, the eye dropper may be washed and reused indefinitely.

<span class="mw-page-title-main">Policeman (laboratory)</span> Plastic scraper

A policeman is a hand-held flexible natural-rubber or plastic scraper. The common type of it is attached to a glass rod and used in chemical laboratories to transfer residues of precipitate or solid on glass surfaces when performing gravimetric analysis. This equipment works well under gentle, delicate and precise requirement. A policeman also comes in various sizes, shapes, and types. Some of them come in one-piece flexible plastic version and some in stainless. The origin of the policeman and its name cannot be identified for sure but some clues led back to the 19th century from German chemist Carl Remigius Fresenius.

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An evaporating dish is a piece of laboratory glassware used for the evaporation of solutions and supernatant liquids, and sometimes to their melting point. Evaporating dishes are used to evaporate excess solvents – most commonly water – to produce a concentrated solution or a solid precipitate of the dissolved substance.

<span class="mw-page-title-main">Fritted glass</span> Finely porous glass permeable to fluids

Fritted glass is finely porous glass through which gas or liquid may pass, made by sintering together glass particles into a solid but porous body. This porous glass body can also be called a frit. Applications in laboratory glassware include use in fritted glass filter items, scrubbers, or spargers. Other laboratory applications of fritted glass include packing in chromatography columns and resin beds for special chemical synthesis.

References

  1. Henry Paul Talbot (1897). An Introductory Course of Quantitative Chemical Analysis: With Explanatory Notes and Stoichiometrical Problems.
  2. "MBL® Stirring rod, glass with button and paddle ends". Archived from the original on 2019-06-29. Retrieved 2017-08-12.
  3. "Nalgene® 6169-0010 Stirring Rod and Rubber Policeman with Flat & Triangular Paddle Ends, Polypropylene, Length: 9.75-Inch, Thermo Scientific". Archived from the original on 2018-12-27. Retrieved 2017-08-12.
  4. "Laboratory Techniques" (PDF). Archived from the original (PDF) on 2019-06-09. Retrieved 2016-02-28.
  5. "Stir Rods". orgchem.colorado.edu. Archived from the original on 2015-06-20. Retrieved 2015-07-09.
  6. "Vanishing Rods". littleshop. colostate. Oct 6, 1997. Archived from the original on 2016-03-19. Retrieved 2016-02-28.
  7. "PhysicsLAB: Electrostatics Fundamentals". dev.physicslab.org. Archived from the original on 2019-06-06. Retrieved 2016-02-28.